Estabilidade de agregados de um latossolo vermelho tratado com cama de peru

Recentemente, tem ocorrido um grande aumento na produção de aves, com destaque para a carne de peru, motivado pelo aumento das exportações e a conquista de novos mercados. Como conseqüência, tem sido gerada uma grande quantidade de resíduos orgânicos com potencial impacto sobre o ambiente. A cama de peru constitui-se no principal resíduo dessa atividade avícola, e uma das formas de sua utilização é a sua disposição em solos como condicionador de suas características físicas e químicas. Assim, objetivou-se com este trabalho avaliar o efeito da aplicação da cama de peru na estabilidade de agregados de um Latossolo Vermelho Distrófico típico, sob pastagem de Brachiaria decumbens, localizado em Uberlândia, no Triângulo Mineiro, Minas Gerais. A cama de peru foi aplicada nas dosagens de: 0 (controle), 1.200, 2.400 e 4.800 kg ha-1 e 2.400 kg ha-1 + adubação mineral (36 kg ha-1 N, 60 kg ha-1 K2O e 60 kg ha-1de P2O5). As aplicações foram realizadas em janeiro de 2004 e o solo amostrado em duas épocas distintas (60 e 210 dias após aplicação) nas camadas de 0-20 e 20-40 cm para análise da estabilidade de agregados, avaliada pela percentagem total de agregados, percentagem de agregados maiores que 2mm, menores que 0,25mm e diâmetro médio geométrico (DMG). Não houve efeito das dosagens de cama de peru aplicadas na agregação do solo, entretanto, independentemente da dose aplicada houve um aumento na estabilidade de agregados, ao longo do tempo, notadamente na camada de 0-20 cm.

Escala Baptista de Depressão (Versão Adulto) - EBADEP-A: validade convergente e estabilidade temporal

Os objetivos principais desta pesquisa foram avaliar evidências de validade convergente entre a Escala Baptista de Depressão (Versão Adulto) - EBADEP-A e o Inventário de Depressão de Beck - BDI-II, além de avaliar a estabilidade temporal da EBADEP-A por intermédio do teste e reteste em um período de um mês. Fizeram parte da pesquisa 173 universitários de uma amostra de conveniência com média de idade de 24,45 (DP=8,45), a maioria mulheres (87,9%). Após um mês, 65 participantes, a maioria mulheres (90,8%), com média de 21 anos (DP=5,48) responderam novamente os instrumentos. Os resultados demonstraram, de acordo com critérios internacionais, excelentes índices de correlação entre ambas as escalas, bem como no teste e reteste, demonstrando adequadas qualidades psicométrica da EBADEP-A também nesses quesitos, comprovando outros estudos já realizados. Esses resultados e as limitações do estudo também são discutidos.

EFEITO DE SURFACTANTES NA ESTABILIDADE DE COMPOSTOS DE USO TERAPEUTICO

A critical revision of literature as regards to the drug stability in the presence of surfactants were realized. The functional groups envolved in the drug decomposition were used to the development of the discussion. The analysis indicated that the detergent effect can be used to control the rates and mechanisms of drug decomposition and to obtain specific information about the drug reactivity in the environment of pharmacological action.

ESTABILIDADE TERMICA DO PARACETAMOL EM SOLUCAO: CROMATOGRAFIA EM CAMADA DELGADA (CCD) - ESPECTROFOTOMETRIA ULTRAVIOLETA

The interference practised by the products in degradation of paracetemol when there is the application of spectrophotometry UV is the main obstruction to the execution of studies of thermic stability. The application of chromatography in slender layer to the isolation of paracetamol, besides being the excessively hard to apply was satisfactory to the desired proposal. The type and extension of degradation suffered by paracetamol in solution suggest the convenient inclusion, in the formulations, of one system antioxidant. This practice makes possible the blockage of the oxidation of p-aminophenol, produced by the hydrolytic degradation of paracetamol; this fact propitiated the diminution of the number of products of degradation in the medicine, making the use more secure. On the other hand, considering especially the methodological necessities of the present work, the presence of one antioxidant system facilitated the separation of paracetamol through the Thin Layer Chromatography and consequently optimized its quantification by Spectrophotometry UV during the study of thermic stability. The formulation proposed revealed excellent stability.

