车载式变量施药机控制系统设计与试验

施药控制是提高作业质量、减少化学污染、降低生产成本的关键技术。该文基于单片机AT89C52,采用滞环控制法,设计了一种车载式变量施药机控制系统。该系统能够根据施药机行走速度自动变更喷药量,实现施药量不变。试验表明:加速度小于0.4m/s2时,实际施药量与设定施药量之间的误差不超过8%,且雾化效果良好、生产效率高,还可以减少农药的残留和对环境的污染,能够满足农业生产的需要。

Determination of 266 pesticide residues in apple juice by matrix solid-phase dispersion and gas chromatography-mass selective detection

A macro matrix solid-phase dispersion (MSPD) method was developed to extract 266 pesticides from apple juice samples prior to gas chromatography-mass selective detection (GC-MSD) determination. A 10 g samples was mixed with 20 g diatomaceous earth. The mixture was transferred into a glass column. Pesticide residues were leached with a 160 mL hexane-dichloromethane (1:1) at 5 mL/min. Two hundred and sixty-six pesticides were divided into three groups and detected by GC-MSD under selective ion monitoring. The proposed method takes advantage of both liquid-liquid extraction and conventional MSPD methods. Application was illustrated by the analysis of 236 apple juice samples produced in Shaanxi province China mainland this year. (C) 2004 Elsevier B.V. All rights reserved.