Permeability mapping in porous media by magnetization prepared centric-scan SPRITE

The ability of porous media to transmit fluids is commonly referred to as permeability. The concept of permeability is central for hydrocarbon recovery from petroleum reservoirs and for studies of groundwater flow in aquifers. Spatially resolved measurements of permeability are of great significance for fluid dynamics studies. A convenient concept of local Darcy’s law is suggested for parallel flow systems. The product of porosity and mean velocity images in the plane across the average flow direction is directly proportional to permeability. Single Point Ramped Imaging with T 1 Enhancement (SPRITE) permits reliable quantification of local fluid content and flow in porous media. It is particularly advantageous for reservoir rocks characterized by fast magnetic relaxation of a saturating fluid. Velocity encoding using the Cotts pulsed field gradient scheme improves the accuracy of measured flow parameters. The method is illustrated through measurements of 2D permeability maps in a capillary bundle, glass bead packs and composite sandstone samples.

Who are the older Australians referred for a bone density scan? Data from the Barwon region

We investigated the reasons for referral of older Australians aged 70 years and older to dual energy X-ray absorptiometry (DXA). The most common clinical indication was being aged 70 years and older, followed by monitoring for fracture or low bone mineral density (BMD). Compared to males, females were twice as likely to have osteoporotic BMD.

Golden opportunities: a horizon scan to expand sandy beach ecology

Robust ecological paradigms and theories should, ideally, hold across several ecosystems. Yet, limited testing of generalities has occurred in some habitats despite these habitats offering unique features to make them good model systems for experiments. We contend this is the case for the ocean-exposed sandy beaches. Beaches have several distinctive traits, including extreme malleability of habitats, strong environmental control of biota, intense cross-boundary exchanges, and food webs highly reliant on imported subsidies. Here we sketch broad topical themes and theoretical concepts of general ecology that are particularly well-suited for ecological studies on sandy shores. These span a broad range: the historical legacies and species traits that determine community assemblages; food-web architectures; novel ecosystems; landscape and spatial ecology and animal movements; invasive species dynamics; ecology of disturbances; ecological thresholds and ecosystem resilience; and habitat restoration and recovery. Collectively, these concepts have the potential to shape the outlook for beach ecology and they should also encourage marine ecologists to embrace, via cross-disciplinary ecological research, exposed sandy beach systems that link the oceans with the land.

Built-up edge mechanisms in the machining of duplex stainless steels

 The thesis work was aimed at resolving long established issues with difficult-to-machine materials. The main thesis contribution, is the academic community now has a better understanding of how the issue of built-up edge is occurring when machining duplex stainless steel alloys, which will aid in the machining sector.

Weldability of duplex stainless steel

Duplex stainless steels (DSSs) have many advantages due to the unique structural combination of ferrite and austenite grains. The structural change of these materials is very complex during welding, and it deteriorates the functional properties. This research investigates different welding processes such as laser beam, resistance, tungsten inert gas, friction stir, submerged arc, and plasma arc weldings considering the research available in the literature. The welding mechanism, change of material structure, and control parameters have been analyzed for every welding process. This analysis clearly shows that DSS melts in all most all welding processes, but the thermal cycle and maximum heat input are different. This difference affects the resulting structure and functional properties of the weld significantly.

Chip formation mechanism and machinability of wrought duplex stainless steel alloys

This paper investigates the chip formation mechanism and machinability of two-phase materials, such as, wrought duplex stainless steel alloys SAF 2205 and SAF 2507. SEM and optical microscopic details of the frozen cutting zone and chips revealed that the harder austenite phase dissipates in the advancement of the cutting tool, being effectively squeezed out of the softer ferrite phase. Microhardness profiles reveal correlation in hardness from the workpiece material transitioning to the chip. The tool wear (TiAIN + TiN coated solid carbide twist drill) and machining forces were investigated. Tool wear, was dominantly due to the adhesion process which developed from built-up edge formation, is highly detrimental to the flank face. Flute damage was also observed as a major issue in the drilling of duplex alloys leading to premature tool failure. Duplex 2507 shows higher sensitivity to cutting speed during machining and strain hardening at higher velocity and less machinability due to presence of higher percentage of Ni, Mo and Cr.

