Method design and validation for the determination of uranium levels in human urine using high-resolution alpha spectrometry

Quantification of uranium in human urine is a valuable technique for assessing occupational and public exposure to uranium. A reliable method has been developed and validated in the ARPANSA Radiochemistry Laboratory by means of standard radiochemical separation and purification techniques and measurement using high-resolution alpha spectrometry. This method can be used to evaluate the levels of naturally occurring ²³⁴U, ²³⁵U and ²³⁸U in urine. Method design and validation is the process of defining an analytical requirement, and then confirming that the method under consideration has performance capabilities consistent with what the application requires. The method was designed to measure levels down to 2 mBq/day of total uranium, corresponding to approximately 1/100th of the annual committed effective dose of 20 mSv. Validation tests were developed to assess selectivity, accuracy, recovery and quantification of uncertainty. The radiochemical recovery of this method was measured using ²³²U tracer. The typical minimum detectable concentration for total uranium for 24-h urine samples is approximately 0.6 mBq/day or 0.019 μg/day.

Performance evaluation of 3D printed miniature electromagnetic energy harvesters driven by air flow

As a renewable and non-polluting energy source, wind is used to produce electricity via large-diameter horizontal or vertical axis wind turbines. Such large wind turbines have been well designed and widely applied in industry. However, little attention has been paid to the design and development of miniature wind energy harvesters, which have great potential to be applied to the HVAC (heating, ventilating and air conditions) ventilation exhaust systems and household personal properties. In this work, 10 air-driven electromagnetic energy harvesters are fabricated using 3D printing technology. Parametric measurements are then conducted to study the effects of (1) the blade number, (2) its geometric size, (3) aspect ratio, presence or absence of (4) solid central shaft, (5) end plates, and (6) blade orientation. The maximum electrical power is 0.305 W. To demonstrate its practical application, the electricity generated is used to power 4 LED (light-emitting diode) lights. The maximum overall efficiency ηmax is approximately 6.59%. The cut-in and minimum operating Reynolds numbers are measured. The present study reveals that the 3D printed miniature energy harvesters provide a more efficient platform for harnessing ‘wind power’.