Ethyl Carbamate Analysis in German Fruit Spirits and Brazilian Sugarcane Spirits (Cachaca): Improved Sample Cleanup with Automated Parallel Evaporation

The analysis of alcoholic beverages for the important carcinogenic contaminant ethyl carbamate is very time-consuming and expensive. Due to possible matrix interferences, sample cleanup using diatomaceous earth (Extrelut) column is required prior to gas chromatographic and mass spectrometric measurement. A limiting step in this process is the rotary evaporation of the eluate containing the analyte in organic solvents, which is currently conducted manually and requires approximately 20-30 min per sample. This paper introduces the use of a parallel evaporation device for ethyl carbamate analysis, which allows for the simultaneous evaporation of 12 samples to a specified residual volume without manual intervention. A more efficient and, less expensive analysis is therefore possible. The method validation showed no differences between the fully-automated parallel evaporation and the manual operation. The applicability was proven by analyzing authentic spirit samples from Germany, Canada and Brazil. It is interesting to note that Brazilian cachacas had a relatively high incidence for ethyl carbamate contamination (55% of all samples were above 0.15 mg/l), which may be of public health relevance and requires further evaluation.

Kinematic analysis in healthy and hip-dysplastic German Shepherd dogs

This study investigated kinematic patterns in clinically normal German Shepherd dogs (GSDs) compared to those with hip dysplasia and with no clinical signs of lameness. Two groups of GSDs, including 10 clinically healthy dogs (G1) and 10 with hip dysplasia (G2), were trotted on a treadmill at a constant speed. Kinematic data were collected by a 3-camera system and analysed by a motion-analysis program. Flexion and extension joint angles and angular velocities were determined for the shoulder, elbow, carpal, hip, stifle, and tarsal joints.Within each group, the differences between the right and left limbs in all kinematic variables were not significant. Minimum angle, angular displacement and minimum angular velocity did not differ between groups. Significant differences were observed in the maximum angular velocity and maximum angle of the hip joint (dysplastic. >. healthy), and in the maximum angular velocity of the carpal joint (healthy. >. dysplastic). It was concluded that, when trotting on a treadmill, dysplastic dogs with no signs of lameness may present joint kinematic alterations in the hind as well as the forelimbs. © 2012 Elsevier Ltd.

A contemplação estética como ideal do nirvana búdico

Pós-graduação em Filosofia - FFC

Geografias do drama humano: leituras do espaço em São Bernardo, de Graciliano Ramos e Pedro Páramo, de Juan Rulfo

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Martins Pena crítico-folhetinista: um espectador ideal do teatro lírico na corte

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Traços épico-brechtianos na dramaturgia portuguesa: O render dos heróis de Cardoso Pires e Felizmente há luar! de Sttau Monteiro

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Interação trófica entre cultivares de algodoeiro colorido, Aphis gossypii Glöver, 1877 (Hemiptera: Aphididae), Harmonia axyridis (PALLAS, 1773) E Eriopis connexa (German, 1824) (Coleoptera: Coccinellidae)

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Um palimpsesto em andamento: formas e reformas de uma personagem azevediana

Pós-graduação em Estudos Literários - FCLAR

Intervalo de dessecação de Urochloa ruziziensis (R. German & Evrard) Crins e seu efeito alelopático na cultura da soja RR

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Encontros e desencontros casuais: os epigramas mímicos da Antologia Palatina 5

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Geografias do drama humano: leituras do espaço em São Bernardo, de Graciliano Ramos, e Pedro Páramo, de Juan Rulfo

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Semen characteristics of captive common marmoset (Callithrix jacchus): a comparison of a German with a Brazilian colony

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Pólis vs. Oikos: a investigação do papel feminino no drama grego

This work analyzes the consequences of the intersection between the two spheres polis and oikos. It does so by examining themes present in three plays: Medea, Agamemnon and Lysistrata. The focus of the analysis is the way in which the feminine characters react to conflicts of interests in their respective situations. To fully comprehend which values correspond to which mentioned institution, the work also necessarily investigates the socialization and functions of both genders in fifth-century Athenian society. The analysis of the feminine condition in the creation myth implies the importance of the misogynistic sense of that time, which culminated in the silencing, discrediting, and systemic repression of females. The role of women in society, instilled in all girls starting in early childhood, is to succeed in marriage and domestic permanence. This lies opposite the masculine role, which was focused outside of the family center and to environments relating to war and public life. Matrimony and family, traditional female values, were threatened when overlapping with male interests, such as unavoidable war or social ascension through a different matrimonial bond. Therefore, it is possible to affirm that the opposition evident in the definitions male vs. female indicates that, in certain contexts, the interests of each element cause the conflicts present in the chosen plays