Desenvolvimento de detector eletroquímico para cromatografia líquida de alta eficiência baseado em um eletrodo modificado com nanopartículas metálicas para determinação de ácidos carboxílicos em vinhaça de cana-de-açúcar

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Boro em cana-de-açúcar cultivada em solução nutritiva

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Experimental and numerical study of heat transfer in hot machined workpiece using infrared radiation

One of the greatest problems found in machining is related to the cutting tool wear. A way for increasing the tool life points out to the development of materials more resistant to wear, such as PCBN inserts. However, the unit cost of these tools is considerable high, around 10 to 20 times compared to coated carbide insert, besides its better performance occurs in high speeds requiring modern machine tools. Another way, less studied is the workpiece heating in order to diminish the shear stress material and thus reduce the machining forces allowing an increase of tool life. For understanding the heat transfer influences by conduction in this machining process, a mathematical model was developed to allow a simplified numerical simulation, using the finite element method, in order to determine the temperature profiles inside the workpiece.

Ultra-precision face grinding with constant pressure, lapping kinematics, and SiC grinding wheels dressed with overlap factor

Several machining processes have been created and improved in order to achieve the best results ever accomplished in hard and difficult to machine materials. Some of these abrasive manufacturing processes emerging on the science frontier can be defined as ultra-precision grinding. For finishing flat surfaces, researchers have been putting together the main advantages of traditional abrasive processes such as face grinding with constant pressure, fixed abrasives for two-body removal mechanism, total contact of the part with the tool, and lapping kinematics as well as some specific operations to keep grinding wheel sharpness and form. In the present work, both U d-lap grinding process and its machine tool were studied aiming nanometric finishing on flat metallic surfaces. Such hypothesis was investigated on AISI 420 stainless steel workpieces U d-lap ground with different values of overlap factor on dressing (Ud=1, 3, and 5) and grit sizes of conventional grinding wheels (silicon carbide (SiC)=#800, #600, and #300) applying a new machine tool especially designed and built for such finishing. The best results, obtained after 10 min of machining, were average surface roughness (Ra) of 1.92 nm, 1.19-μm flatness deviation of 25.4-mm-diameter workpieces, and mirrored surface finishing. Given the surface quality achieved, the U d-lap grinding process can be included among the ultra-precision abrasive processes and, depending on the application, the chaining steps of grinding, lapping, and polishing can be replaced by the proposed abrasive process.

Avaliação do estado nutricional de mudas de Gonçalo Alves (Astronium Fraxinifolium)

The planting of seedlings, the establishment and maintenance of the natural regeneration process, or the combination thereof, are methods used in the recovery of degraded or disturbed environments, however, often require the addition of soil conditioners. This study aimed to evaluate the influence of conditioners, introduced in degraded soil on growth and nutritional status of Astronium fraxinifolium seedlings. To conduct the experimentation were used as degraded soil conditioner, ash from sugarcane bagasse (CZ) and macrophytes (MC), at the doses of 0, 15, 30 and 45 t ha-1 and 0, 16 and 32 t ha-1 respectively, which combined produced 12 treatments, with three replications, and for field installation, was used the experimental randomized block design. Astronium fraxinifolium (Gonçalo Alves) seedlings, native tree species in cerrado, were introduced in the experimental area and, after 12 months, were evaluated for leaf concentration of nitrogen, phosphorus, potassium, calcium, magnesium, sulfur, boron, copper, iron, manganese and zinc (N, P, K, Ca, Mg, S, B, Cu, Fe, Mn and Zn, respectively). Seedlings and adult plants of A. fraxinifolium were collected in preserved cerrado reserve were also analyzed for nutrients foliar concentration to perform a comparative analysis. The leaves collection in the preserved cerrado and experimental area, was accompanied by soil sampling (0.0 - 0,20 m deep), which was analyzed for phosphorus, OM (organic matter), pH, K, Ca, Mg, Al+H (potential acidity), Al (aluminum), Cu, Fe, Mn and Zn. The results show that the applied residues contributed to raise the foliar concentration of Cu and Fe. The foliar concentration of nutrients was higher in A. fraxinifolium seedlings from preserved cerrado, except for B, which was similar between areas, besides Cu and Fe with higher levels in the seedlings from experimental area. The combined addition of residues (MC and CZ), led to increase the plants height and diameter. This...