Estabilidade física de péletes protegidos por diferentes produtos impermeabilizantes

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Novos resultados sobre a estabilidade e controle de sistemas nao-lineares utilizando modelos fuzzy e LMI

Relaxed conditions for the stability study of nonlinear, continuous and discrete-time systems given by fuzzy models are presented. A theoretical analysis shows that the proposed method provides better or at least the same results of the methods presented in the literature. Digital simulations exemplify this fact. These results are also used for the fuzzy regulators design. The nonlinear systems are represented by the fuzzy models proposed by Takagi and Sugeno. The stability analysis and the design of controllers are described by LMIs (Linear Matrix Inequalities), that can be solved efficiently by convex programming techniques. The specification of the decay rate, constraints on control input and output are also described by LMIs. Finally, the proposed design method is applied in the control of an inverted pendulum.

Influência da concentração de antioxidante na estabilidade do ácido retinóico

Retinoic acid, which has been prescribed for some forms of acne since 1962, is subject to isomerization provoked by atmospheric oxygen and ambient light. Therefore it is very important to keep this material intact through the use of antioxidants. We tested two antioxidants: various concentrations of butylhydroxytoluene or BHT, widely used in cosmetic and dermatological preparations, and vitamin E, found in grape oil, an ingredient of skin lotion. Recently prepared lotions were subject to heat stress and the residual concentrations of retinoic acid determined at predetermined intervals through UV spectrophotometry. The shelf life of the various preparations were determined by the Arrhenius equation. The antioxidants helped conserve the retinoic acid, however, there was no synergism in antioxidant activity between the vitamin E in the grape seed oil and BHT.

Utilização de índices de estabilidade transitória para a avaliação de segurança dinâmica

Indices that report how much a contingency is stable or unstable in an electrical power system have been the object of several studies in the last decades. In some approaches, indices are obtained from time-domain simulation; others explore the calculation of the stability margin from the so-called direct methods, or even by neural networks.The goal is always to obtain a fast and reliable way of analysing large disturbance that might occur on the power systems. A fast classification in stable and unstable, as a function of transient stability is crucial for a dynamic security analysis. All good propositions as how to analyse contingencies must present some important features: classification of contingencies; precision and reliability; and efficiency computation. Indices obtained from time-domain simulations have been used to classify the contingencies as stable or unstable. These indices are based on the concepts of coherence, transient energy conversion between kinetic energy and potential energy, and three dot products of state variable. The classification of the contingencies using the indices individually is not reliable, since the performance of these indices varies with each simulated condition. However, collapsing these indices into a single one can improve the analysis significantly. In this paper, it is presented the results of an approach to filter the contingencies, by a simple classification of them into stable, unstable or marginal. This classification is performed from the composite indices obtained from step by step simulation with a time period of the clearing time plus 0.5 second. The contingencies originally classified as stable or unstable do not require this extra simulation. The methodology requires an initial effort to obtain the values of the intervals for classification, and the weights. This is performed once for each power system and can be used in different operating conditions and for different contingencies. No misplaced classification o- - ccurred in any of the tests, i.e., we detected no stable case classified as unstable or otherwise. The methodology is thus well fitted for it allows for a rapid conclusion about the stability of th system, for the majority of the contingencies (Stable or Unstable Cases). The tests, results and discussions are presented using two power systems: (1) the IEEE17 system, composed of 17 generators, 162 buses and 284 transmission lines; and (2) a South Brazilian system configuration, with 10 generators, 45 buses and 71 lines.

