Determination of atenolol in environmental water samples and pharmaceutical formulations at a graphite-epoxy composite electrode
| Contribuinte(s) |
UNIVERSIDADE DE SÃO PAULO |
|---|---|
| Data(s) |
06/11/2013
06/11/2013
2012
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| Resumo |
A bare graphite-epoxy composite was evaluated as an electrode material in the determination of atenolol in natural water samples and pharmaceutical formulations for which the analyte was spiked. Using a DPV procedure, a linear response was observed in the 4.45-84.7 mu mol L-1 range with a LOD = 2.23 mu mol L-1, without need of surface renewal between successive runs, and recoveries between 92.5 and 107.5% for pharmaceutical formulations. The results obtained from the proposed procedure agreed with HPLC results within a 95% confidence level. During the determination of atenolol in water samples, recoveries between 96.1 and 102.6% were found. FAPESP FAPESP CMFC [08/03537-7] CMFC |
| Identificador |
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, ABINGDON, v. 92, n. 5, supl. 1, Part 6, pp. 561-570, SEP, 2012 0306-7319 http://www.producao.usp.br/handle/BDPI/42285 10.1080/03067310903582358 |
| Idioma(s) |
eng |
| Publicador |
TAYLOR & FRANCIS LTD ABINGDON |
| Relação |
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY |
| Direitos |
restrictedAccess Copyright TAYLOR & FRANCIS LTD |
| Palavras-Chave | #ATENOLOL #GRAPHITE-EPOXY COMPOSITE ELECTRODE #DPV #OIL POLYURETHANE COMPOSITE #TANDEM MASS-SPECTROMETRY #LIQUID-CHROMATOGRAPHY #BETA-BLOCKERS #PLASMA #PHASE #HPLC #CHEMISTRY, ANALYTICAL #ENVIRONMENTAL SCIENCES |
| Tipo |
article original article publishedVersion |
