The generation of new high angle boundaries during the hot torsional deformation of aluminium

The crystallographic rotation field for deformation in torsion is such that it is possible for orientations close to stable orientations to rotate away from the stable orientation. A Taylor type model was used to demonstrate that this phenomenon has the potential to transform randomly generated low-angle boundaries into high-angle boundaries. After imposing an equivalent strain of 1.2, up to 40% of the simulated boundaries displayed a disorientation in excess of 15°. These high-angle boundaries were characterised by a disorientation axis close to parallel with the sample radial direction. A series of hot torsion tests was carried out on 1050 aluminium to seek evidence for boundaries formed by this mechanism. A number of deformation-induced high-angle boundaries were identified. Many of these boundaries showed disorientation axes and rotation senses similar to those seen in the simulations. Between 10% and 25% of all the high-angle boundary present in samples twisted to equivalent strains between 2 and 7 could be attributed to the present mechanism.

Correlation between the deformation and post-deformation softening behaviours in hot worked Austenite

The relation between the deformation and post-deformation softening behaviours of austenite is examined in a 304 stainless steel. This correlation has been exploited in the modelling of hot rolling and it is argued here that the key to this understanding lies in the deformation structure. The latter is characterized in the present work by the fraction of dynamic recrystallization. The value of this fraction at the peak in the flow stress curve is found to decrease with increasing stress (i.e. with decreasing temperature and increasing strain rate). By contrast, the fraction of dynamic  recrystallization at the strain corresponding to the point where  post-deformation softening becomes strain independent is found to be constant. These observations are used to explain the nature of the important difference between the flow curve peak and the onset of strain independent post-deformation softening.

Plastic deformation in the annealed Zr41Ti14Cu12.5Ni10Be22.5 bulk metal glass under indenter

Vickers and nanoindentationswere carried out on an annealed Zr₄₁Ti₁₄Cu_12.5Ni₁₀Be_22.5 bulk metallic glass (BMG), and the evolution of the shear bands in the annealed BMG was investigated and compared to that in the as-cast alloy. Results indicate that the plastic deformation in the BMG with the structure relaxation is accommodated by the semicircular (primary) and radial (secondary) as well as tertiary shear bands. Quantitatively, the shear band density in the annealed alloywas much lower than that in the as-cast alloy. The load-displacement curve of nanoindentation test for the annealed alloy exhibited a more flat serrated flow. The annihilation of free volume caused by the annealing was responsible for the embrittlement of the annealed sample.

The generation of new high-angle boundaries in aluminium during hot torsion

The crystallographic rotation field for deformation in torsion is such that it is possible for orientations close to stable orientations to rotate away from the stable orientation. A Taylor type model was used to demonstrate that this phenomenon has the potential to transform randomly generated low-angle boundaries into high-angle boundaries. After imposing an equivalent strain of 1.2, up to 40% of the simulated boundaries displayed a disorientation in excess of 15°. These high-angle boundaries were characterised by a disorientation axis close to parallel with the sample radial direction. A series of hot torsion tests was carried out on 1050 aluminium to seek evidence for boundaries formed by this mechanism. A number of deformation-induced high-angle boundaries were identified. Many of these boundaries showed disorientation axes and rotation senses similar to those seen in the simulations. Between 10% and 25% of all the high-angle boundary present in samples twisted to equivalent strains between 2 and 7 could be attributed to the present mechanism.

Development of ultrafine grained steels through thermomechanical processing

The formation of ultrafine ferrite by strain induced transformation is assessed using rolling and hot torsion experiments. These experiments are used to examine the impact of thermomechanical processing conditions and steel chemistry on strain induced austenite to ferrite transformation and the formation of ultrafine ferrite. The critical strain for dynamic strain induced transformation increased with increasing carbon equivalence, deformation temperature and austenite grain size. The deformation structure in the austenite grains changes with the thermomechanical processing conditions. Drawing on these results and the current literature, the important factors for the production of ultrafine ferrite are described and a mechanism is proposed.

Formation of ultrafine ferrite by dynamic strain-induced transformation

In the current study, the role of dynamic strain induced transformation on ferrite grain refinement was investigated using different thermomechanical processing routes. A Ni-30Fe austenitic model alloy was also employed to study the evolution of the deformation structure under different deformation conditions. It was shown that the extreme refinement of ferrite is more likely due to the formation of extensive high angle intragranular defects in the austenite through deformation. Among the different thermomechanical parameters, the deformation temperature had a significant effect on the intragranular defect characteristics. There was a transition where the cell dislocation structure changed to laminar microband structures with a decrease in the deformation temperature. Moreover, the ultrafine grained structure was also successfully produced through static transformation using warm deformation process; in other words, concurrent deformation and transformation are not necessary for ultrafine ferrite formation.

