Ultrassonic Analysis of UO2 Pellets

Ceramic materials have been widely used for various purposes in many different industries due to certain characteristics, such as high melting point and high resistance to corrosion. In the nuclear area, ceramics are of great importance due to the process of fabrication of fuel pellets for nuclear reactors. Generally, high accuracy destructive techniques are used to characterize nuclear materials for fuel fabrication. These techniques usually require costly equipment and facilities, as well as experienced personnel. This paper aims at presenting an analysis methodology for UO2 pellets using a non-destructive ultrasonic technique for porosity measurement. This technique differs from traditional ultrasonic techniques in the sense it uses ultrasonic pulses in frequency domain instead of time domain. Therefore, specific characteristics of the analyzed material are associated with the obtained frequency spectrum. In the present work, four fuel grade UO2 pellets were analyzed and the corresponding results evaluated.

Analysis of Ultrasonic Techniques for the Characterization of Microfiltration Polymeric Membranes

The use of polymeric membranes is extremely important in several industries such as nuclear, biotechnology, chemical and pharmaceutical. In the nuclear area, for instance, systems based on membrane separation technologies are currently being used in the treatment of radioactive liquid effluent, and new technologies using membranes are being developed at a great rate. The knowledge of the physical characteristics of these membranes, such as, pore size and the pore size distribution, is very important to the membranes separation processes. Only after these characteristics are known is it possible to determine the type and to choose a particular membrane for a specific application. In this work, two ultrasonic non destructive techniques were used to determine the porosity of membranes: pulse echo and transmission. A 25 MHz immersion transducer was used. Ultrasonic signals were acquired, for both techniques, after the ultrasonic waves passed through a microfiltration polymeric membrane of pore size of 0.45 μm and thickness of 180 μm. After the emitted ultrasonic signal crossed the membrane, the received signal brought several information on the influence of the membrane porosity in the standard signal of the ultrasonic wave. The ultrasonic signals were acquired in the time domain and changed to the frequency domain by application of the Fourier Fast Transform (FFT), thus generating the material frequency spectrum. For the pulse echo technique, the ultrasonic spectrum frequency changed after the ultrasonic wave crossed the membrane. With the transmission technique there was only a displacement of the ultrasonic signal at the time domain.