Bonding ability of paste-paste glass ionomer systems to tooth structure: in vitro studies

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Erosive cola-based drinks affect the bonding to enamel surface: an in vitro study

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Influência do agente de união na resistência ao cisalhamento da interface titânio/polímero de vidro

There is little information regarding bond strengths of polyglass to metal alloys. This study evaluated the influence of bonding system on shear bond strength of a composite resin (Artglass/Heraeus Kulzer) to cast titanium (Ti). Twenty metallic structures (4mm in diameter, 5mm thick) of titanium grade I were cast shaped and abraded with 250mm aluminum oxide and separated into two groups. For each group was applied one bonding system (Siloc or Retention Flow) before opaque and dentin polymer superposition. This procedure was managed using teflon matrices. They were manipulated and polymerized according to the manufacturer's recommendations. The samples were stored in distilled water for 24 hours at 37º and thermocycled (5º and 55ºC/500 cycles). Shear bond strength tests were performed by using an Instron Universal testing machine at a crosshead speed of 5mm/min. Results were analyzed statistically with one-way ANOVA (a=0,5) and they indicated that the Retention Flow system was statistically better than Siloc (20.74 MPa and 11.65 MPa , respectively). It was possible to conclude that the bonding agent influenced the adhesion between polymer and cast titanium.

Heat treatment of pre-hydrolyzed silane increases adhesion of phosphate monomer-based resin cement to glass ceramic

This study evaluated the influence of different forms of heat treatment on a pre-hydrolyzed silane to improve the adhesion of phosphate monomer-based (MDP) resin cement to glass ceramic. Resin and feldspathic ceramic blocks (n=48, n=6 for bond test, n=2 for microscopy) were randomly divided into 6 groups and subject to surface treatments: G1: Hydrofluoric acid (HF) 9.6% for 20 s + Silane + MDP resin cement (Panavia F); G2: HF 9.6% for 20 s + Silane + Heat Treatment (oven) + Panavia F; G3: Silane + Heat Treatment (oven) + Panavia F; G4: HF 9.6% for 20 s + Silane + Heat Treatment (hot air) + Panavia F; G5: Silane + Heat Treatment (hot air) + Panavia F; G6: Silane + Panavia F. Microtensile bond strength (MTBS) test was performed using a universal testing machine (1 mm/min). After debonding, the substrate and adherent surfaces were analyzed using stereomicroscope and scanning electron microscope (SEM) to categorize the failure types. Data were analyzed statistically using two-way test ANOVA and Tukey's test (=0.05). Heat treatment of the silane containing MDP, with prior etching with HF (G2: 13.15 ± 0.89a; G4: 12.58 ± 1.03a) presented significantly higher bond strength values than the control group (G1: 9.16 ± 0.64b). The groups without prior etching (G3: 10.47 ± 0.70b; G5: 9.47 ± 0.32b) showed statistically similar bond strength values between them and the control group (G1). The silane application without prior etching and heat treatment resulted in the lowest mean bond strength (G6: 8.05 ± 0.37c). SEM analysis showed predominantly adhesive failures and EDS analysis showed common elements of spectra (Si, Na, Al, K, O, C) characterizing the microstructure of the glass-ceramic studied. Heat treatment of the pre-hydrolyzed silane containing MDP in an oven at 100 °C for 2 min or with hot air application at 50 ± 5 ºC for 1 min, was effective in increasing the bond strength values between the ceramic and resin cement containing MDP.

