Variant selection during the c-to-ab phase transformation in hot-rolled bainitic TRIP-aided steels

The variant selection phenomenon during the austenite to bainite phase transformation in hot-rolled TRIP-aided steels was quantitatively characterized at the level of individual austenite grains. The reconstruction of the electron backscatter diffraction maps provided evidence that bainite grows by packets of laths sharing a common {1 1 1}_y plane in the austenite. The affect of hot deformation is to reduce the number of packets that form. It is suggested that slip activity is important in understanding this effect.

Habitat suitability for marine fishes using presence-only modelling and multibeam sonar

Improved access to multibeam sonar and underwater video technology is enabling scientists to use spatially-explicit, predictive modelling to improve our understanding of marine ecosystems. With the growing number of modelling approaches available, knowledge of the relative performance of different models in the marine environment is required. Habitat suitability of 5 demersal fish taxa in Discovery Bay, south-east Australia, were modelled using 10 presence-only algorithms: BIOCLIM, DOMAIN, ENFA (distance geometric mean [GM], distance harmonic mean [HM], median [M], area-adjusted median [Ma], median + extremum [Me], area-adjusted median + extremum [Mae] and minimum distance [Min]), and MAXENT. Model performance was assessed using kappa and area under curve (AUC) of the receiver operator characteristic. The influence of spatial range (area of occupancy) and environmental niches (marginality and tolerance) on modelling performance were also tested. MAXENT generally performed best, followed by ENFA-GM and -HM, DOMAIN, BIOCLIM, ENFA-M, -Min, -Ma, -Mae and -Me algorithms. Fish with clearly definable niches (i.e. high marginality) were most accurately modelled. Generally, Euclidean distance to nearest reef, HSI-b (backscatter), rugosity and maximum curvature were the most important variables in determining suitable habitat for the 5 demersal fish taxa investigated. This comparative study encourages ongoing use of presence-only approaches, particularly MAXENT, in modelling suitable habitat for demersal marine fishes.

Comparison of automated classification techniques for predicting benthic biological communities using hydroacoustics and video observations

The effective management of our marine ecosystems requires the capability to identify, characterise and predict the distribution of benthic biological communities within the overall seascape architecture. The rapid expansion of seabed mapping studies has seen an increase in the application of automated classification techniques to efficiently map benthic habitats, and the need of techniques to assess confidence of model outputs. We use towed video observations and 11 seafloor complexity variables derived from multibeam echosounder (MBES) bathymetry and backscatter to predict the distribution of 8 dominant benthic biological communities in a 54 km² site, off the central coast of Victoria, Australia. The same training and evaluation datasets were used to compare the accuracies of a Maximum Likelihood Classifier (MLC) and two new generation decision tree methods, QUEST (Quick Unbiased Efficient Statistical Tree) and CRUISE (Classification Rule with Unbiased Interaction Selection and Estimation), for predicting dominant biological communities. The QUEST classifier produced significantly better results than CRUISE and MLC model runs, with an overall accuracy of 80% (Kappa 0.75). We found that the level of accuracy with the size of training set varies for different algorithms. The QUEST results generally increased in a linear fashion, CRUISE performed well with smaller training data sets, and MLC performed least favourably overall, generating anomalous results with changes to training size. We also demonstrate how predicted habitat maps can provide insights into habitat spatial complexity on the continental shelf. Significant variation between patch-size and habitat types and significant correlations between patch size and depth were also observed.

Development of asymmetric rolling for the better control over structure and mechanical properties in IF steel

In the present study, the effects of kinematic and geometric asymmetries in rolling during multi-pass processing of IF steel are examined. The theoretical investigation by final element simulations and experimental investigations by means of electron-backscatter diffraction analysis and tensile tests suggest that asymmetric rolling increases the total imposed strain compared to symmetric rolling, and largely re-distributes the strain components due to additional shear. This enhances the intensity of grain refinement, strengthens and tilts crystallographic orientations, and increases mechanical strength. The effect is highest in the asymmetric rolling with differential roll diameters.

