Preparative separation of the naphthopyranone glycosides by high-speed counter-current chromatography


Autoria(s): dos Santos, L. C.; Vilegas, Wagner
Contribuinte(s)

Universidade Estadual Paulista (UNESP)

Data(s)

20/05/2014

20/05/2014

27/04/2001

Resumo

High-speed counter-current chromatography was applied to the preparative separation and purification of naphthopyranone glycosides from a crude 70% ethanolic extract of the capitula of Paepalanthus microphyllus. The solvent system used was composed of water-ethanol-ethyl acetate-hexane (10:4:10:4, v/v). This technique led to the separation of four different naphthopyranone glycosides in pure form in only 7 h. (C) 2001 Elsevier B.V. B.V. All rights reserved.

Formato

259-263

Identificador

http://dx.doi.org/10.1016/S0021-9673(01)00666-5

Journal of Chromatography A. Amsterdam: Elsevier B.V., v. 915, n. 1-2, p. 259-263, 2001.

0021-9673

http://hdl.handle.net/11449/36868

10.1016/S0021-9673(01)00666-5

WOS:000168206500027

Idioma(s)

eng

Publicador

Elsevier B.V.

Relação

Journal of Chromatography A

Direitos

closedAccess

Palavras-Chave #counter-current chromatography #preparative chromatography #Paepalanthus microphyllus #glycosides #naphthopyranones #carbohydrates
Tipo

info:eu-repo/semantics/article