32 resultados para Mercury intrusion porosimetry


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Understanding the amalgamation mechanisms between mercury and gold is of fundamental interest and importance to many mercury sensing applications. However, there is only limited and piecemeal discussion in the literature of the mechanisms by which Au-Hg amalgams are formed on thin Au films. Here, we present a comprehensive description of a series of morphological changes occurring in a thin polycrystalline Au film during Au-Hg amalgamation investigated by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), and atomic force microscopy (AFM). These microscopic investigations enable us to offer a coherent explanation for the features and the mechanisms of amalgamation of Hg with Au in the film. We also use an optical technique (fringes of equal chromatic order, FECO) to observe changes in optical thickness and reflectivity of the film. Amalgamation reactions in the film render it inhomogeneous, thus making optical techniques unsuitable as a method for quantitative monitoring of Hg vapor using Au films of this type.

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Anomaly detection as a kind of intrusion detection is good at detecting the unknown attacks or new attacks, and it has attracted much attention during recent years. In this paper, a new hierarchy anomaly intrusion detection model that combines the fuzzy c-means (FCM) based on genetic algorithm and SVM is proposed. During the process of detecting intrusion, the membership function and the fuzzy interval are applied to it, and the process is extended to soft classification from the previous hard classification. Then a fuzzy error correction sub interval is introduced, so when the detection result of a data instance belongs to this range, the data will be re-detected in order to improve the effectiveness of intrusion detection. Experimental results show that the proposed model can effectively detect the vast majority of network attack types, which provides a feasible solution for solving the problems of false alarm rate and detection rate in anomaly intrusion detection model.