一种面向不完整数据流上的k-支配skyline查询算法

skyline查询是数据挖掘一个重要的研究方向,在基于数据的决策支持等应用中有着重要的作用.由于现实应用中存在着大量的不完整数据流,但大多数现有的skyline查询算法都依赖于如下的假设:1)任意数据点的所有维度值都是已知的;2)数据集是稳定、有界的并且可以随意访问.此外,随着数据维度的增加,skyline数据点的个数会变得过多,因此引入了k-支配skyline的概念,但是不完整数据的k-支配关系并不具有传递性,现有的skyline查询算法都无法适用.基于这些问题,考虑到数据流高维、无界、顺序性的特点,并且在某些维度上可能具有缺失值的特性,提出了一种新的基于滑动窗口的不完整数据流的k-支配skyline查询算法,实验结果表明,算法不仅可以支持不完整数据流上的k-支配skyline计算,并能够保证效率和性能.

落地原油对芦苇湿地生态工程净化系统影响

以芦苇湿地为介质净化石油开采过程中落于地面的原油 ,研究了中试条件下芦苇湿地的净化效果及落地原油对土壤和芦苇介质的影响。结果表明 :芦苇湿地对不同施入剂量的落地原油都有较好的净化率 ,在试验运行期内 ,芦苇湿地对矿物油的净化率高达 88%～ 96 %。落地原油对土壤的污染基本局限于表层 ,对深层土壤的污染趋势并不明显 ,一般 4 0～6 0 cm土层的矿物油含量已接近或低于对照区表层土的背景值 ;落地原油对芦苇生长指标的影响表现出两面性 ,一方面抑制芦苇的叶龄指数和株高生长量 ,另一方面又能刺激芦苇的长粗、增加芦苇的生物量 ;落地原油对纤维素、木质素、戊糖、纤维素宽及纤维素长宽比等芦苇品质指标的影响很小 ,一些指标甚至优于对照区。

南亚热带森林群落演替过程中林下土壤的呼吸特征

采用CI-310便携式光合作用系统及其附件,测定了广东省黑石顶自然保护区南亚热带森林演替系列中的马尾松林和松阔混交林林下土壤的呼吸速率。测定结果显示:在自然条件下,马尾松林土壤呼吸速率在1.650~4.0μmolCO2m-2s-1,松阔混交林土壤呼吸速率在1.70~3.950μmolCO2m-2s-1之间。林下土壤呼吸速率与温度和土壤空气相对湿度可用拟合,据此并结合当地气象资料推算出马尾松林和松阔混交林的年均土壤呼吸量分别为31.027、36.629 tCO2hm-2,后者高于前者。

田间管理措施减少玉米黄曲霉侵染的效果研究

[目的]减少黄曲霉侵染作物的几率。[方法]结合辽宁地区玉米生产状况,选择耕作措施、灌溉状况、施氮水平、作物品种、种植密度为影响因子,研究田间管理措施减少玉米田间黄曲霉种群侵染的效果。[结果]耕作措施能明显减少土壤中黄曲霉种群数量,与连作相比,轮作能降低土壤中黄曲霉数量。灌溉状况、施氮水平、作物品种和种植密度对土壤中黄曲霉数量没有影响。连作田间的黄曲霉平均菌落数大于轮作田间。灌溉状况对减少玉米黄曲霉侵染的效应优于其他因素。检测到黄曲霉的土壤含水量在5%~13%,当田间土壤含水量低于13%时,应及时灌溉。[结论]在田间管理中实施合理轮作和适时灌溉,可预防黄曲霉侵染。

Hydrothermal synthesis, crystal structure and electrochemical properties of a novel 3D Dawson-type polyoxometalate supramolecular network

A novel Dawson-type polyoxometalate supramolecular architecture of the formula [4,4'-H(2)bipy](2.5)center dot[4,4'-Hbipy]center dot[P2W18O62]center dot 6.25H(2)O (4,4'-bipy = 4,4'-bipyridine) has been hydrothermally synthesised and characterised by means of elemental analysis, IR, CV and X-ray single-crystal diffraction. X-ray crystallography indicates that the title compound consists of Dawson-type polyoxoaions [P2W18O62](6-), water molecules and 4,4'-bipy units. The polyoxoanion clusters together with 4,4'-bipy units and water molecules to construct the three-dimensional supramolecular network through hydrogen bonds. The crystal structure analyses reveal that water molecules and 4,4'-bipy units play the important role on the packing arrangements of crystals. Cyclic voltammetry shows that the title compound exhibits three chemically reversible steps

