262 resultados para Soxhlet Extractor


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The objective of this work was to determine the ether extract content of peanut and canola seeds, with extraction in Soxhlet apparatus and with three types of processing: grinding in ball mill type; maceration in mortar and grind into micro mill after maceration in mortar. Data were analyzed in an entirely randomized design with 3 treatments and 12 replicates, submitted to variance analysis and the means were compared using Tukey test (P<0.05) with routines of the SAS statistical package. The largest percentage of ether extract was obtained in the treatment which the peanuts were subjected to a greater number of extractions (56.43%), and all treatments presented different results(P <0.05). In canola grains, it was observed that the extraction with the method of grinding in ball mill and the method of sequential extraction (macerate + ground in micro mill) were statistically similar (43.52 and 42.35% respectively), and these methods were more efficient (P <0.05) to extract the ether extract than the treatment in which the grains were only macerated. For peanut grains it was concluded that the most efficient method was the sequential one and to the canola grain, it can be used only a grinding mill as samples processing witch will be submitted to ether extract extraction.

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The efficiency of monitoring fertigation by means of porous capsule extractors is directly related to its correct placement, since the nutrients applied through fertigation have different mobility throughout the soil profile. The objective of this study was to evaluate the distributions of NO3, P, and K in the soil solution, when applied in citrus in sandy soil through drip fertigation systems, aiming to define the proper placement of the solution extractors. In order to measure the concentration of ions in the soil solution, the extractors were installed at four different distances (5, 15, 25, and 35 cm) and depths (15, 30, 60, and 90 cm) with an emitter located under the projection of the tree canopy. The experiment was conducted in a Valencia orange orchard on citrumelo Swingle rootstock, in Reginópolis/SP. The experimental design was randomized blocks and the treatment arrangement was a 4 x 4 factorial design with five repetitions. Sixteen soil solution extractors were installed per block, with a total of 80 extractors in the experiment. According to the obtained results, to determine P and K, it is recommended to install the solution extractor at 15 cm horizontal and 30 cm depth from the emitter. For NO3, the extractor recommended placement is 25 cm horizontal and 30 cm depth. The soil solution extractor proved to be a sensitive tool, capable of determining the ions mobility in the wet bulb.

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The study of growth and uptake of nutrients is important to determine the times of increased demand in order to schedule the fertigation. The present research was developed with the objective of evaluating the effects of different levels of electrical conductivity on growth and accumulation of nutrients in chrysanthemum plants under greenhouse conditions. The electrical conductivity levels on the applied solution were 1.42, 1.65, 1.89, 2.13 and 2.36 dS m-1 (bud vegetative stage); 1.71, 1.97, 2.28, 2.57 and 2.85 dS m-1 (bud stage). The dry mass of the aerial portion of the plant and the contents of macronutrients and micronutrients were determined every 14 days. The nutrient accumulation in chrysanthemum plant showed similar trend as compared to dry matter accumulation. The nutrients presented the following order of absorption: K>N>Ca>Mg>P>S (1425, 892, 184, 150, 110 and 59 mg plant-1) and Fe>Zn>B>Mn>Cu (2254, 2219, 1725, 1287, 210 μg plant-1). The content of most nutrients increased with increase in electrical conductivity of the solution, without salt effect up to EC of 2.85 dS m-1.

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This study examined the relationships between gross chemical composition and ultrasonographic characteristics of the ram testes. Ten testes from sexually mature Karakul rams were scanned ex situ with an 8-MHz linear-array transducer, in a transverse and longitudinal plane. All ultrasonograms were saved as digital images and subjected to computerized analyses. Crude protein content was determined by the Kjeldahl method, moisture was determined with an oven-drying method, and fat was measured by the Soxhlet extraction of dried samples. Mean pixel values (r = -0.64, P = 0.04), pixel heterogeneity (standard deviation of pixel values; r = -0.64, P = 0.04) and maximum pixel intensity (r = -0.76, P = 0.01) were all negatively correlated with parenchymal protein content. Pixel heterogeneity correlated directly with extractable lipids (r = 0.66, P = 0.02). The quantitative correlations between echotextural and biochemical parameters found in the present experiment confirm the utility of ultrasonographic imaging combined with computer-assisted image analysis for determining changes in testicular histophysiology. © 2013 Elsevier Ltd. All rights reserved.

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The objective of the present study was to analyze the most appropriate water depth for maintaining a good quality of Bermudas Grass (Cynodon dactylon) for soccer fields while saving water and electrical resources. Four treatments were used: T1 - irrigated with a water depth of 50% of evapotranspiration (ETo), T2 - irrigated with a water depth of 75% of ETo, T3 - irrigated with a water depth of 100% of ETo and T4 - irrigated with a water depth of 150% of ETo, all treatments were irrigated daily. The reference ETo was obtained by the Penman-Monteith method. The study was conducted in an experimental area of the Instituto Federal de Educação, Ciência e Tecnologia do Triângulo Mineiro - Campus Uberaba, Uberaba, Minas Gerais, Brazil, from June to September 2010 and from January to March 2011. Three evaluations of the variables were performed during the experimental period. The samples were obtained with the help of a cylindrical extractor with 10 cm in diameter and 30 cm in height. In each sample height and dry organic matter (leaf, root and organic material) were analyzed. The experimental design was randomized block with four treatments in five blocks. No significant differences were observed for dry matter and height (roots and organic material). The best results were those for T4 which obtained the greatest height.

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Pós-graduação em Agronomia (Agricultura) - FCA

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

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Pós-graduação em Biociências e Biotecnologia Aplicadas à Farmácia - FCFAR

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Pós-graduação em Agronomia (Energia na Agricultura) - FCA

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Pós-graduação em Agronomia (Proteção de Plantas) - FCA

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This study was to evaluate the solubility of nepheline syenite rocks and glauconite as alternative sources of K by organic humic acid arrays, citrus and coffee pods at various times from 0 to 180 days of incubation. The experiment was conducted in the fertility laboratory in the Department of Soil Science at the Federal University of Lavras in a completely randomized design with 90 treatments and 3 replications. The treatments were arranged in a factorial arrangement (2 x 3 x 7 + 3), 2 nepheline syenite rocks and glauconite incubated with water and 3 matrix organic humic acid, citric acid and coffee husk in six different incubation times of 0, 7, 15, 30, 75, 120 and 180 days, incubation were performed with the three above-mentioned organic matrix in increasing doses of 0, 1, 2, 5 and 10% humic acids and citric 0, 5, 10 20 and 40% for coffee husk. We evaluated the K2O content by different extractants soluble in 2% citric acid and water all treatments at all incubation times quoted above. Incubation and the application of organic matrix rocks nepheline syenite and generally glauconite provided a significant increase in solubility of K of the rocks studied in this work. Among the organic matrix has been observed that the coffee husk which provided the greatest release of K2O in both rocks mainly into the extractor 2% citric acid showed that the most efficient extraction K2O in all treatments.