A temporary connection for an aluminium space frame

This thesis examines theoretically and experimentally the behaviour of a temporary end plate connection for an aluminium space frame structure, subjected to static loading conditions. Theoretical weld failure criterions are derived from basic fundamentals for both tensile and shear fillet welds. Direct account of weld penetration is taken by incorporating it into a more exact poposed weld model. Theoretical relationships between weld penetration and weld failure loads, failure planes and failure lengths are derived. Also, the variation in strength between tensile and shear fillet welds is shown to be dependent upon the extent of weld penetration achieved/ The proposed tensile weld failure theory is extended to predict the theoretical failure of the welds in the end plate space frame connection. A finite element analysis is conducted to verify the assumptions made for this theory. Experimental hardness and tensile tests are conducted to substantiate the extent and severity of the heat affected zone in aluminium alloy 6082-T6. Simple transverse and longitudinal fillet welded specimens of the same alloy, are tested to failure. These results together with those of other authors are compared to the theoretical predictions made by the proposed weld failure theories and by those made using Kamtekar's and Kato and Morita's failure equations, the -formula and BS 8118. Experimental tests are also conducted on the temporary space frame connection. The maximum stresses and displacements recorded are checked against results obtained from a finite element analysis of the connection. Failure predictions made by the proposed extended weld failure theory, are compared against the experimental results.

The removal of temporary organic binder from vitreous silicon carbide grinding wheels during firing

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Dehydroacetic acid based dioxaborine styryl dye:effective fluorescent probe for ammonia and amine detection

The newly synthesized dioxaborine dyes, derivatives of dehydroacetic acid, were tested for the detection of amines and ammonia. To discriminate the substance with efficient sensing parameters, series of ca. 20 dioxaborine dyes were synthesized and tested for reactivity with amines. The most promising one showed the fluorescent sensitivity to amines in the range of 1-4 ppm. © (2014) Trans Tech Publications.

Emergence of additional visible range photoluminescence due to aggregation of cyanine dye:astraphloxin on carbon nanotubes dispersed with anionic surfactant

Self-organization of organic molecules with carbon nanomaterials leads to formation of functionalized molecular nano-complexes with advanced features. We present a study of physical and chemical properties of carbon nanotube-surfactant-indocarbocyanine dye (astraphloxin) in water focusing on aggregation of the dye and resonant energy transfer from the dye to the nanotubes. Self-assembly of astraphloxin is evidenced in absorbance and photoluminescence depending dramatically on the concentrations of both the dye and surfactant in the mixtures. We observed an appearance of new photoluminescence peaks in visible range from the dye aggregates. The aggregates characterized with red shifted photoluminescence peaks at 595, 635 and 675 nm are formed mainly due to the presence of surfactant at the premicellar concentration. The energy transfer from the dye to the nanotubes amplifying near-infrared photoluminescence from the nanotubes is not affected by the aggregation of astraphloxin molecules providing important knowledge for further development of advanced molecular nano-complexes. The aggregation with the turned-on peaks and the energy transfer with amplified photoluminescence create powerful tools of visualization and/or detection of the nanotubes in visible and near-infrared spectral range, respectively, boosting its possible applications in sensors, energy generation/storage, and healthcare.