Weldability and machinability of duplex stainless steel

This chapter investigates two important processing methods, such as welding and machine of duplex stainless steel. The welding process welding generally degrades the properties of these materials by redistributing the phases during melting and solidification. On the other hand, the redistribution during machining mainly take place combined effect of stress, strain rate and temperature. Mechanism of machining process and several welding methods has been analysed in details. It was found that outcomes of welding processes depend on the welding methods. Most of the cases an appropriate annealing process can be used to restore the expected properties of the weld joints though the parameters of annealing process are different in different welding methods. Nonmetallic inclusions and the low carbon content of duplex stainless steel reduce the machinability of duplex stainless steel. SEM and optical microscopic details of the frozen cutting zone and chips revealed that the harder austenite phase dissipates in the advancement of the cutting tool, being effectively squeezed out of the softer ferrite phase. Abrasion and adhesion were the most common wear modes developed on the flank and rake faces. Adhesion wear being the most prevalent on the flank face, appeared to be initiated by built-up edge formation.

Investigation on the behavior of austenite and ferrite phases at stagnation region in the turning of duplex stainless steel alloys

This paper investigates the deformation mechanisms and plastic behavior of austenite and ferrite phases in duplex stainless steel alloys 2205 and 2507 under chip formation from a machine turning operation. SEM images and EBSD phase mapping of frozen chip root samples detected a build-up of ferrite bands in the stagnation region, and between 65 and 85 pct, more ferrite was identified in the stagnation region compared to austenite. SEM images detected micro-cracks developing in the ferrite phase, indicating ferritic build-up in the stagnation region as a potential triggering mechanism to the formation of built-up edge, as transgranular micro-cracks found in the stagnation region are similar to micro-cracks initiating built-up edge formation. Higher plasticity of austenite due to softening under high strain is seen responsible for the ferrite build-up. Flow lines indicate that austenite is plastically deforming at a greater rate into the chip, while ferrite shows to partition most of the strain during deformation. The loss of annealing twins and activation of multiple slip planes triggered at high strain may explain the highly plastic behavior shown by austenite.

The microstructure evolution and softening processes during high-temperature deformation of a 21Cr-10Ni-3Mo duplex stainless steel

The austenite and ferrite microstructure evolution and softening mechanisms have been investigated in a 21Cr-10Ni-3Mo duplex stainless steel, containing about 60% austenite, deformed in torsion at 1200°C using a strain rate of 0.7 s-1. The above experimental conditions led to the formation of a small volume fraction of new austenite grains through discontinuous dynamic recrystallization (DDRX), which could not account for the observed large softening on the flow curve. DDRX grains mainly formed through the strain-induced migration of the pre-existing austenite grain boundaries, known to dominate in single-phase austenite, complemented by subgrain growth in the interface regions with ferrite. A significant portion of austenite dynamic softening has been attributed to the large-scale subgrain coalescence, the extent of which increased with strain, which seems to have contributed substantially to the observed flow stress decrease. The above process thus appears to represent an alternative mode of austenite dynamic softening to the classical DDRX in the duplex austenite/ferrite microstructure, characterised by limited availability of the pre-existing austenite/austenite high-angle boundaries, deformed at a high temperature. The softening mechanism within ferrite has been classified as "continuous DRX", characterised by a gradual increase in misorientations between neighbouring subgrains with strain and resulting in the progressive conversion of subgrains into "crystallites" bounded partly by low-angle and partly by large-angle boundaries.

Premature thermal fatigue failure of aluminium injection dies with duplex surface treatment

The premature failure of an aluminium injection die with a duplex surface treatment (plasma nitriding and physical vapor deposition coating) was investigated, in an effort to identify the causes of such premature failure of the component. The manufacturing and the operating conditions were documented. Analytical tools were used, including scanning electron microscopy with energy dispersive X-ray capability, X-ray diffraction, and instrumented microhardness testing. Preliminary observations showed a microstructure of coarse tempered martensite, and a considerably rough surface with porosity and cracks. A detailed analysis of crack initiation sites identified sulfur inclusions in the subsurface, underneath the coating. A further revision of the processing conditions revealed that a sulfur-impregnated grinding stone had been used to polish the die. The chemical composition of such grinding stone matched that of the inclusions found in the subsurface of the failed component. Thus, searched causes of premature failure could be discussed on the lights of the present findings.