Plastic deformation in Zr41 Ti14 Cu12.5 Ni10 Be22.5 bulk metal glass under vickers indenter

Vickers indentation was conducted on an as-cast Zr41Ti14Cu12.5Ni10Be22.5 bulk metal glass (BMG) to study shear band formation using a bonded interface technique. The results indicate that the plastic deformation in the BMG is accommodated by the semi-circular (primary) and radial (secondary) shear bands. The inter-band spacing of the semi-circular shear bands is found to be independent of the applied load. The measured size of the deformation zone is in good agreement with the prediction of the theoretical model proposed by Zhang et al.

Enhanced tensile ductility of an ultra-fine-grained aluminium alloy

Aluminum alloy 6082 was subjected to equal-channel angular pressing (ECAP), which resulted in an ultra-fine-grained (UFG) microstructure with an average grain size of 0.2–0.4 μm. There was a pronounced effect of the grain refinement on the strain-rate sensitivity and tensile ductility. The Hart criterion of tensile necking fails to explain the observed ductility of the UFG material at low strain rates. A correlation between the observed stronger-than-expected ductility and a tendency to microshear band formation at low strain rates was established.

Application of the strain localization CAFE model to investigate extrusion with various die shapes

Multi scale CAFE model for the prediction of initiation and propagation of the micro shear bands and shear bands in metallic materials subjected to plastic deformation is presented. The CAFE approach is the combination of the Cellular Automata (CA) and the Finite Element (FE) methods. The application of the developed CAFE model to analyze material flow during extrusion is the objective of the present work. The proposed CAFE approach is applied in this work to simulation of the extrusion with flat face and convex dies and to investigate differences in the material flow. The initial FE meshes with the set of the CA point are generated for the numerical tests and the results of the metal flow predicted by the CAFE method are presented in the paper.

Some issues relating to the ductility of wrought magnesium alloys

The present work is concerned with gaining a better understanding of the factors that control the ductility of wrought magnesium alloys. The ultimate aim is to develop alloys with vastly improved room temperature formability. It is shown that 3D tomography of fractured tensile specimens reveals disk shaped voids aligned more or less at 45 deg. to the tensile axis. These voids are consistent with twin induced void formation. It is also shown that the double twins that produce such voids form in contradiction to Schmid predictions. Finally, it is demonstrated that low levels of rare-earth additions leads to vastly improved texture and ductility in extrusions, as they do in rolled sheet.

Electron back scattered diffraction (EBSD) characterization of warm rolled and accumulative roll bonding (ARB) processed ferrite

An interstitial free (IF) steel was severely deformed using accumulative roll bonding (ARB) process and warm rolling. The maximum equivalent strains for ARB and warm rolling were 4.8 and 4.0, respectively. The microstructure and micro-texture were studied using optical microscopy and scanning electron microscopy equipped with electron back scattered diffraction (EBSD). The grain size and misorientation obtained by both methods are in the same range. The microstructure in the ARB samples after 6 cycles is homogeneous, although a grain size gradient is observed at the layers close to the surface. The through thickness texture gradient in the ARB samples is different from the warm rolled samples. While a shear texture (⟨110⟩//rolling plane normal direction (ND)) at the surface and rolling texture at the center region is developed in the ARB  samples, the overall texture is weak. The warm rolled samples display a sharp rolling texture through the thickness with increasing the sharpness toward the center. These differences are attributed to the fact that the central region of ARB strip is comprised of material that was once at the surface. The ARB process  can suppress the formation of shear bands which are conventional at warm rolled IF steels. EBSD study on the sample with 6th cycle of ARB following the annealing at 750 ◦C verified a texture gradient through the thickness of the sheet. The shear orientations at the surface and at the quarter thickness layers can be identified even after annealing. The overall weak texture and existence of shear orientations make ARB processed samples unfavorable for sheet metal forming in compare with warm rolled samples.

Effect of structure relaxation on the plastic deformation behaviour in a Zr-based BMG under indenter

Vickers and nano indentations were performed on a structurally relaxed Zr₄₁Ti₁₄Cu_12.5Ni₁₀Be_22.5 bulk metallic glass (BMG), and the evolution of the shear bands in the relaxed BMG was investigated and compared to that in the as-cast alloy. Results indicate that the plastic deformation in the BMG with structure relaxation is accommodated by the semicircular (primary) and radial (secondary) as well as tertiary shear bands. Quantitatively, the shear band density in the relaxed alloy was much lower than that in the as-cast alloy. The annihilation of free volume caused by the annealing was responsible for the embrittlement of the sample with structure relaxation.

Plastic deformation in the annealed Zr41Ti14Cu12.5Ni10Be22.5 bulk metal glass under indenter

Vickers and nanoindentationswere carried out on an annealed Zr₄₁Ti₁₄Cu_12.5Ni₁₀Be_22.5 bulk metallic glass (BMG), and the evolution of the shear bands in the annealed BMG was investigated and compared to that in the as-cast alloy. Results indicate that the plastic deformation in the BMG with the structure relaxation is accommodated by the semicircular (primary) and radial (secondary) as well as tertiary shear bands. Quantitatively, the shear band density in the annealed alloywas much lower than that in the as-cast alloy. The load-displacement curve of nanoindentation test for the annealed alloy exhibited a more flat serrated flow. The annihilation of free volume caused by the annealing was responsible for the embrittlement of the annealed sample.

