Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
Contribuinte(s) |
Universidade Estadual Paulista (UNESP) |
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Data(s) |
20/05/2014
20/05/2014
01/03/1999
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Resumo |
This paper reports the separation of the indole alkaloids from the benzene extract of the root barks of Tabernaemontana hilariana (Apocynaceae). The crude alkaloid fraction was fractionated by droplet counter-current chromatography using a low polarity mixture (hexane:ethyl acetate:ethanol:water). Nine indole alkaloids (3-hydroxycoronaridine, coronaridine, voacangine, 3-(2-oxopropyl) coronaridine, voacangine hydroxyindolenine, ibogamine, voacangine pseudoindoxyl, coronaridine pseudoindoxyl and tabernanthine) were identified using thin laver chromatography gas chromatography coupled with mass spectrometry and nuclear magnetic resonance spectroscopy. Copyright (C) 1999 John Wiley & Sons, Ltd. |
Formato |
60-63 |
Identificador |
http://dx.doi.org/10.1002/(SICI)1099-1565(199903/04)10:2<60 Phytochemical Analysis. W Sussex: John Wiley & Sons Ltd, v. 10, n. 2, p. 60-63, 1999. 0958-0344 http://hdl.handle.net/11449/32273 10.1002/(SICI)1099-1565(199903/04)10:2<60 WOS:000079489900002 |
Idioma(s) |
eng |
Publicador |
Wiley-Blackwell |
Relação |
Phytochemical Analysis |
Direitos |
openAccess |
Palavras-Chave | #Tabernaemontana hilariana #Apocynacene #droplet counter-current chromatography #indole alkaloids |
Tipo |
info:eu-repo/semantics/article |