Synthesis, characterization and thermal behaviour of heavy lanthanide and yttrium pyruvates in the solid state
Contribuinte(s) |
Universidade Estadual Paulista (UNESP) |
---|---|
Data(s) |
20/05/2014
20/05/2014
01/04/2010
|
Resumo |
Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq) Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES) Processo FAPESP: 90/2932-4 Processo FAPESP: 05/00926-4 Solid-state Ln-L compounds, where Ln stands for heavy trivalent lanthanides or yttrium (III) (Tb-Lu, Y) and where L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal behaviour, ligand denticity of the isolated complexes. |
Formato |
95-100 |
Identificador |
http://dx.doi.org/10.1007/s10973-009-0537-y Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 100, n. 1, p. 95-100, 2010. 1388-6150 http://hdl.handle.net/11449/42201 10.1007/s10973-009-0537-y WOS:000276744500014 |
Idioma(s) |
eng |
Publicador |
Springer |
Relação |
Journal of Thermal Analysis and Calorimetry |
Direitos |
closedAccess |
Palavras-Chave | #Heavy lanthanides and yttrium #Pyruvate #Characterization #Thermal behaviour |
Tipo |
info:eu-repo/semantics/article |