Synthesis, characterization and thermal behaviour of solid 2-methoxybenzoates of trivalent metals


Autoria(s): Siqueira, A. B.; Carvalho, C. T.; Ionashiro, E. Y.; Bannach, Gilbert; Rodrigues, E. C.; Ionashiro, Massao
Contribuinte(s)

Universidade Estadual Paulista (UNESP)

Data(s)

20/05/2014

20/05/2014

01/06/2008

Resumo

Solid-state Ln(L)(3) compounds, where Ln stands for trivalent Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and Y and L is 2-methoxybenzoate have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results provided information on the composition, dehydration, coordination mode, structure, thermal behaviour and thermal decomposition.

Formato

945-951

Identificador

http://dx.doi.org/10.1007/s10973-007-8546-1

Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 92, n. 3, p. 945-951, 2008.

1388-6150

http://hdl.handle.net/11449/40745

10.1007/s10973-007-8546-1

WOS:000257023200048

Idioma(s)

eng

Publicador

Springer

Relação

Journal of Thermal Analysis and Calorimetry

Direitos

closedAccess

Palavras-Chave #characterization #heavier lanthanides #2-methoxybenzoate #thermal behaviour
Tipo

info:eu-repo/semantics/article