Resistência ao cisalhamento de diferentes sistemas adesivos no esmalte dental

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Resistência de união entre um cimento resinoso e uma cerâmica aluminizada submetida a diferentes tratamentos de superfície

Pós-graduação em Odontologia Restauradora - ICT

Influência de agentes clareadores na resistência de união de um sistema restaurador ao esmalte em função do tempo de armazenamento em saliva artificial

Pós-graduação em Odontologia Restauradora - ICT

Pré tratamento dentinário influência do condicionamento ácido, irradiação laser e hipermineralização na resistência ao cisalhamento de sistema adesivo multi uso

The disadvantages generated by the acid etching of the dentin, such as an increase in its permeability, in the surface moisture and in the potential to denature the external dentinal collagen, the formation of a fragility zone and the citotoxicity of the adhesive monomers; which are all aggravated by the depth of the dentin, have stimulated new and different treatment philosophies of the dentin. The purpose of the present study, therefore, was to investigate the effects of three dentin treatments: laser irradiation, acid etching and hypermineralization, in the shear bond strength of the SMP Plus bonding system. Sixty bovine incisors were extracted and randomly selected immediatly alter the animal's death. They were kept frozen (-18°C) for no longer than 14 days. After buccal dentinal surface had been exposed, X-Rays were taken to control the dentin thickness. The specimens were separated into two groups: (1) Control, kept in distilled water at 4ºC; (2) Mineralized, kept in hypermineralized solution at 4°C for 14 days. Each group was divided into three sub-groups according to the type of dentin treatment used: group F - followed the manufacturer instructions (acid-etching + primer + bond), group AL (acid-etching + primer + bond + laser) and group LA (laser + (laser + acid-etching + primer + bond). A composite resin standard cylinder (Z100-3M) was bond to the dentinal surface and the shear bond strength performed on a Universal lnstron machine 4301, with 500 Kg load and at 0,5mm/min. speed. The analysis of variance (ANOVA) determined that the treatments influenced the shear bond strength values (p<0,05) with the following average shearing load at failure: AL (9,96 MPa), F (7,28MPa) e LA (4,87 MPa). The interaction between the two factors analyzed Group (control and mineralized) and treatment (F, AL, LA) also influenced the shear bond strength (p<0,05). The highest values were obtained...

Avaliação dos preparos da superfície cerâmica para a colagem de acessórios ortodônticos

The purpose of this study was to evaluate the effects of two conditioning methods used to enhance the shear strength of orthodontic brackets bonded to porcelain surfaces. A total of 18 feldspathic specimens were used. The specimens were divided randomly into two groups (n = 9): group free silane, the porcelain specimens were etched with hidrofuoric acid 10% (Acid Gel-Maquira) for 4 minutes followed by adhesive-primer (Transbond XT) and the metallic brackets (Morelli Roth Light .022" x .030") were bonded with a light-cured microfilled resin (Transbond XT Light Cure Orthodontic Adhesive); group silane, the porcelain specimens were etched with hidrofuoric acid 10% (Acid Gel-Maquira) for 4 minutes followed by silane (Silano Ângelus) for 1 minute, adhesive-primer (Transbond XT) and the metallic brackets (Morelli Roth Light .022" x .030") were bonded with a light-cured microfilled resin (Transbond XT Light Cure Orthodontic Adhesive). All specimens were stored in solution of artificial saliva at ambient temperature for 24 hours. The debonding was done with shear strength through a universal testing machine (DL 500-Emic) calibrated with a fixed speed of 1mm/minute. Statical analysis was performed using the Student t test. The results indicated that in the free silane group the mean bond strength was 9,97 MPA, significantly lower than the silane group, that was 12,38 MPa (p < 0,05). The both groups were effective for bonding, although the silane group had the highest bond strength values.

Resistência de união e estabilidade de um sistema adesivo universal à dentina erodida/abrasionada após desproteinização

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação do efeito do plasma não térmico na resistência adesiva à dentina supericial e profunda

Pós-graduação em Odontologia Restauradora - ICT

Análise da interface adesiva entre pinos de fibra de vidro e dentina intrarradicular submetida à irrigação com diferentes agentes condicionantes

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Resistência de união de cimentos resinosos, convencional e autoadesivo, em substratos dentinários normal e hipermineralizado artificalmente

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Propriedades mecânicas, físico-químicas e biológica de adesivo experimental com incorporação de epigalocatequina-3-galato

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Avaliação da resistência de união da resina composta ao esmalte desmineralizado submetido à remineralização e infiltração resinosa de lesão de cárie

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)