Aplicação e contribuição da cromoendoscopia no trato digestório superior de cães, uilizando Lugol, Índigo Carmim e Azul de Metileno

Pós-graduação em Medicina Veterinária - FMVZ

Avaliação da eficácia analgésica da farmacopuntura com meloxicam e da aquapuntura preemptivas em gatas submetidas à ovariosalpingohisterectomia (OSH)

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Um estudo da dependência do índice de refração linear com a composição dos vidros teluretos dos sistemas TeO2-Li2O-TiO2 e TeO2-Li2O-WO3

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Desenvolvimento de metodologia alternativa limpa para análise de nitrito

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Soroprevalência da artrite-encefalite caprina a vírus no estado de São Paulo

Pós-graduação em Medicina Veterinária - FMVZ

Imobilização multipontual das peroxidases da casca da soja e chuchu em suportes alternativos de pó de sabugo de milho e celulose bacteriana

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Preparação de filmes finos ferroelétricos de SrBi2'('TA IND.1-x''NB IND.x)ÍND.2 'O IND.9' puro e dopado com tungstênio, obtidos pelo método dos precursores poliméricos

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Preditores de recidiva hemorrágica ou óbito na hemorragia digestiva alta por úlcera péptica ou lesão aguda da mucosa gastroduodenal

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Imagens da polícia: relações entre cidadania e violência caracterizadas nas representações da polícia paulista: janeiro/83 - março/85

Pós-graduação em História - FCLAS

Desenvolvimento de novos procedimentos analíticos para diferenciação in situ de espécies lábeis e inertes em sistemas aquáticos e para especiação de Cu(II) e Pb(II) complexados com nanopartículas de sílica

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Coordinative versatility of a Schiff base containing thiophene: Synthesis, characterization and biological activity of zinc(II) and silver(I) complexes

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

A insegurança e as novas práticas espaciais em cidades brasileiras

New real estate launch products and closed residential spaces, occurs with increasing frequency in Brazilian cities and are based on the assumption that there is a general increase in violence, as we address urban insecurity, which involves individual coping, and privatizing adept practices of exacerbated control mechanisms. We researched deployment and appropriation of residential spaces in middle cities of Sao Paulo (Brazil). We identify social representations of the others, blamed for insecurity growing, and analyzed from everyday life perspective. We hypothesized that new forms of production of urban space with a tendency to social and spatial fragmentation, generate new practices.

A simple method based on ICP-MS for estimation of background levels of arsenic, cadmium, copper, manganese, nickel, lead, and selenium in blood of the Brazillian population

Throughout the world, biomonitoring has become the standard for assessing exposure of individuals to toxic elements as well as for responding to serious environmental public health problems. However, extensive biomonitoring surveys require rapid and simple analytical methods. Thus, a simple and high-throughput method is proposed for the determination of arsenic (As), cadmium (Cd), copper (Cu), manganese (Mn), nickel (Ni), lead (Pb), and selenium (Se) in blood samples by using inductively coupled plasma–mass spectrometry (ICPMS). Prior to analysis, 200 ml of blood samples was mixed with 500 ml of 10% v/v tetramethylammonium hydroxide (TMAH) solution, incubated for 10 min, and subsequently diluted to 10 ml with a solution containing 0.05% w/v ethylenediamine tetraacetic acid (EDTA) + 0.005% v/v Triton X-100. After that, samples were directly analyzed by ICP-MS (ELAN DRC II). Rhodium was selected as an internal standard with matrix-matching calibration. Method detection limits were 0.08, 0.04, 0.5, 0.09, 0.12, 0.04, and 0.1 mg//L for As, Cd, Cu, Mn, Ni, Pb, and Se, respectively. Validation data are provided based on the analysis of blood samples from the trace elements inter-\comparison program operated by the Institut National de Santé Publique du Quebec, Canada. Additional validation was provided by the analysis of human blood samples by the proposed method and by using electrothermal atomic absorption spectrometry (ETAAS). The method was subsequently applied for the estimation of background metal blood values in the Brazilian population. In general, the mean concentrations of As, Cd, Cu, Mn, Ni, Pb, and Se in blood were 1.1, 0.4, 890, 9.6, 2.1, 65.4, and 89.3 mg/L, respectively, and are in agreement with other global populations. Influences of age, gender, smoking habits, alcohol consumption, and geographical variation on the values were also considered. Smoking habits influenced the levels of Cd in blood. The levels of Cu, Mn, and Pb were significantly correlated with gender, whereas Cu and Pb were significantly correlated with age. There were also interesting differences in Mn and Se levels in the population living in the north of Brazil compared to the south.

Bromofhenol blue discoloration using peroxidase immobilized on highly activated corncob powder

The aim of the present study was to evaluate the efficacy of peroxidase immobilized on corncob powder for the discoloration of dye. Peroxidase was extracted from soybean seed coat, followed by amination of the surface of the tertiary structure. The aminated peroxidase was immobilized on highly activated corncob powder and employed for the discoloration of bromophenol blue. Amination was performed with 10 or 50 mmol.L-1 carbodiimide and 1 mol.L-1 ethylenediamine. The amount of protein in the extract was 0.235 ± 0.011 mg.mL-1 and specific peroxidase activity was 86.06 ± 1.52 µmol min-1 . mg-1, using 1 mmol.L-1 ABTS as substrate. Ten mmol.L-1 and 50 mmol.L-1 aminated peroxidase retained 88 and 100% of the initial activity. Following covalent immobilization on a corncob powder-glyoxyl support, 10 and 50 mmol.L-1 aminated peroxidase retained 74 and 86% of activity, respectively. Derivatives were used for the discoloration of 0.02 mmol.L-1 bromophenol blue solution. After 30 min, 93 and 89% discoloration was achieved with the 10 mmol.L-1 and 50 mmol.L-1 derivatives, respectively. Moreover, these derivatives retained 60% of the catalytic properties when used three times. Peroxidase extracted from soybean seed coat immobilized on a low-cost corncob powder support exhibited improved thermal stability.

Synthesis and vibrational spectra of bimetallic compounds of the type [(NH3)(L)ZnFe(CO)4] (L = bidentate amine

New compounds with the general formulae [(NH3)(L)ZnFE(CO4] (L = ethylenediamine, N-methylethylenediamine, N,N′-dimethylethylenediamine and 1,3-propanediamine) were prepared and studied by vibrational spectroscopy. The data suggest that they may be formulated as monomers with a trigonal bipyramidal configuration around the iron atom. © 1984.