Variabilidade espacial da estabilidade de agregados e matéria orgânica em solos de relevos diferentes

Soils submitted to the same management system in places with small relief variation manifest different spatial variability on their attributes. The objective of this work was to evaluate the spatial variability of the geometric medium diameter, aggregates in the >2 mm class, aggregates in the 2-1 mm class and organic matter of an Oxisol under culture of the sugarcane. Samplings of the soil in regular intervals of 10 m, in grid form, totaling 100 points, collected in the depths of 0.0-0.2 m and 0.2-0.4 m were made. Data were submitted to descriptive statistics, geostatistics and in sequence to kriging analyzes. Values of the variation coefficient were low for organic matter in the depth of 0.0-0.2 m, mean in the depth of 0.2-0.4 m, high for geometric medium diameter and mean for aggregates in the >2 mm class, aggregates in the 2-1 mm class in all studied depths. The occurrence of space dependence was observed for all the variables, and the largest ones were observed in the depth of 0.0-0.2 m. Small variations in the forms of the relief condition spatial variability differentiated for organic matter and stability of aggregates in the studied depths.

Estudo da estabilidade de lipossomas compostos de fosfatidilcolina de soja e fosfatidilcolina de soja hidrogenada adicionados ou não de colesterol por método turbidimétrico

Liposomes are structures composed by phospholipids as soy phosphatidylcholine (PC) and hydrogenated soy phosphatydylcholine (PCH). Among the methods used to prove liposomes stability, turbidity method is widely used. The objective of this work was to study the liposomes stability containing PC or PCH with and without cholesterol (CHOL) by turbidity method. Liposomes were stored a 30°C during 90 days and periodically absorbance readings at 410 nm were made to verify possible turbidity alterations. Increases in the turbidity with time occurred for PC liposomes. In the presence of CHOL higher turbidity was obtained probably reflecting the increase in the size of liposomes. For PCH liposomes the presence of CHOL did not affect the turbidity suggesting higher physical stability of the structures.

Polimorfismo da beta-lactoglobulina não afeta as caracterí sticas físico-químicas e a estabilidade do leite bovino

The objective of this study was to evaluate the effect of beta-lactoglobulin polymorphism, breed and seasonality on physico-chemical characteristics and stability of bovine milk. Six Holstein-Zebu (H-Z) and five Holstein dairy herds were selected, of which 660 Holstein and 293 crossbred Holstein-Zebu milk and blood samples were collected, adding up 953 samples, distributed in two collecting periods at rainy and two at dry seasons. Each milk sample was analyzed for titratable acidity, pH, freezing point and milk ethanol stability, at the following ethanol concentrations: 70, 76, 80 and 84GL. Individual blood samples were submitted to polymerase chain reaction (PCR) for the determination of beta-lactoglobulin polymorphism. No effect of beta-lactoglobulin polymorphism was observed in physico-chemical characteristics of milk, in both studied breed. Breed effect for Holstein and H-Z, respectively, was observed on titratable acidity (16.16 and 17.07°D, while effect of seasonality (for rainy and dry seasons, respectively) was also observed on freezing point (-0.5411 and -0.5376°H). Effects of breed and seasonality on milk stability were observed (Holstein-Zebu milk was less stable on dry season), however, no effect of beta-lactoglobulin on milk stability was observed.

Avaliação da capacidade imunoestimulante e da estabilidade de um probiótico empregado em rações de cães

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Protocolo para ensaios físico-químicos de estabilidade de fitocosméticos

The growing demand for stable, safe and effective cosmetics has required increasingly complex studies by the scientific community and the use of more efficient techniques to determine the stability of these products. The use of active principles from the Brazilian flora has led to the development of numerous products, in the most varied pharmaceutical forms, making it, even more difficult to standardize experimental protocols to certify the stability of cosmetic preparations. While in Brazil there is no one protocol that standardizes the tests that should be carried out to determine product stability, several studies have been conducted in academic laboratories to determine the stability of specific raw materials. The rheological properties of topical use products have to be taken into account in their manufacture, storage and application. The determination of the rheological behavior of a formulation helps in evaluating the physicochemical nature of the vehicle, allowing early signs of physical instability to be detected and thus enabling quality control of the constituents, test formulations and final products. Thermal analysis has also been used to assist in the study of cosmetic stability and differential scanning calorimetry to guide the development of new products. Other tools, such as fluorimetry and laser granulometry can be used to help the study and development of both emulsified and non-emulsified systems. The aim of the present study is to develop a protocol for the investigation of the physical and chemical stability of phytocosmetics - systems containing active compounds extracted from the Brazilian biodiversity.