Rietveld analysis of mechanically activated BaCO(3)-TiO(2) system

BaTiO(3) powders were prepared through mechanical activation chemistry and analyzed by Rietveld refinement with X-ray diffraction data. Raw BaCO(3) and TiO(2) powders were dry milled for 5 and 20 h and then calcinated for 2 and 4 h at 800 degrees C. The milling process was found to have broken up the BaCO(3) and TiO(2) crystals into smaller crystals and formed only small amounts ( 1.5 wt%) of BaTiO(3). Subsequence calcinations for 2 and 4 h at 800 degrees C successfully produced large amounts (>97.7 wt%) of BaTiO(3) crystals. The calcination process also generated microstrains and crystallite-size anisotropy in BaTiO(3). An increase in the calcination time from 2 to 4 h increased the BaTiO(3) weight percentage and the crystal lite-shape anisotropy, but decreased the tetragonal distortion anisotropic microstrains in BaTiO(3) crystals. (C) 2008 International Centre for Diffraction Data.

Teatro e a dialética das linguagens: Cia Teatral Bumba Meu Baco

Este trabalho é centrado na análise específica das vivências teatrais do grupo “Cia. Bumba meu Baco”, projeto reconhecido pela PROEX desde 2006, do Campus da UNESP de Rio Claro. Desta forma, utiliza-se das experiências vividas pelo grupo durante todo o período de sua criação até o presente momento, para demonstrar como a linguagem teatral trata de assuntos da ciência geográfica e como ela pode chegar a gerar discussões e resultados no âmbito geográfico. Para isso, analisa-se em um primeiro momento a evolução da companhia, que ao longo dos anos pesquisou e trabalhou diferentes temas chegando ao seu trabalho mais relevante no ano de 2009, que utilizou como um dos métodos o teatro épico de Bertolt Brecht. Com o cunho político e social que possui, tal método ajudou o grupo a expandir a relação entre arte cênica e temas em geografia humana, além de gerar outros acréscimos a todos os que participaram direta e indiretamente deste processo

Chelating agent effects in the synthesis of mesoscopic-size superconducting particles

Several routes and procedures have been used in these last years as an effort to achieve single-phase mesoscopic-size superconducting samples. In this paper, the effects of using citric acid (CA), tartaric acid (TA) and ethylenediaminetetraacetic acid (EDTA) as chelating agents and ethylene-glycol (EG) as polyhydroxy alcohol were studied in order to establish conditions to avoid the occurrence of BaCO(3) undesirable secondary phase in YBa(2)Cu(3)O(7-delta) (YBCO). Thermal evolution of intermediate compounds formed during the calcinations process by the use of different chelating agents was traced using thermogravimetric and spectroscopic methods. The obtained results indicated that the polymer breakdown of samples prepared using EDTA occurs at higher temperatures than others chelating agents and also reduces the occurrence of BaCO(3) secondary phase as studied by X-ray diffraction measurements. Furthermore, the magnetic response of the mesoscopic-size YBCO specimens obtained was verified showing that samples present different superconducting response.

Intense blue and green photoluminescence emissions at room temperature in barium zirconate powders

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Microwave-hydrothermal synthesis of barium strontium titanate nanoparticles

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Barium titanate screen-printed thick films

Barium titanate (BT) thick films were prepared from mechanically activated powders based on BaCO(3) and TiO(2). After homogenization and milling in a high-energy vibro mill, the powders were calcined at 700 degreesC for 2 h by slow heating and cooling rates. A thick film paste was prepared by mixing BT fine powders with small amount of low temperature sintering aid and organic binder. The thick films were screen-printed on alumina substrates electroded with Ag-Pd. The BT films were sintered at 850 degreesC for 1 h. The thickness was 25-75 mum depending of number of layers. The microstructure of thick films and the compatibility between BT layers and substrate were investigated by SEM Results of dielectric property measurements are also reported. (C) 2002 Elsevier B.V. Ltd and Techna S.r.l. All rights reserved.

Screen printed barium titanate thick films prepared from mechanically activated powders

Barium titanate thick films were prepared from mechanically activated powders based on BaCO 3 and TiO 2. The thick films were screen-printed on alumina substrates electroded with Ag/Pd. The BT films were sintered at 850°C for 1 hour. The thickness was 30-75 μm depending of number of layers. The microstructure of thick films and the compatibility between BT layers and substrate was investigated by SEM. The dielectric properties were measured and the results were reported.

Fatores de crescimento e citocinas envolvidos na angiogênese de melanoma em animais selecionados pela intensidade da resposta inflamatória aguda

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Cuidado de si e a educação matemática: perspectivas, reflexões e práticas de atores sociais (1925-1945)

Pós-graduação em Educação Matemática - IGCE

Estudo exploratório sobre o desempenho em aritmética utilizando o soroban como ferramenta auxiliar

Pós-graduação em Matemática em Rede Nacional - IBILCE

Anatomical description of arterial segment of spleen of deer

The anatomosurgical segmentation of the arteries of the spleen was studied in 31 deer of the species Mazama gouazoubira and Blastocerus dichotomus by means of vascular injection with latex and vinyl acetate and radiographic examination. The arteria lienalis penetrated through the hilus lienis in 87% of the cases, whereas an extrahilar artery was present in the other cases. An extraparenchymal division of the lineal artery into two, three or four segmental arteries was observed in 74% of the cases. Anastomoses between intraparenchymal arterial branches were rare and of a reduced calibre.

Sentidos e significados do conceito de divisão provenientes de Atividade Orientadora de Ensino

Pós-graduação em Docência para a Educação Básica - FC

Interpretação racional do ensaio DPL

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Ensino e aprendizagem de matemática: o uso de recursos manipulativos em sala de aula

In this work, we understand the importance of the use of manipulative resources for learning mathematics. For both we developed a qualitative phenomenological approach. Performing a case study with nine 7th grade students of the Elementary School, we used the abacus of the integers to examine in what way the use of Abacus contributes to students learning. The choice of material was made according to the focus of research, understanding the signs rule. In the analysis and interpretation of data, highlight lines of students, subject of the research, units of meaning that allow us to say that the material using awakened interest in students Who actively participated in the research and enabled them to understand the rule of signs, to operate with integers enabled them to understand the rule of signs, to operate with integers