New methodology for a faster synthesis of SrSnO3 by the modified Pechini method


Autoria(s): Lucena, G. L.; Souza, J. J N; Maia, A. S.; Soledade, L. E B; Longo, Elson; Souza, A. G.; Santos, I. M G
Contribuinte(s)

Universidade Estadual Paulista (UNESP)

Data(s)

27/05/2014

27/05/2014

01/04/2013

Resumo

SrSnO3, a perovskite-type complex oxide, was synthesized by the modified Pechini method using two different precursors, tin chloride and metallic tin. The first one is already traditional in the literature and it claims about 30 days, only for the cleaning of tin citrate aiming at the elimination of the chloride. The second route was developed by our research group and saves time, taking 6 h to complete the synthesis of the resin. The results show that SrSnO3 obtained from the metallic tin show a higher short range order, leading to a band gap value higher than those reported in the literature, besides a meaningful reduction in the formation of SrCO 3, as compared to the one obtained from tin chloride.

Formato

249-253

Identificador

http://dx.doi.org/10.1590/S0366-69132013000200009

Ceramica, v. 59, n. 350, p. 249-253, 2013.

0366-6913

1678-4553

http://hdl.handle.net/11449/75004

10.1590/S0366-69132013000200009

S0366-69132013000200009

2-s2.0-84885051893

2-s2.0-84885051893.pdf

Idioma(s)

eng

Relação

Cerâmica

Direitos

openAccess

Palavras-Chave #Chemical synthesis #Perovskite #Stannate
Tipo

info:eu-repo/semantics/article