Cu0.5Zn0.5Fe2O4 ferrite for application as a soft magnetic material

This work involved the synthesis and characterization of Cu0.5Zn0.5Fe2O4 ferrite powders prepared by combustion reaction for use as soft magnetic materials. The powders were characterized by nitrogen adsorption (BET), XRD, Rietveld refinement, SEM, TEM and magnetic measures. The results indicate that the combustion reaction yielded crystalline powders containing spinel ferrite as the primary phase and traces of Fe2O3 as secondary phase. The crystallite size and lattice microdeformation calculated from Rietveld refinements were 36 and 0.24 nm, respectively. The micrographic analysis revealed particles smaller than 100 nm and fine particle agglomerates. The particles were approximately spherical and their size, calculated by TEM, was 29 nm. The magnetic parameters indicated that the Cu-Zn ferrite powders presented closed hysteresis loops and soft magnetic properties. © (2012) Trans Tech Publications, Switzerland.

Effect of molybdenum on the formation of Ti6Si2B in mechanically alloyed Ti-Mo-Si-B powders

This paper discusses on effect of molybdenum on the Ti6Si2B formation in mechanically alloyed and hot-pressed Ti-xMo-22Si-11B (x= 2, 5, 7 and 10 at%) alloys. High-energy ball milling and hot pressing were utilized to produce homogeneous and dense materials, which were characterized by scanning electron microscopy, X-ray diffraction, electron dispersive spectrometry, and Vickers hardness. The excessive agglomeration during milling was more pronounced in Moricher powders, which was minimized with the formation of brittle phases. Hot pressing of mechanically alloyed Ti-xMo-22Si-11B powders produced dense samples containing lower pore amounts than 1%. Ti6Si2B was formed in microstructure of the hot-pressed Ti-2Mo-22Si-11B alloy only. In Mo-richer quaternary alloys, the Ti3Si and Ti5Si3 phases were preferentially formed during hot pressing. Oppositely to the ternary phase, the Ti3Si phase dissolved a significant Mo amount. Vickers hardness values were reduced in hot-pressed Ti-xMo-22Si-11B alloys containing larger Mo amounts, which were dissolved preferentially in Ti solid solution. © (2012) Trans Tech Publications, Switzerland.

Physicochemical analysis of Ti-Si-B powder aalloys

Titanium alloys of Ti-Si-B system were manufactured by blended elemental powder method using Ti, Si and B powders as starting materials. It was found that uniaxial and isostatic pressing followed by hot pressing at around 1000°C, for 20 minutes, provided good densification of such alloys. The physicochemical studies were performed by means of scanning electron microscopy, X-ray diffraction, atomic force microscopy and microindentation/wear tests. The investigations revealed a multiphase microstructure formed mainly by α-titanium, Ti6Si2B, Ti5Si3, TiB and Ti3Si phases. The phase transformations after pressureless sintering at 1200°C was also studied by X-ray diffraction for the Ti-18Si-6B composition. As stated in some other researches, these intermetallics in the α-titanium matrix provide high wear resistance and hardness, with the best wear rate of 0.2 mm3/N.m and the highest hardness of around 1300 HV. © (2012) Trans Tech Publications, Switzerland.

High-pressure assisted sintering of Ti-20Si-10B and Ti-10Si-5B powders

This work presents the structural characterization of Ti-10Si-5B and Ti-20Si-10B (at-%) alloys produced by high-pressure assisted sintering. Sintering was performed in air at 1100 and 1200°C for 60 s using pressure levels of 5 GPa. Structural evaluation of sintered samples was conducted by means of scanning electron microscopy and energy dispersive spectrometry. Samples were successfully consolidated after sintering, which presented theoretical density values higher than 99%. The microstructures of the sintered Ti-10Si-5B and Ti-20Si-10B alloys revealed the presence of the TiSS, TiB, TiB2, Ti5Si3, Ti5Si4, TiSi, and TiSi2.phases. A small amount of Ti6Si2B was formed after high-pressure assisted sintering of the Ti-20Si-10B alloy (5GPa, 1100°C for 60 s) indicating that equilibrium structures were not achieved during short sintering times. No oxygen and carbon contamination was detected in structures of Ti-Si-B alloys after high-pressure sintering at 1100 and 1200°C without controlled atmosphere. © (2012) Trans Tech Publications, Switzerland.

