Thiosaccharine disulfide: synthesis, crystal structure, spectroscopic characterization and theoretical study
| Contribuinte(s) |
UNIVERSIDADE DE SÃO PAULO |
|---|---|
| Data(s) |
21/05/2014
21/05/2014
01/01/2013
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| Resumo |
The title compound, (thiosaccharine disulfide), bis[1,10dioxide-2,3-dihidro-1,2-benzoisothiazol]disulfide, (tsac)2 has been synthesized and fully characterized by UV–Visible, IR, Raman, 1H and 13C NMR spectroscopy elemental analysis and structural X-ray crystallography. A DFT theoretical study has been performed and good agreement between experimental and theoretical values of structural parameters and vibration frequencies have been achieved. Universidad Nacional del Sur (UNS) - Secretaría General de Ciencia y Tecnología (SGCyT) (M24/Q043) CONICET FAPESP |
| Identificador |
Journal of Molecular Structure, Amsterdam : Elsevier BV, v. 1032, p. 48-55, Jan. 2013 0022-2860 http://www.producao.usp.br/handle/BDPI/44968 10.1016/j.molstruc.2012.07.043 |
| Idioma(s) |
eng |
| Publicador |
Elsevier BV Amsterdam |
| Relação |
Journal of Molecular Structure |
| Direitos |
restrictedAccess Copyright Elsevier B.V. |
| Palavras-Chave | #Thiosaccharine #Disulfide #Crystal structure #Infrared #Raman #UV–Visible spectroscopy #CRISTALOGRAFIA ESTRUTURAL #INFRAVERMELHO #ESPECTROSCOPIA RAMAN |
| Tipo |
article original article publishedVersion |
