Strain hardening behavior of high performance FBDP, TRIP and TWIP steels

Based on n-value differential equation and microstructural observation, strain hardening behaviors of FBDP, TRIP, and TWIP steels during uniaxial tension were investigated. TRIP steel exhibits both superior strength and ductility than FBDP steel, and TWIP steel displays much higher total and uniform elongations in comparison to FBDP and TRIP steels. The instantaneous n values of FBDP and TRIP steels increase at small strains, reach a maximum value, smoothly decrease at higher strains, and then rapidly drop up to the specimen rupture. The strain hardening of TRIP steel persists at higher strains where that of FBDP steel begins to diminish. TWIP steel exhibits gradually increased instantaneous n values over the whole uniform plastic deformation, implying that TWIP steel shows a much larger strain hardening capability than FBDP and TRIP steels.

Transmission electron microscopy characterization of the bake-hardening behavior of transformation-induced plasticity and dual-phase steels

The effect of prestraining (PS) and bake hardening (BH) on the microstructures and mechanical properties has been studied in transformation-induced plasticity (TRIP) and dual-phase (DP) steels after intercritical annealing. The DP steel showed an increase in the yield strength and the appearance of the upper and lower yield points after a single BH treatment as compared with the as-received condition, whereas the mechanical properties of the TRIP steel remained unchanged. This difference appears to be because of the formation of plastic deformation zones with high dislocation density around the “as-quenched” martensite in the DP steel, which allowed carbon to pin these dislocations, which, in turn, increased the yield strength. It was found for both steels that the BH behavior depends on the dislocation rearrangement in ferrite with the formation of cell, microbands, and shear band structures after PS. The strain-induced transformation of retained austenite to martensite in the TRIP steel contributes to the formation of a complex dislocation structure.

Characterization of the bake-hardening behavior of transformation induced plasticity and dual-phase steels using advanced analytical techniques

The bake-hardening (BH) behavior of TRansformation Induced Plasticity (TRIP) and Dual-Phase (DP) steels after intercritical annealing (IA) has been studied using transmission electron microscopy, X-ray diffraction and three dimensional atom probe tomography. It was found for the DP steel that carbon can segregate to dislocations in the ferrite plastic deformation zones where there is a high dislocation density around the "asquenched" martensite. The carbon pinning of these dislocations, in turn, increases the yield strength after aging. It was shown that bake-hardening also leads to rearrangement of carbon in the martensite leading to the formation of rod-like low temperature carbides in the DP steel. Segregation of carbon to microtwins in retained austenite of the TRIP steel was also evident. These factors, in combination with the dislocation rearrangement in ferrite through the formation of cells and microbands in the TRIP steel after pre-straining, lead to the different bake-hardening responses of the two steels.

Effect of initial processing on the microstructure-property relationships in bake-hardened C-Mn-Si TRIP steels

The effect of pre-straining (PS) and bake-hardening (BH) on the microstructure and mechanical properties has been studied in C-Mn-Si TRansformation Induced Plasticity (TRIP) steels after: (i) thermomechanically processing (TMP) and (ii) intercritical annealing. The steels were characterised before and after PS/BH by transmission electron microscopy (TEM), X-ray diffraction (XRD), and tensile tests. The main microstructural differences were the higher volume fraction of bainite and more stable retained austenite in the TMP steel. This led to a difference in the strain-hardening behavior before and after BH treatment. The higher dislocation density in ferrite and formation of microbands in the TMP steel after PS and the formation of Fe3C carbides between the bainitic ferrite laths during BH for both steels also affected the strain-hardening behavior. However, both steels after PS/BH treatment demonstrated an increase in the yield and tensile strength.

A constitutive model of the deformation behaviour of twinning induced plasticity (TWIP) steel at different temperatures

The mechanical behaviour of Fe-18Mn-0.6C-1Al (wt%) TWIP steel was modelled in the temperature range from room temperature to 400°C. The proposed constitutive model was based on the Kocks-Mecking-Estrin (KME) model. The model parameters were determined using extensive experimental measurements of the physical parameters such as the dislocation mean free path and the volume fraction of twinned grains. More than 100 grains with a total area of ~300μm2 were examined at different strain levels over the entire stress-strain curve. Uniaxial tensile deformation of the TWIP steel was modelled for different deformation temperatures using a modelling approach which considers two distinct populations of grains: twinned and twin-free ones. A key point of the work was a meticulous experimental determination of the evolution of the volume fraction of twinned grains during uniaxial tensile deformation. This information was implemented in a phase-mixture model that yielded a very good agreement with the experimental tensile behaviour for the tested range of deformation temperatures. © 2014 Elsevier B.V.

Severe plastic deformation of TWIP steel

The severe plastic deformation of a Twinning Induced Plasticity (TWIP), 0.61C-22.3Mn-0.19Si-0.14Ni-0.27Cr (wt. %) steel by Equal Channel Angular Pressing (ECAP) at elevated temperatures was used to study the deformation mechanism as a function of accumulated strain and processing parameters. The relationship between the microstructures after different deformation schedules of ECAP at the temperatures of 200, 300 and 400oC, strain hardening behavior and mechanical properties was studied. The best balance between strength and ductility (1702 MPa and 24%) was found after 2 passes at 400oC and 300oC of ECAP. It was due to the formation of deformation microbands and twins in the microstructure. The twinning was observed after all deformation schedules except after 1 pass at 400oC. The important finding was the formation of twins in the ultrafine grains. Moreover, the stacking faults were observed in the subgrains with the size of 50nm. It is also worth mentioning the formation of nano- twins within the micro-twins at the same time. It was found that the deformation schedule affects the dislocation substructure with formation of deformation bands, cells, subgrains, two variants of twins that, in turn, influence the strain-hardening behavior and mechanical properties. Keywords: Twinning Induced Plasticity steels; Equal Channel Angular Pressing; mechanical properties; transmission electron microscopy; micro/nano twins; dislocation substructure.

