28 resultados para Electron microscopes


Relevância:

60.00% 60.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Purpose: This study aimed to evaluate the survival probability of four narrow-diameter implant systems when subjected to fatigue loading. Materials and Methods: Seventy-two narrow-diameter implants to be restored with single-unit crowns were divided into four groups (n = 18): Astra Tech (3.5-mm diameter), with a standard connection (ASC); BioHorizon (3.4-mm diameter), with a standard connection (BSC); Intra-Lock (3.4-mm diameter), with a standard multilobular connection (ISC); and Intra-Lock (3.4-diameter), with a modified square connection (IMC). The corresponding abutments were screwed onto the implants, and standardized metal crowns (maxillary central incisors) were cemented and subjected to step-stress accelerated life testing in water. Use-level probability Weibull curves and reliability for 100,000 cycles at 150 and 200 N (90% two-sided confidence intervals) were calculated. Polarized light and scanning electron microscopes were used to access the failure modes. Results: The calculated survival probability for 100,000 cycles at 150 N was approximately 93% in group ASC, 98% in group BSC, 94% in group ISC, and 99% in group IMC. At 200 N, the survival rate was estimated to be approximately < 0.1% for ASC, 77% for BSC, 34% for ISC, and 93% for IMC. Abutment screw fracture was the main failure mode for all groups. Conclusions: Although the probability of survival was not significantly different among systems at a load of 150 N, a significant decrease was observed at 200 N for all groups except IMC.

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Purpose: To evaluate and compare the reliability of implant-supported single crowns cemented onto abutments retained with coated (C) or noncoated (NC) screws and onto platform-switched abutments with coated screws. Materials and Methods: Fifty-four implants (DT Implant 4-mm Standard Platform, Intra-Lock International) were divided into three groups (n = 18 each) as follows: matching-platform abutments secured with noncoated abutment screws (MNC); matching-platform abutments tightened with coated abutment screws (MC); and switched-platform abutments secured with coated abutment screws (SC). Screws were characterized by scanning electron microscopy and x-ray photoelectron spectroscopy (XPS). The specimens were subjected to step-stress accelerated life testing. Use-level probability Weibull curves and reliability for 100,000 cycles at 200 N and 300 N (90% two-sided confidence intervals) were calculated. Polarized light and scanning electron microscopes were used for fractographic analysis. Results: Scanning electron microscopy revealed differences in surface texture; noncoated screws presented the typical machining grooves texture, whereas coated screws presented a plastically deformed surface layer. XPS revealed the same base components for both screws, with the exception of higher degrees of silicon in the SiO2 form for the coated samples. For 100,000 cycles at 300 N, reliability values were 0.06 (0.01 to 0.16), 0.25 (0.09 to 0.45), and 0.25 (0.08 to 0.45), for MNC, MC, and SC, respectively. The most common failure mechanism for MNC was fracture of the abutment screw, followed by bending, or its fracture, along with fracture of the abutment or implant. Coated abutment screws most commonly fractured along with the abutment, irrespective of abutment type. Conclusion: Reliability was higher for both groups with the coated screw than with the uncoated screw. Failure modes differed between coated and uncoated groups.

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Geological researches conducted in the past few years detected, through deep drill hole data, the presence of alkaline rocks in the region of Três Fontes-MG, where the Barbacena Group rocks, the Morro do Ferro Greenstone Belt rocks and Araxá/Canastra groups‟ rocks are exposed. This paper aimed the petrographic and chemical characterization of these alkaline rock types, which have not yet been described in the literature. Based on petrographic descriptions and geochemical and Scanning Electron Microscopy analysis, it was possible to characterize the rock in question as lamprophyre, rich in carbonates, phlogopite, pyroxene, olivine, titaniferous opaque minerals and apatite concentrations that reach 7%. This occurrence corresponds to an alkaline intrusion, which caused brecciation of host rocks, possibly indicating that the material is explosive, however, in the study area there was no evidence of volcanic activity on the surface

Relevância:

60.00% 60.00%

Publicador:

Resumo:

In this work is studied the fluid dynamic characteristics of sugarcane bagasse for gasification applications and use of syngas in the sugarcane sector. This is an experimental work, which is initially performed the particle size separation of sugarcane bagasse particles, using appropriate equipment. Through the experiment is possible to determine the average diameter of particles pomace typical sugarcane mill. The equipment used for the grading sieve separation assembly consists of several dimensions, arranged vertically and which shows adequate for good separation from the pulp. Later, it makes immediate analysis for the determination of moisture, ash, volatile materials and fixed carbon. The study also determines the gross calorific value and allows analysis of densities of particles of sugar cane bagasse. Also studied the bagasse morphology using electron microscopes, where it was possible to visualize the geometry of the particles of bagasse. The use of Electronic Scanning Microscopy (SEM) provided better understand the morphology and particle size measured by using photography methods. Two methods for determining the sphericity of the particles were also used. The experiments carried out using appropriate standards and specific equations, allowing compare the present results with the values found by several researchers. Subsequently, fluid dynamic simulations were performed for the determination of porosity and minimum fluidization velocity theoretical. It follows that the sphericity and porosity of the bagasse particles influence the minimum fluidization velocity of biomass

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Relevância:

60.00% 60.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Relevância:

40.00% 40.00%

Publicador:

Resumo:

Correlative fractography is a new expression proposed here to describe a new method for the association between scanning electron microscopy (SEM) and light microscopy (LM) for the qualitative and quantitative analysis of fracture surfaces. This article presents a new method involving the fusion of one elevation map obtained by extended depth from focus reconstruction from LM with exactly the same area by SEM and associated techniques, as X-ray mapping. The true topographic information is perfectly associated to local fracture mechanisms with this new technique, presented here as an alternative to stereo-pair reconstruction for the investigation of fractured components. The great advantage of this technique resides in the possibility of combining any imaging methods associated with LM and SEM for the same observed field from fracture surface. © Microscopy Society of America 2013.

Relevância:

30.00% 30.00%

Publicador:

Resumo:

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)