41 resultados para Extracción de contextos definitorios

em Repositório Institucional UNESP - Universidade Estadual Paulista "Julio de Mesquita Filho"


Relevância:

20.00% 20.00%

Publicador:

Resumo:

A rapid and reliable method for the determination of 25 compounds selected from four classes of pesticides in samples of fresh apples, grapes, pears, and strawberries purchased at a local supermarket, is presented. The study describes two different methods of extraction: solid-liquid extraction with acetone and supercritical fluid extraction. Clean-up was based on aminopropyl cartridge extraction followed by gas chromatography with an electron capture detector for simultaneous determinations. Confirmatory analysis was carried out by gas chromatography with mass spectrometry in the selected-ion monitoring (SIM) mode. Extraction efficiencies were directly compared and the methods were applied to the analysis of real samples. Recoveries for a majority of pesticides from standard samples at enrichment levels of 0.04-0.10 mg/ kg ranged from 77 to 96 % for both methods. The supercritical fluid extraction method showed good limits of detection (less than 0.01 mg/kg, depending on the pesticide and matrix) as well as minimizing environmental concerns, time, and laboratory effort. © 2006 Centro de Información Tecnológica.

Relevância:

20.00% 20.00%

Publicador:

Resumo:

In this article we tried to show the paths outlined during the past years by the Research Group on History of Mathematics and/or its relations with Mathematics Education (GPHM) at UNESP in Rio Claro - Brazil, as well as the contributions we believe we have made to Mathematics Education. The group's production has focused on issues that address the history of institutions and characters, linked to the history of disciplines, concepts and learning materials. Also, in broader terms of mathematics education, this article presents results from research that supports the understanding of teachers' conceptions about the use of History of Mathematics in the classroom; material on the history of mathematics accessible to the teacher; the presence of the history of mathematics in textbooks; proposed introductions of real numbers; and the subject of Analysis in teacher education and training.

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Pós-graduação em Psicologia - FCLAS

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Pós-graduação em Ciências Biológicas (Zoologia) - IBRC

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Pós-graduação em Educação - FFC

Relevância:

20.00% 20.00%

Publicador:

Resumo:

Pós-graduação em Geografia - IGCE