Reguladores vegetais e nutrientes minerais no metabolismo de plantas de tomateiro

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Análise do acabamento superficial e da potência consumida na usinagem de fresamento frontal e cilíndrico tangencial da madeira de eucalipto

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Doses e modos de aplicação de boro na produção de mudas de nespereira

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Efeito das diferentes direções de aplicação de jato de fluido de corte no torneamento de um aço de difícil usinagem

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Acúmulo de nutrientes e resposta da alface à adubação fosfatada

Nutrient absorption and response of lettuce to phosphorus fertilization. The objective of this study was to evaluate the response of lettuce (cultivar Verônica) to different levels of phosphorus fertilization. The experiment was conducted from 25/09/2003 (sowing) to 03/12/2003 (harvesting) at the Fazenda Experimental São Manuel, UNESP/FCA, Botucatu/SP, under protective structures. The experiment was conducted in a randomized block design, with five treatments (0, 200, 400, 600 and 800kg.ha-1 of P2 O5, in the form of triple superphosphate) and five replications. Plants were grown in 13L plastic pots containing Latossolo Vermelho Distrófico Típico. A quadratic response was observed for the fresh mass of the plant shoots and leaf area, with maximum equivalent levels of 733 and 756kg.ha-1 of P2 O5 , respectively, as well as for potassium, calcium, magnesium, sulfur, boron, copper, iron, manganese and zinc accumulation. Linear increases were observed with the treatments of P2 O5 for dry mass of the shoots, leaf number, plant height and nitrogen and phosphorus accumulation.

Soil fertility, nutrition and early growth of physic nut as affected by nitrogen fertilization

The initial growth and mineral nutrition of the physic nut (Jatropha curcas L.) as a function of nitrogen (N) fertilization was investigated. The transplanting of seedlings was carried out in plastic pots filled with 50 dm3 of a Rhodic Hapludox, under a plastic greenhouse. In addition to a control treatment, the dosages of 0, 40, 80, 120, and 160 mg dm−3 N were tested. The results demonstrated that N fertilization for the cultivation of physic nut could be added as top dressing from 60 days after planting with a dosage of 65 mg dm−3. A SPAD index of 46 can be used as a nutritional reference to its initial development. Furthermore, the results suggested that the order of nutrient accumulation by the physic nut plants is as follows: potassium (K) > N > magnesium (Mg) > calcium (Ca) > phosphorus (P) > sulfur (S) > iron (Fe) > manganese (Mn) > boron (B) > zinc (Zn) > copper (Cu).

Doses e modos de aplicação de Boro e adubação com Zinco na cultura do milho

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Usinagem do alumínio da classe 6005 com uso de ferramenta cerâmica

The machining process is so much important in the economic world. Many machining parameters have been studied to maximize results, in terms of cost and lifetime. (decrease of cutting tool wear, improved surface finish, among others). The objective of this study is to evaluate the wear of a ceramic tool in the machining of the aluminum alloy 6005 A. The analysis of the wear of the cutting tools is very important due to its big impact on the final finishing of the piece as a whole. The evaluation took place in two stages, first it was done a detailed study of the literature of the whole machining process, where the study of the formation and swarf classification were among the most important steps in this phase. The second step consisted in the machining of the piece of aluminum 6005 A with a ceramic cutting tool constituded of aluminum oxide and magnesium oxide with silicon carbide impregnation. The swarf generated in this process was then photographed with a Zeiss optical microscope and analyzed for its size and shape. Through this comparison it was concluded that the swarf are generated shear swarfs, shaped like a tangled, fragmented and arcs connected, thus classifying the material as medium difficulty machining. Through the image analysis tool it was concluded that the parameter of lower wear was the: Vc = 500m / min, f = 0.10mm / rev and ap = 0.5mm