The origin of "Rare Earth" texture development in extruded Mg-based alloys and its effect on tensile ductility

The extrusion behaviour, texture and tensile ductility of five binary Mg-based alloys have been examined and compared to pure Mg. The five alloying additions examined were Al, Sn, Ca, La and Gd. When these alloys are compared at equivalent grain size, the La- and Gd-containing alloys show the best ductilities. This has been attributed to a weaker extrusion texture. These two alloying additions, La and Gd, were found to also produce a new texture peak with View the MathML source parallel to the extrusion direction. This “rare earth texture” component was found to be suppressed at high extrusion temperatures. It is proposed that the View the MathML source texture component arises from oriented nucleation at shear bands.

Enhanced tensile ductility of an ultra-fine-grained aluminium alloy

Aluminum alloy 6082 was subjected to equal-channel angular pressing (ECAP), which resulted in an ultra-fine-grained (UFG) microstructure with an average grain size of 0.2–0.4 μm. There was a pronounced effect of the grain refinement on the strain-rate sensitivity and tensile ductility. The Hart criterion of tensile necking fails to explain the observed ductility of the UFG material at low strain rates. A correlation between the observed stronger-than-expected ductility and a tendency to microshear band formation at low strain rates was established.

Enhanced ductility and reduced asymmetry of Mg-2Al-1Zn alloy plate processed by torsion and annealing

The ductility and plastic asymmetry of an as-annealed magnesium alloy plate were studied in compression through combined process of torsion and subsequent annealing by optical microscope and EBSD. The yield strength (YS) and ultimate compression strength (UCS) as well as the compression ductility (CD) were simultaneously raised by prior torsion at room temperature. The CD was further enhanced by subsequent annealing. Also, the torqued sample followed by annealing experienced a rising CD with the increase in prior strain, leading to the maximum true strain of 0.279, which is twice that of the as-annealed original one. The sample showed a largely reduced tension-compression yield asymmetry by subjecting to pre-torsion alone or combined with a subsequent annealing. The enhanced ductility and reduced asymmetry are attributed to the development of a gradient microstructure with refined grains, and also randomization of the weakened texture due to torsion and subsequent annealing.

Deep drawing behaviour of ultrafine grained copper : modelling and experiment

Ultrafine grained materials produced by severe plastic deformation methods possess attractive mechanical properties such as high strength compared with traditional coarse grained counterparts and reasonable ductility. Between existing severe plastic deformation methods the Equal Channel Angular Pressing is the most promising for future industrial applications and can produce a variety of ultrafine grained microstructures in materials depending on route, temperature and number of passes during processing. Driven by a rising trend of miniaturisation of parts these materials are promising candidates for microforming processes. Considering that bi-axial deformation of sheet (foil) is the major operation in microforming, the investigation of the influence of the number of ECAP passes on the bi-axial ductility in micro deep drawing test has been examined by experiments and FE simulation in this study. The experiments have showed that high force was required for drawing of the samples processed by ECAP compare to coarse grained materials. The limit drawing ratio of ultrafine grained samples was in the range of 1.9–2.0 with ECAP pass number changing from 1 to 16, while a higher value of 2.2 was obtained for coarse grained copper. However, the notable decrease in tensile ductility with increase in strength was not as pronounced for bi-axial ductility. The FE simulation using standard isotropic hardening model and von Mises yielding criterion confirmed these findings.

Reactive block copolymer modified thermosets : highly ordered nanostructures and improved properties

A highly ordered poly(dimethyl siloxane)-poly(glycidyl methacrylate) (PDMS-PGMA) reactive diblock copolymer was synthesized and used to modify bisphenol A-type epoxy resin (ER). The PDMS-PGMA block copolymer consisted of epoxy-miscible PGMA blocks and an epoxy-immiscible PDMS block. The PGMA reactive block of the block copolymer formed covalent bonds with cured epoxy and was involved in the network formation, and the PDMS block phase separated to give different ordered and disordered nanostructures at different blend compositions. The solvent cast PDMS-PGMA diblock copolymer showed ordered hexagonal cylindrical morphology. A highly ordered morphology consisting of hexagonal cylinders inside the lamellar morphology was observed in the cured PDMS-PGMA block copolymer. In the cured ER/PDMS-PGMA blends, a variety of morphologies including lamellar, cubic and worm-like and spherical nanostructures were detected depending on the blend composition. Moreover, the addition of this reactive diblock copolymer significantly increases the hydrophobicity and the glass transition temperature. It also improves the tensile strength and tensile ductility of the nanostructured thermosets at low diblock copolymer contents.

"Rare Earth" texture development in extruded Mg-based alloys

This data collection addresses the problem of low ductility in magnesium alloys, preventing their wider use. It examines a series of dilute alloys in order to determine the effect of composition on the extrusion behaviour and texture, and on the room temperature tensile ductility.