白光有机发光二极管的制备方法

有机发光二极管(OLEDs)以其制备工艺简单、成本低、发光颜色可在可见光区内任意调节、易于大面积制作和可制成柔性器件等优点,被认为是未来重要的显示技术之一,在照明光源领域也显示了诱人的应用前景。文章阐述了实现白光OLEDs的方法及其近期进展,并结合自身工作介绍了白光OLEDs的制备方法,最后对白光OLEDs目前存在的问题及其发展趋势进行了讨论。

Radiation effects on the immiscible polymer blend of nylon1010 and high-impact strength polystyrene (II): mechanical properties and morphology

The paper studies the morphology and mechanical properties of immiscible binary blends of the nylon 1010 and HIPS through the radiation crosslinking method. In this blend, the HIPS particles were the dispersed phases in the nylon 1010 matrix. With increasing of dose, the elastic modulus increased, However, the tensile strength. elongation at bleak and the energy of fracture increased to a maximum at a dose of 0.34 MGy, then reduced with the increasing of dose. SEM photographs show that the hole sizes are not changed obviously at low dose and at high dose, remnants that cannot be dissolved in formic acid and THF can be observed in the holes and on the surface. TEM photographs showed that radiation destroys the rubber phases in the polymer blend. (C) 2001 Elsevier Science Ltd. All rights reserved.

Fluorescence and aggregation behavior of a polyimide in solutions

The UV-visible absorption and fluorescence spectra of a soluble polyimide, YS-30, in several organic solvents were measured over a wide range of concentration. The experimental results show that there exist both intramolecular and intermolecular electron donor acceptor interactions for YS-30 molecules. The fluorescence behavior of YS-30 in N,N-dimethylacetamide and in chloroform solutions is similar in general, except that its ground-state intermolecular charge transfer emission is more obvious in N,N-dimethylacetamide solution. This difference is attributed to the greater extent of disruption of the chain packing by solvent or/and the more efficient radiationless energy dissipation process from the excited state complexes to chloroform. The intensity ratio of intermolecular charge transfer emission to intramolecular charge transfer emission is used to characterize the state of aggregation of YS-30 molecules in solutions. The plot of this ratio versus concentration indicates the existence of two critical concentrations. It is also found from the same plot that the decrease of coil size is very pronounced during the initial stage of shrinkage.

La_(1-x)Li_xMnO_3体系的输运特性及EPR研究

利用固相反应法合成了掺杂锂的La1-xLixMnO3(x=0,0.10,0.15,0.20,0.25,0.30)钙钛矿氧化物．XRD测试表明，所有样品均为菱方结构．除x=0,0.3外，其它样品均随温度的降低在液氮温区可观察到从绝缘态到金属态的转变，其中x=0.15样品的转变温度最高为167K．在H=1T的磁场下，出现了负磁阻现象．EPR谱上的ｇ＝2.00信号与Mn3+和Mn4+组成的复合团簇有关

《热分析》评介

热分析技术应用甚广,尤其自80年代初我国开始热分析学会活动以来,10余年间我国在该领域取得了长足的进步,尽管相继出现了一些热分析的译著和专著,但适于作教材的著述,由蔡正千编写的《热分析》(高等教育出版社1993年出版)还是第一本。作者基于多年从事热分析教学和科研的切身体会和坚实基础,用简明的语言,阐述了热分析的一些基本问题,作到了言简意赅,深入浅出。表现出如下一些明显特点: ·本书作为教材详简适度,布局合理。全书258页,21万字。首先从基本的物理化学概念,如物质的热学性质和热量传递等入手,接着讲解几种主要的热分析方法,再讲一些典型的应用示例。从上述几个侧面,可让学习者通过为数不多的课时就可了解热分析总的概貌。

