适宜海水钻井液体系新前置液实验和现场试验

前置液是影响固井质量的重要因素之一,对于海水钻井液体系,如何选用前置液是一个新的课题.提出了一种适宜于海水钻井液体系的新型前置液,对其在固井过程中的各种性能进行了室内实验研究,结果表明:新型前置液与海水钻井液、固井水泥浆及盐水等环境流体有良好的相容性,对井壁具有稳定作用,其中的固体颗粒及表面活性剂有利于冲刷海水钻井液形成的泥饼.在此基础上,将新型前置液应用于胜利油田的固井作业,进行现场试验,发现:应用新型前置液后,环空水泥浆界面清晰,混浆段长度缩短,第2界面的胶结质量有明显提高.

PIXE and ICP-AES analysis of early glass unearthed from Xinjiang (China)

Early glasses (about 1066 BC-220 AD) unearthed from Xinjiang of China were chemically characterized by using PIXE and ICP-AES. It was found that these glasses were basically attributed to PbO-BaO-SiO2 system, K2O-SiO2 system, Na2O-CaO-SiO2 system and Na2O-CaO-PbO-SiO2 system. The results from the cluster analysis showed that some glasses had basically similar recipe and technology. The PbO-BaO-SiO2 glass and the K2O-SiO2 glass were thought to come from the central area and the south of ancient China, respectively. The part of the Na2O-CaO-SiO2 glass (including the Na2O-CaO-PbO-SiO2 glass) might be imported from Mesopotamia, while the other part might be locally produced. (c) 2005 Elsevier B.V. All rights reserved.

DELINEATION OF DEFECTS IN SIMOX STRUCTURES USING A CHEMICAL ETCHING TECHNIQUE

Residual defects in the overlayer of fully annealed SIMOX material have been studied by means of a chemical etching technique. The etching procedure has been calibrated and an optimum recipe is reported. Observations using optical microscopy and transmission electron microscopy have been used to quantify the defect densities and good agreement between the two techniques has been established, confirming that the optimised chemical etching process can be used with confidence to determine the dislocation density for values < 10(7) cm-2.