Influência do aporte de calor e da velocidade de soldagem na tenacidade da solda HF-ERW

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Caracterização mecânica, microestrutural e avaliação da fragilização pelo hidrogênio em tubos de aço API 5L grau X65MS PSL2

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação da tenacidade à fratura na região de transição dúctil-frágil dos aços API 5L X70 e X80 utilizando a metodologia da curva mestra

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

CHARACTERIZATION OF A AISI/SAE 4340 STEEL IN DIFFERENT MICROSTRUCTURAL CONDITIONS

The 4340 are classified as ultra-high strength steels used by the aviation industry and aerospace applications such as aircraft landing gear and several structural applications, usually in quenched and tempered condition. In this situation occurs reduction of toughness, which encourages the study of multiphasic and bainitic structures, in order to maintain strength without loss of toughness. In this study, ferritic-pearlitic structure was compared to bainitic and martensitic structure, identified by the reagents Nital, LePera and Sodium Metabisulfite. Sliding wear tests of the type pin-on-disk were realized and the results related to the microstructure of these materials and also to their hardnesses. It is noted that these different microstructures had very similar behavior, concluding that all three tested pairs can be used according to the request level.

Isolation and biochemical characterization of a gamma-type phospholipase A2 inhibitor from Crotalus durissus collilineatus snake serum

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Determinação da temperatura de referência T0 da curva mestre na região de transição dúctil-frágil de aços ARBL

Materiais estruturais utilizados no projeto de equipamentos e instalações industriais podem apresentar mudança de seu comportamento à fratura quando se varia a temperatura. Este tipo de comportamento caracteriza-se pela existência de uma curva de transição, onde 3 regiões ficam bem definidas: os patamares inferior e superior e a região de transição. Na região de transição, os resultados experimentais apresentam alto espalhamento e são bastante dependentes da geometria ensaiada. Para solucionar este problema, foi desenvolvido um modelo analítico experimental, que resultou na edição da norma ASTM E1921-97. O trabalho inclui um estudo da influência de diversas rotas de tratamentos térmicos aplicadas em um aço 4130 utilizado pela indústria aeronáutica, um aço de qualidade API utilizado pela indústria petrolífera e um aço da classe A516 atualmente utilizado pela indústria nacional de vasos de pressão, na microestrutura, propriedades mecânicas de tração e tenacidade à fratura. Os resultados mostraram que o aço 4130 A450, apresentou a melhor correlação entre resistência e tenacidade entre as microestruturas pesquisadas. Este comportamento deve estar associado a rota de tratamento térmico aplicada a esta condição. O tratamento de austêmpera possibilita a formação de bainita que, tradicionalmente é conhecida por apresentar elevados valores de tenacidade. O método proposto pela ASTM pode ser considerado viável para as diversas microestruturas pesquisadas ampliando a aplicação da metodologia que recomenda o ensaio apenas para aços ferríticos. No entanto, a metodologia da Curva Mestra em materiais tratados termicamente deve ser conduzida de forma a se estabelecer parâmetros que considerem as modificações microestruturais sofridas pelo material.

Heat Treatment and Yb-Fiber Laser Welding of a Maraging Steel

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação da tenacidade CHARPY-V de um tubo de aço API 5L X70 soldado com arco submerso

This research project focused primarily on assessing the impact toughness of the weld and the base material of a steel pipe API 5L X70 submerged arc welded, used to conduct remote oil and gas (linepipes). The analysis followed strictly the Specification for Line Pipe - API 5L Standard, regarding the removal of the specimens of regions-of-proof-long section of the pipe, at 90o and 180o from the welded joint, and mechanical properties of toughness and Charpy-V, both the joint welded as the base material. Specimens of steel tube supplied by Tenaris Confab-SA were sized for tensile and Charpy-V, according to ASTM E 8M and ASTM E23, respectively. The result obtained showed that the API X70 steel tube has high Charpy-V toughness, near to each other at both 90o and 180o from the welded joint of the tube, and both higher than the weld metal. Microstructural and microhardness analysis complemented the present study

Determinação experimental da tenacidade à fratura em baixas temperaturas de tubos de aço API 5L X70

Because of the great metallurgical advances, the welded tubes by HF / ERW (High Frequency / Electrical Resistance Welding) have played a more active role in the oil and gas, gradually replacing tubes produced by other processes (UOE, SAW, and others) to deep water applications, in high and extremely low temperatures, highpressure conditions and in highly corrosive environments. However, studies have revealed that defects in the welded joints are in one of main causes of failures in pipelines. Associated with damage external and the stringent requirements of this sector, the welded joints become particularly critical for his toughness and the determination of this particular property is fundamental. This study aims to evaluate the toughness of the HF / ERW pipes in HSLA steel API X70 class, used in pipelines transport systems of gas and oil from data obtained with CTOD tests (Crack Tip Opening Displacement). The main objectives of this project are: mechanical and microstructural characterization of steels API X70 manufactured in Brazil; and evaluation of the toughness of weld process by HF / ERW steel API X70 national. After having the tests done, mechanical, chemical and metallurgical, we have the conclusion that those pipe are in agreement to API 5L 42ª edition for X70MO and the toughness behaves like the expected

Investigação experimental da tenacidade em tubos de aço API 5L X70 soldados pelo processo HF/ERW