介体型双酶D-氨基酸传感器的制备

用一种全氟代磺酸酯阳离子交换树酯(East-man AQ-55),将D-氨基酸氧化酶(DAAO),辣根过氧化物酶(HRP)以及1,1′-二(α-羟基乙基)二茂铁(BHFc)同时包埋在玻碳电极(GCE)表面,制成双酶D-氨基酸电流式传感器。电极的工作电位为+0.18V(vs.SCE)响应时间小于50s。对于D-丙氨酸来说,测定的最适宜pH为7.8,测定的线性范围为0.05～0.75mmol/L该电极具有良好的重现性,可以连续使用200次。

Chandrananimycins A-C: Production of novel anticancer antibiotics from a marine Actinomadura sp isolate M048 by variation of medium composition and growth conditions

In our screening of marine actinomycetes for bioactive principles, three novel antibiotics designated as chandrananimycin A (3c), B (3d) and C (4) were isolated from the culture broth of a marine Actinomadura sp. isolate M045. The structures of the new antibiotics were determined by detailed interpretation of mass, 1 D and 2 D NMR spectra.

Molecular cloning and expression of a novel Kazal-type serine proteinase inhibitor gene from Zhikong scallop Chlamys farreri, and the inhibitory activity of its recombinant domain

Serine proteinase inhibitors (SPIs) play important roles in host physiological and immunological processes in all multicellular organisms. A novel Kazal-type SPI gene was cloned from the Zhikong scallop Chlamys farreri (designated as CfKZSPI) by expressed sequence tag (EST) and rapid amplification of cDNA ends (RACE) approaches. The full-length cDNA of CfKZSPI was of 1788 nucleotides with a canonical polyadenylation signal sequence AATAAA and a polyA tail, and an open reading frame (ORF) encoding a polypeptide of 509 amino acids with a putative signal peptide of 22 amino acids. The deduced amino acid sequence of CfKZSPI contained 12 tandem Kazal domains with high similarity to other Kazal-type SPIs. The temporal expression of CfKZSPI in hemocytes after Vibrio anguillorum challenge was recorded by quantitative real-time RT-PCR. The relative mRNA expression level of CfKZSPI was up-regulated and reached 43.6-fold at 3 h post-challenge. After a decrease at 6 h, the expression Level increased again and reached 207.8-fold at 12 h post-challenge. The 12th Kazal domain of CfKZSPI was recombined into pET-32a(+) and expressed in Escherichia coli Rosetta-gami (DE3) to investigate its inhibitory activity. The purified recombinant protein (rCf KZSPI-1 2) showed significant inhibitory activity against trypsin but no activity against thrombin. When the molar ratio of inhibitor to trypsin reached 1:1, almost 90% of the enzyme activity could be inhibited, which suggested that one molecule of rCfKZSPI-12 was able to inhibit one molecule of trypsin. Kinetics analysis with Dixon plot showed that the inhibition constant (K-i) of rCfKZSPI-12 to trypsin was 173 nmol L-1. These results indicated that CfKZSPI was a novel Kazal-type SPI with significant inhibitory activity against trypsin, and was suspected to be involved in scallop immune response. (c) 2008 Elsevier Ltd. All rights reserved.

Determination of fractional energy loss of waves in nearshore waters using an improved high-order Boussinesq-type model

Fractional energy losses of waves due to wave breaking when passing over a submerged bar are studied systematically using a modified numerical code that is based on the high-order Boussinesq-type equations. The model is first tested by the additional experimental data, and the model's capability of simulating the wave transformation over both gentle slope and steep slope is demonstrated. Then, the model's breaking index is replaced and tested. The new breaking index, which is optimized from the several breaking indices, is not sensitive to the spatial grid length and includes the bottom slopes. Numerical tests show that the modified model with the new breaking index is more stable and efficient for the shallow-water wave breaking. Finally, the modified model is used to study the fractional energy losses for the regular waves propagating and breaking over a submerged bar. Our results have revealed that how the nonlinearity and the dispersion of the incident waves as well as the dimensionless bar height (normalized by water depth) dominate the fractional energy losses. It is also found that the bar slope (limited to gentle slopes that less than 1:10) and the dimensionless bar length (normalized by incident wave length) have negligible effects on the fractional energy losses.