Microstructural analysis of pre-strained TRIP steel after fatigue testing

The widespread introduction of multiphase sheet steels in the automotive industry has led to considerable interest in the fatigue properties of these materials. The different microstructural phases within matelials such as TRIP steels can influence the fatigue behaviour due to the manner in which the cyclic strain is accommodated within these phases. In this study fully reversed straincontrolled fatigue tests were perfonnrmed on a commercially-produced uncoated TRIP 780 steel both in the as-received and 20 % prestrained condition. The pre-strained TRIP steel showed significant cyclic softening at higher strain amplitudes, whereas some initial work hardening was observed at lower strain amplitudes before cyclic softening. The cyclic stabilised strength of the pre-strained TRIP steel was independent of strain amplitude, while the cyclic stabilised strength of the as-received TRIP steel increased with strain amplitude. Transmission Electron Microscopy TEM was used to examine the effect of the cyclic deformation on the microstructure of the different conditions, with the differences in fatigue behaviour explained based on the differences in the deformation structure formed within the steel (i.e. dislocation density and sub-structure and microband formation).

Effect of structure relaxation on the plastic deformation behaviour in a Zr-based BMG under indenter

Vickers and nano indentations were performed on a structurally relaxed Zr₄₁Ti₁₄Cu_12.5Ni₁₀Be_22.5 bulk metallic glass (BMG), and the evolution of the shear bands in the relaxed BMG was investigated and compared to that in the as-cast alloy. Results indicate that the plastic deformation in the BMG with structure relaxation is accommodated by the semicircular (primary) and radial (secondary) as well as tertiary shear bands. Quantitatively, the shear band density in the relaxed alloy was much lower than that in the as-cast alloy. The annihilation of free volume caused by the annealing was responsible for the embrittlement of the sample with structure relaxation.

Fine structure of shear bands formed during hot deformation of two austenitic steels

Shear bands formed during both cold and hot plastic deformation have been linked with several proposed mechanisms for the formation of ultrafine grains. The aim of the present work was to undertake a detailed investigation of the microstructural and crystallographic characteristics of the shear bands formed during hot deformation of a 22Cr-19Ni-3Mo (mass%) austenitic stainless steel and a Fe-30 mass%Ni based austenitic model alloy. These alloys were subjected to deformation in torsion and plane strain compression (PSC), respectively, at temperatures of 900°C and 950°C and strain rates of 0.7s_-1 and 10s_-1, respectively. Transmission electron microscopy and electron backscatter diffraction in conjunction with scanning electron microscopy were employed in the investigation. It has been observed that shear bands already started to form at moderate strains in a matrix of pre-existing microbands and were composed of fine, slightly elongated subgrains (fragments). These bands propagated along a similar macroscopic path and the subgrains, present within their substructure, were rotated relative to the surrounding matrix about axes approximately parallel to the sample radial and transverse directions for deformation in torsion and PSC, respectively. The subgrain boundaries were largely observed to be non-crystallographic, suggesting that the subgrains generally formed via multiple slip processes. Shear bands appeared to form through a co-operative nucleation of originally isolated subgrains that gradually interconnected with the others to form long, thin bands that subsequently thickened via the formation of new subgrains. The observed small dimensions of the subgrains present within shear bands and their large misorientations clearly indicate that these subgrains can serve as potent nucleation sites for the formation of ultrafine grain structures during both subsequent recrystallisation, as observed during the present PSC experiments, and phase transformation.

Influence of deformation conditions and texture on the high temperature flow stress of magnesium AZ31

The evolution of hot working flow stress with strain is examined in torsion, uniaxial compression and channel die compression. The flow stress was found to be strongly dependent on texture and deformation mode. At low strains this dependency accounted for a difference in flow stress of up to a factor of two. At higher strains the influence of texture and deformation mode was less marked. The stresses corresponding to an equivalent strain of 0.5 were modelled using a power law expression with an activation energy of 147 kJ/mol and a strain rate exponent of 0.15. The influence of texture and deformation mode on flow stress is rationalised in terms of the influence of prismatic slip, twinning and dynamic recrystallisation on deformation stress and structure.

Microstructural evolution of ultrafine grained structure in plain carbon steels through single pass rolling

In the present study, the effect of nominal equivalent strain (between 0 and 1.2), deformation temperature (790– 750°C) and carbon content (0.06 – 0.35%C) was investigated on ferrite grain refinement through dynamic strain induced transformation (DSIT) in plain carbon steels in single pass rolling. The microstructural evolution of the transformation of austenite to ferrite has been evaluated through the thickness of the strip. The results showed a number of important microstructural features as a function of strain, which could be classified into three regions; no DSIT region, DSIT region, and ultrafine ferrite (UFF) grain region. Hence, two critical strains; dynamic strain induced transformation (εC, DSIT) and ultrafine ferrite formation (εC, UFF) were determined. These strains were increased significantly with an increase in carbon content. The critical strain for UFF formation reduced with decrease in deformation temperature. The UFF microstructure consisted of ultrafine, equiaxed ferrite grains (<2 μm) with very fine cementite particles. In the centre of the rolled strip, there was a conventional ferrite– pearlite microstructure, although ferrite grain refinement and the volume fraction of ferrite increased with increase in the nominal equivalent strain.

Mapping the hot deformation microstructure of Ni-30Fe alloy

The evolution of structure during the hot working of an austenitic Ni-30%Fe alloy is studied using EBSD analysis of samples tested in torsion. A microstructural map in temperature-strain space that plots grain size, cell size, fracture and dynamic recrystallization is presented.