Improved bonding and conductivity of polypyrrole on polyester by gaseous plasma treatment

A systematic study was conducted using argon, oxygen, and nitrogen plasma to improve the adhesion of polypyrrole coating to polyester (PET) fabric for improving conductivity and to understand the mechanisms involved. PET thin film was used as a reference sample. The changes in wettability, surface chemistry and morphology were studied by water contact angle, X-ray photoelectron spectroscopy, and atomic force and scanning electron microscopy. It was found that both the highest conductivity and the strongest interfacial bonding were achieved by oxygen plasma treatment. The increase in hydrophilicity, surface functionalization, and suitable nano-scale roughness gave improved adhesion.

Characterization and tribological performance of Cu-based intermetallic layers

Fluidized bed reactor chemical vapor deposition (FBR-CVD) has been used to enrich the surface of oxygen free high conductivity (OFHC) copper with titanium, silicon and aluminum. This technique enables the production of coherent and adherent intermetallic surface layers of uniform thickness and high hardness. The characterization of the coatings was performed using backscatter scanning electron microscopy (BS-SEM), X-ray diffraction (XRD), glow discharge optical emission spectroscopy (GDOES) and micro-hardness. The tribological properties of the coatings in dry sliding contact with steel were evaluated by pin-on-disc wear testing.

Asymmetric rolling of interstitial-free steel using differential roll diameters. Part I : mechanical properties and deformation textures

IF steel sheets were processed by conventional symmetric and asymmetric rolling (ASR) at ambient temperature. The asymmetry was introduced in a geometric way using differential roll diameters with a number of different ratios. The material strength was measured by tensile testing and the microstructure was analyzed by optical and transmission electron microscopy as well as electron backscatter diffraction (EBSD) analysis. Texture was also successfully measured by EBSD using large surface areas. Finite element (FE) simulations were carried out for multiple passes to obtain the strain distribution after rolling. From the FE results, the velocity gradient along selected flow lines was extracted and the evolution of the texture was simulated using polycrystal plasticity modeling. The best mechanical properties were obtained after ASR using a roll diameter ratio of 2. The textures appeared to be tilted up to 12 deg around the transverse direction, which were simulated with the FE-combined polycrystal plasticity modeling in good agreement with measurements. The simulation work revealed that the shear component introduced by ASR was about the same magnitude as the normal component of the rolling strain tensor.

Quantitative experimental comparison of single-beam, sidescan, and multibeam benthic habitat maps

Map comparison is a relatively uncommon practice in acoustic seabed classification to date, contrary to the field of land remote sensing, where it has been developed extensively over recent decades. The aim here is to illustrate the benefits of map comparison in the underwater realm with a case study of three maps independently describing the seabed habitats of the Te Matuku Marine Reserve (Hauraki Gulf, New Zealand). The maps are obtained from a QTC View classification of a single-beam echosounder (SBES) dataset, manual segmentation of a sidescan sonar (SSS) mosaic, and automatic classification of a backscatter dataset from a multibeam echosounder (MBES). The maps are compared using pixel-to-pixel similarity measures derived from the literature in land remote sensing. All measures agree in presenting the MBES and SSS maps as the most similar, and the SBES and SSS maps as the least similar. The results are discussed with reference to the potential of MBES backscatter as an alternative to SSS mosaic for imagery segmentation and to the potential of joint SBES–SSS survey for improved habitat mapping. Other applications of map-similarity measures in acoustic classification of the seabed are suggested.

Comparison of a self-processed EM3000 multibeam echosounder dataset with a QTC view habitat mapping and a sidescan sonar imagery, Tamaki Strait, New Zealand

A methodology for automatically processing the data files from an EM3000 multibeam echosounder (Kongsberg Maritime, 300 kHz) is presented. Written in MatLab, it includes data extraction, bathymetry processing, computation of seafloor local slope, and a simple correction of the backscatter along-track banding effect. The success of the latter is dependent on operational restrictions, which are also detailed. This processing is applied to a dataset acquired in 2007 in the Tamaki Strait, New Zealand. The resulting maps are compared with a habitat classification obtained with the acoustic ground-discrimination software QTC View linked to a 200-kHz single-beam echosounder and to the imagery from a 100-kHz sidescan sonar survey, both performed in 2002. The multibeam backscatter map was found to be very similar to the sidescan imagery, quite correlated to the QTC View map on one site but mainly uncorrelated on another site. Hypotheses to explain these results are formulated and discussed. The maps and the comparison to prior surveys are used to draw conclusions on the quality of the code for further research on multibeam benthic habitat mapping.

