16 resultados para anidride maleica pirofosfato di vanadile n-butano 1-butanolo niobio

em BORIS: Bern Open Repository and Information System - Berna - Suiça


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* naissance 18.6.1876 à Zofingue,décès 15.10.1960 à Zofingue, prot., de Zofingue. Fils de Johann Franz Emil, imprimeur, et d'Elisabeth Caroline Steiner. ∞ 1) Ida Brack, 2) Emmy Mathys. Apprentissage d'imprimeur. R. reprit la petite entreprise de son père en 1898. Il en fit la principale imprimerie et maison d'édition de Suisse en adoptant et développant le procédé de l'héliogravure. R. édita de nombreuses revues et journaux, dont la Schweizer Illustrierte Zeitung dès 1911 (Schweizer Illustrierte depuis 1965), L'Illustré à partir de 1921 et le Blick dès 1959. Bibliographie – B. Meier, T. Häussler, Zwischen Masse, Markt und Macht, 2009

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This study evaluated the correlation between three strip-type, colorimetric tests and two laboratory methods with respect to the analysis of salivary buffering. The strip-type tests were saliva-check buffer, Dentobuff strip and CRT(®) Buffer test. The laboratory methods included Ericsson's laboratory method and a monotone acid/base titration to create a reference scale for the salivary titratable acidity. Additionally, defined buffer solutions were prepared and tested to simulate the carbonate, phosphate and protein buffer systems of saliva. The correlation between the methods was analysed by the Spearman's rank test. Disagreement was detected between buffering capacity values obtained with three strip-type tests that was more pronounced in case of saliva samples with medium and low buffering capacities. All strip-type tests were able to assign the hydrogencarbonate, di-hydrogenphosphate and 0.1% protein buffer solutions to the correct buffer categories. However, at 0.6% total protein concentrations, none of the test systems worked accurately. Improvements are necessary for strip-type tests because of certain disagreement with the Ericsson's laboratory method and dependence on the protein content of saliva.

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The synthesis of the three N,N′-di(4-coumaroyl)tetramines, i.e., of (E,E)-N-{3-[(2-aminoethyl)amino]propyl}-3,3′-bis(4-hydroxyphenyl)-N,N′-(ethane-1,2-diyl)bis[prop-2-enamide] (1a), (E,E)-N-{4-[(2-aminoethyl)amino]butyl}-3,3′-bis(4-hydroxyphenyl)-N,N′-(ethane-1,2-diyl)bis[prop-2-enamide] (1b), and (E,E)-N-{6-[(2-aminoethyl)amino]hexyl}-3,3′-bis(4-hydroxyphenyl)-N,N′-(ethane-1,2-diyl)bis[prop-2-enamide] (1c), is described. It proceeds through stepwise construction of the symmetric polyamine backbone including protection and deprotection steps of the amino functions. Their behavior on TLC in comparison with that of 1,4-di(4-coumaroyl)spermine (=(E,E)-N-{4-[(3-aminopropyl)amino]butyl}-3,3′-bis(4-hydroxyphenyl)-N,N′-(propane-1,3-diyl)bis[prop-2-enamide]; 2) is discussed.