204 resultados para bromine and iodine determination


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The aim of the present study was to investigate the occurrence of Leishmania sp. infection in dogs (N = 491) living in the municipality of Florianópolis, Santa Catarina (SC), Brazil, which was considered a disease-free region for visceral leishmaniasis until 2011, when autochthonous cases of canine disease were notified. Seroprevalence in this population was assessed by ELISA (0.4%; 2/491) and IFAT (4.09%; 24/491). Only one dog exhibited seroreactivity in both serological methods, comprising a total of 25 (5.3%) seroreagent animals. Leishmania sp. DNA, obtained from a sample of whole blood of this animal, was amplified by both conventional and Real-Time PCR. Sequencing of the amplified DNA and, thereby, determination of the Leishmania species involved, was not possible. Our results suggest the necessity of a thorough epidemiological investigation in Florianópolis. (AU).

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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One of the main tendencies of leprosy worldwide is the simultaneous action of non governmental organizations and official agencies operating eventual different strategies. This paper aims to contribute to such question focusing on some outstanding aspects of respective contemporary evolution. METHODS Application of bibliographic review and contents analysis techniques to primary data from a circumstancial set of open circulation specific publications. RESULTS Successive disagreements registered between both parts refer to the objective to be attained by the fight against the disease, if control or elimination. CONCLUSIONS New perspectives of jointed actions are being searched for now when priority on endemics control is more realistically assumed and social determination is been really considered.

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The present work sought to discriminate, to map and to quantify the areas of soil use of the Stream Monte Belo watershed - Botucatu (SP), obtained by digitale images. The cartographic bases were the shart planialtimetric, edited by IBGE (1969) and the satellite images LANDSAT - 7, passages of 21/01/1999, 08/01/2003 and 23/10/2006. The Software Idrisi Andes 15.0 were used for conversion of the analogical information for digital and for determination of the vegetable coverings areas. The results allowed to verify that the SIG - IDRISI Andes 15.0 were efficient in the quantification of the areas with soil use and that the analysis of the data showed a cash progress of the areas of reforestations to the detriment of the areas of pastures, especially from 1999, 2003 to 2006, when the field areas were substituted by the forestry in his totality. In spite of that progress, the forest areas that you correspond to the Permanent Preservation Areas, They are considerably preserved. That result comes to the encounter of the tendency of expansion of the forestry, especially after the installation of cellulose industries in the area, what worsened the environmental problems originating from of the practice of the monoculture.

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The land use conservation planning requires knowledge of the soil characteristics, natural susceptibility to erosion and the soil loss limit. In this context, the objectives of this study were to perform a detailed soil survey of Ribeirão das Perobas watershed, located in Santa Cruz do Rio Pardo, São Paulo State and to determine and map the erodibility and soil loss tolerance of the soil classes found in the survey. The following techniques were used to perform the detailed soil survey: photopedology, field sampling, physical analysis, chemical analysis, and morphological description of the soil samples and profiles. The erodibility was determined by the methods described by Denardin (1990) and Mannigel et al. (2002), and the determination of soil loss tolerance followed the methodology of Mannigel et al. (2002). The results of erodibility determined by the methodology of Denardin (1990) were not discrepant and they did not distinguish soils that are known to have different susceptibility to erosion., w\Whereas, using the methodology of Mannigel et al. (2002), very high or very low erodibility values were observed in soils with extreme contents of sand silt or clay. The most influent variable to the soil loss tolerance results was the correction factor for the textural gradient of clay between soil horizons.

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

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Pós-graduação em Fisiopatologia em Clínica Médica - FMB

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The detection limit (about 0.017 mu g mL(-1)) for voltammetric determination of iodide (peak at +0.87 V vs. Ag/AgCl at pH 2) at a glutaraldehyde-cross-linked poly-L-lysine modified glassy carbon electrode involving oxidation to iodine was found to be several orders of magnitude lower than that for the voltammetric determination on a bare glassy carbon electrode. This method was applied successfully to the determination of iodide in two medicinal formulations. Idoxuridine was determined indirectly at the same electrode by accumulating it first at -0.8 V vs. Ag/AgCl. At this potential the C-I bond in the adsorbed idoxuridine is reduced giving iodide, which is then determined at the modified electrode. The method was successfully applied to the determination of idoxuridine in a urine sample.