Phase and crystal orientation study of a TRansformation Induced Plasticity steel subjected to cyclic load induced fatigue

An electron backscatter diffraction (EBSD) study of the microstructure of TRIP steel during fatigue failure. Phase and crystal orientation study of a TRIP steel subjected to cyclic load induced fatigue. The relative fractions of austenite, ferrite and martensite are quantified within the strain field of a fatigue crack tip. This data is a subset of data supporting a wider study of the fatigue properties of multiphase steels used in the automotive industry. The different microstructural phases present in these steels can influence the strain life and cyclic stabilized strength of the material due to the way in which these phases accommodate the applied cyclic strain. Fully reversed strain-controlled low-cycle fatigue tests have been used to determine the mechanical fatigue performance of a dual-phase (DP) 590 and transformation induced plasticity (TRIP) 780 steel, with transmission electron microscopy (TEM) and scanning electron microscopy (SEM-EBSD) used to examine the deformed microstructures .

Texture selection mechanisms in uniaxially extruded magnesium alloys

Extrusion textures in magnesium alloys are of high interest due to their influence on yield asymmetry. This data supports work describing three mechanisms of texture selection that may play a role during extrusion. These mechanisms involve localized differences in deformation at the grain level, the change in local environment experienced by grain boundary bulges and shear banding. The work employs visco-plastic crystal plasticity and electron backscattering diffraction.

Influence of orientation on twin nucleation and growth at low strains in a magnesium alloy

The resolved shear stress is believed to play an important role in twin formation. The present study tests this idea for an extruded magnesium alloy by examining "tension" twinning in different grain orientations. Electron backscatter diffraction analysis is employed for alloy AZ31 tested in compression along the extrusion axis to strains between 0.008 and 0.015. For heavily twinned grains, it is seen that twinning occurs on 2.3 twin systems per grain on average. The active systems are also most commonly those with, or very near to, the highest Schmid factor. The most active system in multiply twinned grains accounts on average for ∼0.6 of the twinning events. In addition, it is found that the twin habit plane falls within 6° of the K1 plane. Orientations with the highest Schmid factors (0.45-0.5) for twinning display twin aspect ratios greater by ∼40% and twin number densities greater by ∼10 times than orientations with maximum Schmid factors for twinning of 0.15-0.2. Thus the Schmid factor for twinning is seen to affect nucleation more than thickening in the present material. Viscoplastic crystal plasticity simulations are employed to obtain approximations for the resolved shear stress. Both the twin aspect ratio and number density correlate quite well with this term. The effect of the former can be assumed to be linear and that of the latter follows a power law with exponent ∼13. Increased aspect ratios and number densities are seen at low Schmid factors and this may relate to stress fluctuations, caused most probably in the present material by the stress fields at the tips of blocked twins. Overall, it is evident that the dominance of twinning on high Schmid factor systems is preserved at the low strains examined in the present work, despite the stress fluctuations known to be present. © 2014 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Contribution of twinning to low strain deformation in a Mg alloy

Deformation twinning plays an important role in the yielding of extruded magnesium alloys, especially when loaded in compression along the extrusion axis. The magnitude of this contribution is not accurately known. The present study employs electron backscatter diffraction to reveal the influence of grain orientation on twin-volume fraction for alloy AZ31 tested in compression to strains between 0.008 and 0.015. For these strains, it is seen that approximately 45 pct of the deformation can be attributed to "tensile" twinning. The variation of twin-volume fraction over different orientation classes correlates closely with the maximum Schmid factors for both tensile twinning and basal slip. These effects are readily explained quantitatively using a mean field crystal plasticity model without recourse to stochastic effects. Encouraged by this, we introduce an analytical approximation based on the uniformity of (axial) work. © 2013 The Minerals, Metals & Materials Society and ASM International.