科尔沁沙地69种植物种子重量比较研究

研究了科尔沁沙地 6 9种植物的繁殖体 (30种为种子 ,39种为果实 )重量。结果表明 :1 )传播体为果实的植物可分为 4个组别 (即果实单粒重 <0 .1mg、0 .1～ 0 .9999mg、1～ 9.9999mg、1 0～ 99.9999mg) ;黄蒿 (Artemisiasco paria)果实 (0 .0 5 1 7mg)和小香蒲 (Typhaminima)果实 (0 .0 6 82mg)最轻 ,苍耳 (Xanthiumsibiricum)单个果实 (77.894 3mg)最重 ;2 )传播体为种子的植物可分为 3个组别 (即种子单粒重 0 .1～ 0 .9999mg、1～ 9.9999mg、1 0～ 99.9999mg) ;马齿苋 (Portulacaoleracea)种子 (0 .1 5 1 4mg)最轻 ,苦参 (Sophoraflavescens)种子 (4 6 .781 6mg)最重 ;3)黄蒿、马齿苋、轮叶沙参 (Adenophoratetraphylla)、碱地肤 (Kochiasieversiana)、狼尾花 (Lysimachiabarystachys)、灰绿藜 (Chenopodiumglaucum)、刺沙蓬 (Salsolaruthenica)、菟丝子 (Cuscutachinensis)、大籽蒿 (Artemisiasieversiana)、狗尾草 (Setariaviridis)、野古草 (Arundinellahirta)等植物所以广泛分布可能是因为它们繁殖体轻 (<1mg)且具有持久土壤种子库 ;4 )流沙上的先锋植物或沙生演替系列前期植物沙蓬 (Agriphyllumsquarrosum)、差巴嘎蒿 (Artemisiahalodendron)、乌丹蒿 (Artemisiawudanica)、狗尾草、雾冰藜 (Bassia

Ni_(69.5)Al_(28)Y_(2.5)粉末的机械合金化

对 Ni6 9.5Al2 8Y2 .5粉末进行球磨 ,获得 Ni Al金属间化合物 .研究粉末结构与球磨时间的关系 ,探索以中间合金的形式加入稀土元素的机械合金化方法 .结果表明 ,加入稀土元素后 ,用机械合金化的方法可以生成新的金属间化合物.

Analysis of mussel standard reference material by inductively coupled plasma atomic emission spectrometry and inductively coupled plasma mass spectrometry

A method for the analysis of mussel standard reference material by inductively coupled plasma atomic emission spectrometry( ICP-AES) and inductively coupled plasma mass spectrometry(ICP-MS) was developed. K, Na, Ca, Mg, P, Al, Fe, Zn, Mn and Sr were determined by ICP-AES and As, B, Cd, Co, Cr, Cu, Ga, Ge, Mn, Mo, Ni, Pb, Se, Sr, U and V by ICP-MS, The interference coefficients at the Mn-55, Se-78, Cu-63, Co-59, Ni-58, Ni-60, As-75, Se-77, V-51, Cr-53 and Cr-52 originating from polyatomic ion of the matrix elements (KO)-K-39-O-16, K-39(2), (ArNa)-Ar-40-Na-23, (CaO)-Ca-43-O-16, (CaO)-Ca-42-O-16, (CaO)-Ca-44-O-16, (PO2)-P-31-O-16, (ArCl)-Ar-40-Cl-35, (ArCl)-Ar-40-Cl-37, (ClO)-Cl-35-O-16, (ClO)-Cl-37-O-16 and (ArC)-Ar-40-C-12 were determined under the selected operation parameters. The major matrix elements, such as K, Na and Ca, result in the suppression of analytes signals. The apparent concentration at the significant biological element which was produced by the different digestion methods, (.) HNO3 + H2O2 (3 + 2), HNO3 + HClO4 (3 + 0.5) and HNO3 + H2SO4 (3 + 0.5),was determined. The sample digested by HNO3 + H2O2 did not give rise to interfere on the analyte, and the backgrounds of Se-77, Ga-69, Zn-67, As-75, V-51, Cr-53 and Cr-52 were increased by HNO3 + HClO4 digestion method, that affected the determination of these elements, especially the monoisotope As and V. Sample digested by HNO3 + H2SO4 increased the backgrounds at Cu-65, Zn-64 and Zn-67. Detection limits of ICP-AES are 0.001 similar to 0.75 mg/L and those of ICP-MS are 0.005 similar to 1.01 mu g/L. The relative standard derivations of ICP-AES and ICP-MS are 2.7% similar to 12.8%, 3.4% similar to 24.8%, respectively.