Effect of surface treatment on the bond strength between yttria partially stabilized zirconia ceramics and resin cement

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

Statement of problem. No consensus has been reached on the best bonding protocol between a zirconia ceramic surface and the tooth structure.Purpose. The purpose of this study was to evaluate the extrusion shear strength between yttria partially stabilized zirconia ceramics and resin cement (Panavia F) after different surface treatments.Material and methods. The surface treatments evaluated (n=7) included the following: G1-control group (no surface treatment); G2-treated with MDP primer (Alloy Primer); G3-treated with 40% hydrofluoric acid (210 seconds); and G4-treated with 40% hydrofluoric acid (210 seconds) followed by MDP primer. The specimens were bonded to 2.5-mm-thick disks of bovine root dentin, and the extrusion shear tests were performed after they had been stored for 24 hours in distilled water at 37 degrees C. The surface modifications were assessed on 2 specimens that were selected from each group by scanning electron microscopy. Data were analyzed with 1-way ANOVA and the Tukey-Kramer honestly significant difference test (alpha=.05).Results. G4 (mean 2.84, standard deviation [SD] 0.43 MPa) presented significantly higher (P<.001) extrusion shear strength when compared with the other groups in the study (G1: mean, 1.57; SD 0.28 MPa; G2: mean 1.46, SD 0.28 MPa; G4: mean 1.16, SD 0.41 MPa). No significant differences were found among the other groups in the study.Conclusions. Yttria partially stabilized zirconia ceramics can be treated with 40% hydrofluoric acid for 210 seconds to increase the bond strength with the resin cement.