Plastic deformation in a partially crystallized Zr-based BMG under Vickers indenter

Vickers indentations were carried out on an anneal-introduced partially crystallized Zr₄₁Ti₁₄Cu_12.5 Ni₁₀Be_22.5 bulk metallic glass (BMG), and the evolution of the shear bands in this samplewas investigated and compared to the as-cast, aswell as the structurally relaxed counterparts. The results indicate that the plastic deformation in the partially crystallized BMG was accommodated by the semi-circular (primary) and radial (secondary) shear bands. A full crack or flake that was produced due to the spring back during the load removal was observed. The shear band density in the annealed alloy which was dispersed with crystalliteswas significantly lower than that of the as-cast alloy. The difference of the shear band features among the three kinds of alloy status, i.e., partially crystallized, structurally relaxed and as-cast alloys was discussed in terms of the free volume in the BMGs and the characteristics of nano-composites. It has been demonstrated that the plasticity for the three statuses of alloys queues in the descending order as the as-cast, annealed with partial crystallization, and annealed without crystallization.

Development of the multi-scale analysis model to simulate strain localization occurring during material processing

Abstract A detailed description of possibilities given by the developed Cellular Automata—Finite Element (CAFE) multi scale model for prediction of the initiation and propagation of micro shear bands and shear bands in metallic materials subjected to plastic deformation is presented in the work. Particular emphasis in defining the criterion for initiation of micro shear and shear bands, as well as in defining the transition rules for the cellular automata, is put on accounting for the physical aspects of these phenomena occurring in two different scales in the material. The proposed approach led to the creation of the real multi scale model of strain localization phenomena. This model predicts material behavior in various thermo-mechanical processes. Selected examples of applications of the developed model to simulations of metal forming processes, which involve strain localization, are presented in the work. An approach based on the Smoothed Particle Hydrodynamic, which allows to overcome difficulties with remeshing in the traditional CAFE method, is a subject of this work as well. In the developed model remeshing becomes possible and difficulties limiting application of the CAFE method to simple deformation processes are solved. Obtained results of numerical simulaA detailed description of possibilities given by the developed Cellular Automata—Finite Element (CAFE) multi scale model for prediction of the initiation and propagation of micro shear bands and shear bands in metallic materials subjected to plastic deformation is presented in the work. Particular emphasis in defining the criterion for initiation of micro shear and shear bands, as well as in defining the transition rules for the cellular automata, is put on accounting for the physical aspects of these phenomena occurring in two different scales in the material. The proposed approach led to the creation of the real multi scale model of strain localization phenomena. This model predicts material behavior in various thermo-mechanical processes. Selected examples of applications of the developed model to simulations of metal forming processes, which involve strain localization, are presented in the work. An approach based on the Smoothed Particle Hydrodynamic, which allows to overcome difficulties with remeshing in the traditional CAFE method, is a subject of this work as well. In the developed model remeshing becomes possible and difficulties limiting application of the CAFE method to simple deformation processes are solved. Obtained results of numerical simulations are compared with the experimental results of cold rolling process to show good predicative capabilities of the developed model.tions are compared with the experimental results of cold rolling process to show good predicative capabilities of the developed model.

Mg-based metallic glass / titanium interpenetrating phase composite with high mechanical performance

We report an Mg-based metallic glass/titanium interpenetrating phase composite in which constituent phases form a homogeneously interconnected network. The porous titanium constrains shear bands propagation thoroughly and promotes shear bands branching and intersection subsequently. The homogeneous phase distribution promotes regularly distributed local shear deformation and leads to a uniform deformation for the composites. Moreover, the interpenetrating phase structure introduces a mutual-reinforcement between metallic glass and titanium. Therefore, the composite exhibits excellent mechanical performance with compressive fracture strength of 1783 MPa and fracture strain of 31%.

Microstructure evolution and softening processes in hot deformed austenitic and duplex stainless steels

The microstructure evolution and softening processes occurring in 22Cr-19Ni-3Mo austenitic and 21Cr-10Ni-3Mo duplex stainless steels deformed in torsion at 900 and 1200 °C were studied in the present work. Austenite was observed to soften in both steels via dynamic recovery (DRV) and dynamic recrystallisation (DRX) for the low and high deformation temperatures, respectively. At 900 °C, an "organised", self-screening austenite deformation substructure largely comprising microbands, locally accompanied by micro-shear bands, was formed. By contrast, a "random", accommodating austenite deformation substructure composed of equiaxed subgrains formed at 1200 °C. In the single-phase steel, DRX of austenite largely occurred through straininduced grain boundary migration accompanied by (multiple) twinning. In the duplex steel, this softening mechanism was complemented by the formation of DRX grains through subgrain growth in the austenite/ferrite interface regions and by large-scale subgrain coalescence. At 900 °C, the duplex steel displayed limited stress-assisted phase transformations between austenite and ferrite, characterised by the dissolution of the primary austenite, formation of Widmanstätten secondary austenite and gradual globularisation of the transformed regions with strain. The softening process within ferrite was classified as "extended DRV", characterised by a continuous increase in misorientations across the sub-boundaries with strain, for both deformation temperatures.