2 resultados para REDUCTION REACTION
em Boston University Digital Common
Resumo:
A simple, solventless procedure for reductive amination that results in an impressive color change. Reaction proceeds in three stages: imine formation, reduction, and acetylation and purification is done by crystallization.
Resumo:
A simple experiment to demonstrate nucleophilic addition to a carbonyl. Sodium borohydride-mediated reduction of fluorenone is a fast and high-yielding reaction that is suitable for beginning students. Students isolate their fluorenol product by recrystallization and characterize it by NMR and IR.