Genetic and non-genetic effects on calf vigor at birth and preweaning mortality in nellore calves

The objective of the present study was to evaluate the genetic and non-genetic effects that influencevigor at birth and preweaning mortality in Nellore calves. A total of 11,727 records of births that occurred between 1978 and 2006, offspring of 363 sires, were analyzed. Poor calf vigor at birth (VB) and preweaning mortality divided into stillbirth (SB), early mortality (EM) and total mortality (TM) were analyzed as binary variables. Generalized linear models were used for the evaluation of non-genetic effects and generalized linear mixed models for genetic effects (sire and animal models). The incidences were 4.75% for VB, 2.66% for SB, 5.28% for EM, and 7.99% for TM. Birth weight was the effect that most influenced the traits studied. Calves weighing less than 22kg(females) and less than 24kg (males) were at a higher risk of low vigor and preweaning mortality. Preweaning mortality was higher among calves born from cows aged .3 and .11 years at calving compared with cows aged 7 to 10 years. Male calves presented less vigor and higher preweaning mortality than female calves. Selection for postweaning weight did not influence preweaning mortality. The heritability estimates ranged between 0.01 and 0.09 for VB, 0.00 and 0.27 for SB, 0.03 and 0.17 for EM and 0.02 and 0.10 for TM. Stillbirth should be included as a selection criterion in breeding programs of Nellore cattle, alone or as part of a selection index, aiming to reduce preweaning mortality. © 2013 Sociedade Brasileira de Zootecnia.

Leguminosas arbustivas e arbóreas de fragmentos florestais remanescentes no noroeste paulista, Brasil

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Conflitos de uso do solo em APPs na bacia hidrográfica do córrego Barra Seca (Pederneiras/SP) em função da legislação ambiental

Pós-graduação em Agronomia (Energia na Agricultura) - FCA

Efeito agudo dos exercícios com pesos sobre os níveis de leptina, adiponectina e fator de necrose tumoral alfa em adultos não treinados

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Morfoanatomia e ontogênese de Machaerium Pers. (Fabaceae: Faboideae): fruto, semente e plântula

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Ocorrência de opacidade difusa em molares decíduos como fator preditivo no diagnóstico de fluorose dentária em dentes permanentes

Pós-graduação em Ciência Odontólogica - FOA

Estudo comparativo do acúmulo de massa seca e macronutrientes por plantas de Zea mays e Ipomoea hederifolia

Two experiments were carried out under greenhouse conditions to study the accumulation and distribution of dry mass and macronutrients in maize and Ipomoea hederifolia. Plants of both species had grown, separately, in pots with sand substrate and irrigation with nutrient solution. Treatments were represented by the times of evaluation, realized in intervals of 14 days, starting at 21 days after emergence (DAE). A maize plant showed slight growth up to 30 DAE, when dry mass allocation was higher in roots and leaves (80%); while an I. hederifolia plant, up to 50 DAE, when the allocation of dry mass was higher in offshoots and leaves (79). Dry mass accumulation was almost five times greater in maize (134 g per plant) than in I. hederifolia (29 g per plant). The average values of N and K contents were greater in I. hederifolia. Maximum accumulations of macronutrients by maize were 1,431; 474; 1,832; 594; 340, and 143 mg per plant, while by I. hederifolia, 727; 52; 810; 350; 148, and 65 mg per plant, for N, P, K, Ca, Mg, and S, respectively. Mean accumulation rate of dry mass and macronutrients by maize plants was crescent up to 87 DAE, reaching the maximum value at 103 DAE; while being crescent up to 121 DAE by I. hederifolia plants, reaching the maximum value at 138 DAE. Thus, beyond the interference on harvesting process, a population of I. hederifolia also can compete with maize crop for nutrients.

Search for a new bottomonium state decaying to Upsilon(1S)pi(+)pi(-) in pp collisions at root s=8 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Angular analysis and branching fraction measurement of the decay B-0 -> K*(0)mu(+)mu(-)

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Measurement of the Upsilon(1S), Upsilon(2S), and Upsilon(3S) cross sections in pp collisions at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Measurement of the prompt J/psi and psi(2S) polarizations in pp collisions at root s=7 TeV

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)