Studies about structural integrity are very important when it desires to prevent disasters associated with flaws inherent in materials used in structural components. The welded joints in steel pipes used to conduction and distribution of oil and gas correspond to the regions most susceptible to flaw. Aiming to contribute to this research line, the present study was designed to assess experimentally the structural integrity of welded joints in steel pipes API 5L X70 used in pipeline systems. This assessment is given from tests of CTOD, whose aim is simulate in laboratory the real behaviour of crack from of his propagation on the welded joint obtained by high frequency electric resistance welding. In this case, the analyses are performed from specimens SE(B) obtained directly of steel pipe API 5L X70. The proposed methodology involves tests of CTOD at lower temperature, in order to assess the toughness of material in critical operation conditions. From performance of CTOD tests, was possible assess the toughness of welded joints in terms of quantity through CTOD parameter and in terms of quality from behaviour of curve load versus CMOD. In this study, also, sought to compare CTOD’s results obtained through rules ASTM E1820 (2008) and BS 7448 (1991). Although the two standards cited previously have adopted different parameters to calculated the value of CTOD, concluded that the values of CTOD tend to converge for a common value

Estudo do comportamento em fadiga de uma chapa de aço microligado, grau API 5L X70

In engineering, for correct designing the structural components required for cyclical stresses, it is necessary to determine a limit of resistance to fatigue, which is the maximum amplitude of the applied tension under which the fatigue failure does not occurs after a certain number cycles. The marine environment is hostile, not only by the high pressure, corrosion, but also by low temperatures. Petrol Production units, composed of the risers (pipelines connecting the oil well to the ship), are dimensioned to remain installed for periods of 20 up to 30 years, and must therefore be prepared to support various efforts, such as tidal, wind currents and everything that is related. This paper focuses on a study on the fatigue behavior of microalloyed steel, API 5L Grade X70, used to transport oil and gas by pipelines. For analysis, we obtained the curves S-N (stress vs. number of cycles) using laboratory data collected from cylindrical longitudinal and transverse specimens used in axial fatigue test in accordance with ASTM E466. The tensile tests and microhardness were performed to characterize the mechanical properties of the samples, and it was found that the values meet the specifications of the standard API 5L. To characterize microstructurally the material, it was also made a metallographic analysis of the steel under study, and the origin of the fatigue crack was investigated with the support of a scanning electron microscope (SEM).

Estudo em fadiga no aço API 5L X80 soldado pelo processo HF/ERW

The technological advancement in order to improve the methods of obtaining energy sources such as oil and natural gas is mainly motivated by the recent discovery of oil reserves. So, increasingly , there is a need for a thorough knowledge of the materials used in the manufacture of pipelines for transportation and exploration of oil and natural gas. The steels which follow the API standard (American Petroleum Institute), also known as high strenght low alloy (hsla), are used in the manufacture of these pipes, as they have, with their welded joints, mechanical properties to withstand the working conditions to which these ducts will be submitted . The objective of this study is to evaluate the fatigue behavior in microalloyed steel grade API 5L X80 welded by process HF / ERW . For this, axial fatigue tests to obtain S-N curve (stress vs. number of cycles ) were conducted. To complement the study, it was performed metallographic , fractographic , Vickers hardness tests and tensile tests to characterize the mechanical properties of the steel and check whether the values satisfy the specifications of the API 5L standard . From the fatigue tests , it was concluded that the surface finish influences directly on the fatigue life of the material

Caracterização microestrutural de junta soldada com arco submerso e análise da propagação de trincas em um tubo de aço API X 70

In this work a study of an API 5L X70 steel, which is used in the manufacture of oil and gas pipelines, has been made. This class of steel show high strength and ductility values, and has been increasingly studied due the growing demand of oil and natural gas, which in consequence, increases the needing of new pipelines to transport them. The material studied has been directly taken from a tube provided by TenarisConfab, and a special attention has been given to the fatigue crack growth rate study, which proved that a crack will grow at different rates according to the tube position where it is growing

Avaliação da tenacidade em um aço microligado, grau API, para aplicação em linhas dutoviárias de petróleo e gás

In order to study the mechanical properties of micro alloyed steel API 5L X70, a material used to manufacture pipes for pipeline transportation lines for use in oil and gas, a study was made of toughness, tensile strength, impact strength, hardness and microstructure steel. To perform these various tests were made where they can acquire the characteristics of the material. Were performed at the Faculty of Engineering in Guaratinguetá in the Department of Materials and Technology and the tensile tests, Charpy impact test, metallography and hardness testing of material API 5L X70, all tests were done with the help of technical laboratories. With these data can be an analysis of the material about his tenacity, his toughness and fragility, its hardness, its yield strength and its maximum voltage. After being asked the analyzes discussed the results showed that the micro alloyed steel API 5L X70 steel is a very tenacious, it absorbs impact energy of 300 Joules though without a break for the full body of evidence showing its tenacity

Estudo do comportamento em fadiga de um tubo de aço microligado, grau API 5L X70

This work focuses on a study on the fatigue behavior of a microalloyed steel API 5L X70, used in pipes lines to transport oil and gas. These types of steels have excellent mechanical resistance values and ductility and therefore increased their study driven by increased demand for oil and especially natural gas, which consequently raises the need to build new pipelines to transport these products. The oil extraction units, composed of the risers (pipelines connecting the oil well to the ship), are dimensioned to remain installed for periods of 20 to 30 years in the marine environment, a hostile environment for high pressure, corrosion, low temperatures and the stresses caused by the movement of water and tides. For analysis, the S-N (stress versus number of cycles) curves were obtained from data collected from bodies-of-proof cylindrical longitudinal, transverse and that one removed from the weld area of the pipe, tested in accordance with ASTM E466. Tensile tests were performed for characterizing the mechanical properties of the samples and welded joints, concluded that the values meet the specifications of the standard API 5L. To characterize microstructural material, also metallographic analysis was made of regions of the base metal and the HAZ. The results of fatigue tests demonstrated a higher life for the specimens removed from the longitudinal direction the pipe, followed by those in the transverse direction and, finally, the welded joint. The origins of the fatigue cracks were determined by scanning electron microscopy (SEM)