Enhanced mechanical response of an ultrafine grained Ti-6Al-4V alloy produced through warm symmetric and asymmetric rolling

An equiaxed ultrafine-grained (UFG) microstructure was successfully produced in a Ti-6Al-4V alloy with an average grain size of 110-230. nm through symmetric and asymmetric warm rolling of a martensitic starting microstructure. The UFG material displayed a combination of ultrahigh strength and ductility at room temperature. Compared with the conventional symmetric rolling, the asymmetric rolling process led to a more pronounced effect of microstructure refinement and a higher tensile ductility. The optimum mechanical response was obtained though the asymmetric rolling at 70% reduction, offering an ultimate tensile strength of 1365. MPa and a total elongation of ~23%. Apart from the magnitude of grain refinement, the inclination of basal texture component from the normal towards the rolling direction during asymmetric rolling and possible strain induced β to martensite transformation may concurrently contribute to a remarkable tensile strength-ductility balance.

The effect of thermomechanical treatment on the microstructure and the mechanical behavior of a supersaturated Cu-Ag alloy

Supersaturated Cu-3at.% Ag alloy was processed by cold rolling and short-time annealing in order to achieve a combination of high strength and good tensile ductility. After annealing of the rolled samples a heterogeneous solute atom distribution was developed due to the dissolution of nanosized Ag particles in some volumes of the matrix. In regions with higher solute content, the high dislocation density formed due to rolling was stabilized, while in other volumes the dislocation density decreased. The heterogeneous microstructure obtained after annealing exhibited a much higher ductility and only a slightly lower strength than in the as-rolled state.

The influence of temporary hydrogenation on ECAP formability and low cycle fatigue life of CP titanium

It is generally believed that thermo-hydrogen processing has a beneficial effect on tensile ductility and fatigue properties of titanium. This study was concerned with investigating whether this also applies to titanium of commercial purity (CP) with an ultrafine-grained structure obtained by equal-channel angular pressing (ECAP). It was shown that despite the possibility to manipulate the microstructure of titanium the thermo-hydrogen processing offers, temporary hydrogenation was not able to improve ductility and low cycle fatigue life of CP titanium over the levels achievable by straight ECAP.

Twinning and the ductility of magnesium alloys Part II. “Contraction” twins

Magnesium and its alloys do not in general undergo the same extended range of plasticity as their competitor structural metals. The present work presents part II of a study that examines some of the roles deformation twinning might play in the phenomenon. A series of tensile and compression tests results are reported for common wrought alloys: AZ31, ZK60 and ZM20. These data are combined with EBSD analysis and simple flow stress models to argue the following: (i) that “contraction” double twinning (which enables contraction along the c axis) can decrease the uniform elongation, and (ii) that compression double twinning can also account for shear failure at low strains. The last of these is described as a combined consequence of strain softening of the continuum and the local generation of twin sized voids.

Twinning and the ductility of magnesium alloys Part I: “Tension” twins

Magnesium and its alloys do not in general undergo the same extended range of plasticity as their competitor structural metals. The present work is part I of a study that examines some of the roles deformation twinning might play in the phenomenon. A series of tensile test results are reported for the common wrought alloy AZ31. These data are employed in conjunction with a simple constitutive model to argue that View the MathML source twinning (which gives extension along the c-axis) can increase the uniform elongation in tensile tests. This effect appears to be similar to that seen in Ti, Zr and Cu–Si and in the so called TWIP phenomenon in steel.

Tensile deformation of a ultrafine-grained aluminium alloy: micro shear banding and grain boundary sliding

This work investigates the relationship between the strain rate and the ductility and the underlying deformation mechanisms in an ultrafine-grained Al6082 alloy. At room temperature the uniform elongation of the material exhibits a marked increase with decreasing strain rate. This effect is related to the activation of micro shear banding, which is controlled by grain boundary sliding. The contribution of these mechanisms to uniform elongation is estimated. It is proposed that the grain boundary sliding suppresses the transformation of micro shear bands into macro shear bands. The activity of other deformation mechanisms during plastic deformation of the ultrafine-grained material is also discussed.

T-Shaped equi-channel angular pressing of Pb-Sn eutectic and its tensile properties

Equi-channel angular pressing (ECAP) of a Pb–Sn eutectic alloy up to six passes in a T-shaped die, rather than a conventional L-shaped die, was studied for grain refinement. The effect of ECAP on the hardness and tensile properties was studied. Microstructure predominately changed in the early part of the ECAP process and became equiaxed and uniformly distributed in both the longitudinal and the transverse sections after four passes. There occurred substantial softening over the first two passes—hardness of 10 Hv, yield strength of 14.2 MPa and tensile strength of 16.3 MPa in the as-cast condition decreased upon two passes to 6 Hv, 9.7 MPa and 13.0 MPa, respectively. The ductility (% elongation) increased drastically from <50% in the as-cast condition to 150% upon two passes, and further increased to 230% after four passes. Various tensile properties and concurrent microstructural evolution were used to develop a mutual relationship among them.

Some issues relating to the ductility of wrought magnesium alloys

The present work is concerned with gaining a better understanding of the factors that control the ductility of wrought magnesium alloys. The ultimate aim is to develop alloys with vastly improved room temperature formability. It is shown that 3D tomography of fractured tensile specimens reveals disk shaped voids aligned more or less at 45 deg. to the tensile axis. These voids are consistent with twin induced void formation. It is also shown that the double twins that produce such voids form in contradiction to Schmid predictions. Finally, it is demonstrated that low levels of rare-earth additions leads to vastly improved texture and ductility in extrusions, as they do in rolled sheet.