590 resultados para determinação de corante
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
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This study aimed to establish a calibration model of a TDR equipment to determinate thewood moisture of Grevillea robusta (Cunn.). It was selected alleatory, 11 logs of Grevillea robusta (Cunn.), it was dried in a regulate electric greenhouse at 40o C. During the dry process, the moisture was determinate, periodically and systematically by gravimetric and TDR methods. Through the gravimetric method, moisture vary from 125,88% to 6,62% while the TDR method, the variation was from 119,83% to 5,79%. The best model adjusted to the wood moisture in the determination of the function of relative dielectric constant, using this technique, was the exponential 50,20 132,72 140,27 K U e − = − ⋅ , with a R2 = 0,96, with indicator of trust or performance 0,97 they were classified as very good, according to Camargo and Sentelhas (1997). The correlation between the gravimetric method (reference) and TDR, showed to be equivalent for both methodologies. It was concluded that the TDR can be used to the determination of wood moisture of Grevillea robusta (Cunn.), in a precise and fast way, once it was established it calibration.
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The Resolution number 3 of the Câmara de Educação Básica (CEB)/Conselho Nacional de Educação (CNE), published in 1998, June 26 (BRASIL, 1998), which established the National Curriculum Guidelines for High School Education, emphasizes the interdisciplinarity, in its 8th Article. However, almost fourteen years later, the reality in most of our schools is the adoption of a merely disciplinary methodology, vis-à-vis the difficulty related to educational planning activities of this kind. In this paper, we present a proposal of an interdisciplinary experimental activity that addresses the concept of surface tension, connecting physicists and chemists. The idea is that students determine the alcohol content of “cachaça” and discuss the concepts of surface tension forces between equal molecules, similar and different.
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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This paper presents a study to determine the optimal support positions in bridges, as well as the optimal relation between the spans of beams, aiming both the reduction and the unifirmization of the efforts in these structures. The mathematical problem is formulated in order to minimize the maximum bending moments, taking the coordinate of each internal support as design variable. To take into account possible location limitations, size constraints are also considered in the formulation. The software developed based on this study determines the efforts in each support for load shifting along the structure by the usage of the Displacement Method, and the optimization is performed with a mathematical programming technique. The structures analyzed from the computational implementation of the idealized model point to the validation and efficiency of the proposed procedure.
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In this paper, it is proposed an experimental activity to be developed with high school students, addressing the concepts of density and surface tension from a multidisciplinary approach among Physics, Chemistry and Mathematics. In this proposal, students are challenged to determine the alcohol content of vodkas from intensive physical properties of liquids. Two calibration curves were obtained, one for density and another for surface tension as a function of ethanol concentration in water. The alcohol levels obtained from these properties were very close to the values given by manufacturers, due the similarity of these beverages with ethanol-water binary mixtures.
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The development of the National Curriculum Parameters for High School (PCN) is established from a logic in which the disciplines are integrated and coordinated in order to promote interdisciplinarity. However, there are few didactic-pedagogic activities that enable teachers in practice to reach this goal. In this paper, we propose an experimental activity to be used with High School students, addressing the concept of viscosity from an interdisciplinary perspective between the disciplines of Physics and Chemistry. For that purpose, flow times of sucrose solutions of different concentrations will be measured in a glass Ford and these data will be used to construct a calibration curve, which will be used to determine the concentration of sucrose in artificial flavor syrup of gooseberry.
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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
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Pós-graduação em Zootecnia - FCAV
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Pós-graduação em Engenharia Mecânica - FEG
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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
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The use of pesticides to manage pest problems in agriculture has become a common practice around the world. Pesticides consist in chemical substances or biological agents that act preventing, destroying, repelling or mitigating the damage caused by pests in agriculture. In order to a successful treatment, the correct dosage of pesticide has to be applied for each kind of culture. In this context, this project aims to quantify the levels of the active ingredients Imidacloprid and Chlorpyrifos present in formulated technical products and compare with the reported in the ir commercial leaflets. The analyzes were performed by Ultra Performance Liquid Chromatography coupled to a photodiode array detector (CLUE-DAD). The identification of Imidacloprid and Chlorpyrifos in the samples was realized by comparison of the time of retention and UV spectre of those substances with the commercials patterns, resulting in a excellent method specificity of the method. In the scope of determination of active ingredients in formulated products, the method developed showed good sensitivity in the applied conditions, with suitables limits of detection (4,2.10-² mg L-¹ for Imidacloprid and 1,1.10-¹ mg L-¹ to Chlorpyrifos) and quantitation (1,4.10-¹ mg L-¹ and Imidacloprid 3,6.10-¹ mg L-¹ to Chlorpyrifos) for the concentrations found in matrices analyzed. Furthermore, good results were obtained to the method accuracy with coeficiente of variance values in the range of 0,6 to 0,7% for repeatability (intra-day) and 0,4 to 0,58% for intermediate precision (inter- day). The accuracy of the method was determined by recovery tests, the values were comprised in the range of 98 102%. According to the recommendations of the Associação Brasileira de Normas Técnicas, these values show good accuracy of the method. The concentrations obtained in the quantification of the active ingredients in formulated products showed values within permited by ABNT, 60.1% (w/v) ± 0.6%...
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The problem of dental caries in Brazil and around the world took major considerably over the years. In recent decades, with the advent of fluoridation, this problem has been alleviated. Studies have shown, however, that the lack of control in fluoridation leads to several health of the population. The strict control of fluoride levels in the water distributed, therefore, is essential. The objective of this study is to gather information on the status of fluoridation in some area of Brazil and compare different methods for the quantification of that analyte
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Pós-graduação em Cirurgia Veterinária - FCAV