371 resultados para Solution heat treatment
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The aim of this study was to verify the carrot cooking most suitable method to minimize nutrient losses. Carrot peel slices were subjected to pre cooking tests that were initiated with 0.5 min of duration and then increased in 0.5 min successively. The carrot pieces texture was monitored during the pre tests so all would havethe same texture independent of the type of cooking. The degree of softennes was evaluated by pressuring the pieces between the toes. The carrot pulp and pell were subjected to four types of heat treatment (pressure, immersion, microwave, and steam), after that they were pounded with a food processor and stored at -18 ºC. The nutritional analyses were as follow: The evalu determination of proteins, lipids, fibers, sugars reducers, total of ascorbic acid content and minerals (iron, calcium, zinc, magnesium, potassium, phosphorus, and calcium). The analyses were accomplished with fresh carrot and after cooking with the different methods. The peel of the carrot presented as amounts of proteins, lipids, fibers percentages, sugars reducers, total and ascorbic acid content equivalent to the pulp. In addition, the minerals content was superior in the peel in relation to the pulp, presenting respective percentages of 38,10%, 95,12%, 47,04%, 58,88%, 70,27% and 21,27%. There were nutrient losses in relation to the raw vegetable, when the carrot pieces were submitted to the different cooking methods. The methods of steaming and microwave had lower nutritional losses.
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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
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Pós-graduação em Engenharia Mecânica - FEG
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Pós-graduação em Ciência dos Materiais - FEIS
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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
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Pós-graduação em Química - IQ
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The present work aims to study one-dimensional nanomaterials semiconductors grown via by phase systems Grande oxides Technological Interest for applications in gas sensors. The Used material was tin oxide (SnO2) for their functional properties, and the grow method was the Polymeric Precursors. The films grown were the nanomaterials about substrates of alumina, deposited via spin coating technique, followed by heat treatment at 300C for 1 hour and 650C for 2 hours. Later the films of Performance sensors (sensitivity, speed response, selectivity, and stability) will be in avaliated in a hermetic chamber with controlled atmosphere and temperature. The synthesized materials were its structural and morphological properties characterized in atomic force microscopy (AFM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and transmission electron microscopy (not have this result with Me). We sought to investigate one influence of different conditions for obtaining films (Variation Layers number) in structural and microstructural properties of semiconductors oxides. The synthesis method proved very effective, generating films with micro definitely, uniformity of the nanoparticles and hum high level of porosity, what makes the material of a viable final paragraph applicability
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With advances in health care, has been na increase of demand for material that could replace the functions of the human body parts, thus evolved biomedic prosthesis which today are responsible for the constant improvement of the quality of life. The Titanium alloys are widely used as implants due to its properties, like high mechanical resistance, biocompatibility and corrosion resistance, and the addition alloying elements like Zirconium, may improve some of those properties. Such properties are related to the microstructure and consequently to the type of processing performed. The purpose of this dissertation was to characterize the experimental alloy Ti15Zr after route of processsing and heat treatment in order to extend the knowledge about this alloy. The latter has been abtained by fusion of pure metals in a arc melting furnace with an inert argon atmosphere. The material has been homogenized in a tube furnace at 950ºC for 24h and cold worked by swaging, after that, bars with 10 mm of diameter were obtained by the process of rotary forging. The samples were solubilized at 900º C for 2 hours and quenched in water. After that, 4 samples were submitted to the aging, at 400º C, 450º C, 500º C and 550º C. The microstructure and phase analysis was done by optical microscopy and X-rays diffraction (XRD), the mechanical characterization was carried out by microhardness test and finally, evaluation of corrosion resistance of the alloy by electrochemical tests. The XRD and the optical microscopy made it possible to analyze that the heat treatment influenced the phase shifting from α to α', and probably affected the alloy hardness, at the first aged sample at 500º Chas been a sudden increase in the value of hardness, probably by appearance of omega phase, unwanted phase to the medical application duo to great fragility, and finally ... (Complete abstract click electronic access below)
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The multiphase steels are gaining increasing attention in scientific studies because of the different mechanical and microstructural properties that the material can achieve under different thermomechanical and heat treatments that can be submitted. In the present study, it was made a microstructural study thru the triple attack technic associated with optical microscopy and mechanical characterization of medium carbon AISI 4350 steel thru a tensile strength test, subjected to three routes of heat treatment: annealing, quenching and tempering and isothermal annealing. It was verified the predominance of ferrite-perlite constituent in the specimen annealed, martensitic in the quenched and tempered specimen and bainitic in the annealed isothermally specimen. The annealed material showed a higher ductility, while the hardened and tempered specimen showed the highest hardness and ultimately the bainitic specimen showed a combination of the two abovementioned mechanical properties. Thus, we proved that the multiphase steel SAE 4350 can be a versatile material with great potential for various industrial applications
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In a market environment increasingly competitive, the companies need to control of this process accurately, avoiding rework or rejection of materials during industrialization. This can be achieved by defining procedure that assure the maintenance of the materials characteristics, as specified initially in the projects. This graduation work has the objective of defining the best heat treatment parameter of normalizing for Heads, part of a pressure vessel, formed in P275NH material. The methodology applied is based on the execution of a sequence of Heat Treatments, using different parameters. The process variables were the cooling velocity, the hold time and the hold temperature variation. As a result of this study, it is noticed that the mechanical properties of the materials are strongly influenced by the hold temperature variation and by the cooling velocity, both determined for the heat treatment cycle
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Due to the large use of steel in several processes around the world, there is the increasingly concern to find new materials and/or optimization and improvement of the processes, as the need to reduce the cost and a productivity increase in the primary industry, such as the siderurgy. The rolling is the most used mechanical process in the world and therefore is required the development of new tools in high volume and with optimum characteristics to support the market demand. Forged rolls used are for rolling. These rolls have heat treatment that has the purpose to achieve the appropriated mechanical properties to support the variables of the rolling process. The objective of this work is to analyze the hardness profile and the microstructure a tool steel similar to AISI A2, forged in an opened die process and submitted to heat treatment with water-cooling. The results allowed plotting a hardness profile and performing a microstructure analysis, and whereby to confirm that the heat treatment is not a quenching, but it is a material beneficiation by the hardening of superficial layer, since there is no martensitic microstructure. Therefore, this paper provides the support to future studies about the possibility to perform enhancements in this thermal heat made in the rolls produced at Gerdau Plant in Pindamonhangaba