Synthesis and characterization of silver nanoparticles impregnated into bacterial cellulose


Autoria(s): de Santa Maria, Luiz Claudio; Santos, Ana L. C.; Oliveira, Philippe C.; Barud, Hernane S.; Messaddeq, Younes; Ribeiro, Sidney José Lima
Contribuinte(s)

Universidade Estadual Paulista (UNESP)

Data(s)

20/05/2014

20/05/2014

15/04/2009

Resumo

Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)

Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)

Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)

This article presents a study about the synthesis of colloidal silver (Ag)/biopolymer where Ag submicron particles were prepared in situ on bacterial cellulose (BC) produced by Gluconacetobacter xylinus. Different reducing agents were compared (hydrazine, hydroxylamine or ascorbic acid) together with the influence of gelatin or polyvinylpyrrolidone (PVP) employed as colloid protectors. Particle size distribution and morphology were investigated by scanning electron microscope (SEM). SEM images show silver nanoparticles (40-100 nm) size range attached on (BC) microfibrils. XRD analyses confirmed the Ag cubic phase deposited oil to BC fibrils. The ash contents determined by thermogravimetric analyses have indicated high level of silver loading oil the obtained composites. (c) 2009 Elsevier B.V. All rights reserved.

Formato

797-799

Identificador

http://dx.doi.org/10.1016/j.matlet.2009.01.007

Materials Letters. Amsterdam: Elsevier B.V., v. 63, n. 9-10, p. 797-799, 2009.

0167-577X

http://hdl.handle.net/11449/26138

10.1016/j.matlet.2009.01.007

WOS:000264238200022

Idioma(s)

eng

Publicador

Elsevier B.V.

Relação

Materials Letters

Direitos

closedAccess

Palavras-Chave #Bacterial cellulose #Silver nanoparticles #Nanocomposites #Electron microscopy
Tipo

info:eu-repo/semantics/article