Influence of low-strain deformation characteristics of high strength sheet steel on curl and springback in bend-under-tension tests

The influence of low-strain deformation behavior on curl and springback in advanced high strength steels (AHSS) was assessed using a bend-under-tension test. The effect of yielding behavior on curl and springback was examined by heat-treating two dual-phase steels to induce yield point elongation, while keeping a relatively constant tensile strength and a constant sheet thickness. A dual-phase and TRIP steel with similar initial thickness and tensile strengths were also examined to investigate the effect of work-hardening on curl and springback. It is shown that while current understanding limits prediction of curl and springback in bending under tension using only the initial sheet thickness and tensile strength, both the yielding and work-hardening behavior can affect the results. Explanations for these effects are proposed in terms of the discontinuous yielding and flow stress in the materials.

Uniform elongation and the stress-strain flow curve of steels calculated from hardness using empirical correlations

An empirical relationship between the hardness and uniform elongation of non-Austenitic hypoeutectoid steels has been developed. This new hardness-elongation relationship was combined with previously developed correlations of hardness and strength (yield and ultimate tensile strength) to predict the stressstrain flow curve from a single hardness test. The current study considers both power law hardening behavior and exponential hardening behavior. Reasonable agreement was observed between the experimental and predicted flow curves of a high strength, low alloy steel. Additionally, an empirical correlation of the flow strength at instability with hardness is provided. © ASM International.

On the Bauschinger effect in dual phase steel at high levels of strain

The effect of volume fraction and hardness of martensite on the Bauschinger effect in Dual Phase (DP) steel was investigated for strain levels close to those observed in automotive stamping. Five different grades of DP steel were produced by controlled heat treatment allowing the examination of the Bauschinger effect for three different volume fractions of martensite and three levels of martensite hardness. Compression-tension and shear reversal tests were performed to examine the Bauschinger effect at high levels of forming strain. Good correlation between the shear reversal and the compression-tension test was observed suggesting that for DP steel, shear stress strain data, converted to equivalent stress-strain, may be applied directly to characterize kinematic hardening behavior for numerical simulations. Permanent softening was observed following strain reversal and increased with martensite volume fraction and pre-strain level. While the Bauschinger ratio saturates at 3% pre-strain, the Bauschinger strain increases linearly with forming strain without showing saturation. This suggests that to model material behavior accurately in forming processes involving complex loading paths and high levels of strain, test data generated at high strain is required.

Effects of microstructure on the variation of the unloading behavior of DP780 steels

The nonlinear unloading behavior of three different commercial dual-phase steels (DP780 grade equivalent) was examined. These steels exhibited small variations in chemical composition (0.07 to 0.10 mass percent carbon) and martensite volume fraction (0.23 to 0.28), and they demonstrated similar hardening behavior. Uniaxial loading-unloading-loading tests were conducted at room temperature and quasi-static strain rates between engineering strains of 0.5 and 8%. Steel microstructures were examined using electron backscatter diffraction and nanoindentation techniques. The microplastic component of the unloading strain exhibited no dependence on the martensite volume fraction or the ferrite grain size within the small range encountered in this investigations. Instead, the magnitude of the microplastic component of the unloading strain increased as the strength ratio between the martensite and ferrite phases increased. Correspondingly, the apparent unloading modulus, or chord modulus, exhibited a greater reduction for equivalent increments of strain hardening as the strength ratio increased. These results suggest that springback can be reduced in structures containing two ductile phases if the strength ratio between the harder and softer phases is reduced.

Conversion of the hot torsion test results into flow curve with multiple regimes of hardening

The method of Fields and Backofen has been commonly used to reduce the data obtained by hot torsion test into flow curves. The method, however, is most suitable for materials with monotonic strain hardening behaviour. Other methods such as Stüwe’s method, tubular specimens, differential testing and the inverse method, each suffer from similar drawbacks. It is shown in the current work that for materials with multiple regimes of hardening any method based on an assumption of constant hardening indices introduces some errors into the flow curve obtained from the hot torsion test. Therefore such methods do not enable accurate prediction of onset of recrystallisation where slow softening occurs. A new method to convert results from the hot torsion test into flow curves by taking into account the variation of constitutive parameters during deformation is presented. The method represents the torque twist data by a parametric linear least square model in which Euler and hyperbolic coefficients are used as the parameters. A closed form relationship obtained from the mathematical representation of the data is employed next for flow stress determination. Two different solution strategies, the method of normal equations and singular value decomposition, were used for parametric modelling of the data with hyperbolic basis functions. The performance of both methods is compared. Experimental data obtained by FHTTM, a flexible hot torsion test machine developed at IROST, for a C–Mn austenitic steel was used to demonstrate the method. The results were compared with those obtained using constant strain and strain rate hardening characteristics.

Constitutive modeling of TWIP steel in uni-axial tension

High Mn steels demonstrate an exceptional combination of high strength and ductility due to their high work hardening rate during deformation. The microstructure evolution and work hardening behavior of Fe18Mn0.6C1.5Al TWIP steel in uni-axial tension were examined. The purpose of this study was to determine the contribution of all the relevant deformation mechanism : slip, twinning and dynamic strain aging. Constitutive modeling was carried out based on the Kubin-Estrin model, in which the densities of mobile and forest dislocations are coupled in order to account for the continuous immobilization of mobile dislocations during straining. These coupled dislocation densities were also used for simulating the contribution of dynamic strain aging on the flow stress. The model was modified to include the effect of twinning.