Equipamento de baixo custo para extração em fase sólida em amostras aquosas de grande volume utilizando pressão positiva de N


Autoria(s): Sanson,Ananda L.; Baeta,Bruno E. L.; Rodrigues,Keila L. T.; Afonso,Robson J. C. F.
Data(s)

01/01/2014

Resumo

Extraction/concentration is a crucial step for the analysis of organic compounds at trace level concentrations and dispersed in complex matrices. Solid-phase extraction (SPE) is one of the techniques used for this purpose. In this work, a low cost apparatus for SPE was developed that uses nitrogen under positive pressure and ensures the maintenance of the sample flow, while also allows the simultaneous extraction of different samples without cross-contamination and sample contact with plastic materials. For the system set up, easily accessible materials were used such as hypodermic needles, stainless steel tubes, rubber stoppers, and 3-way valves from serum delivery apparatus.

Formato

text/html

Identificador

http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000100024

Idioma(s)

pt

Publicador

Sociedade Brasileira de Química

Fonte

Química Nova v.37 n.1 2014

Palavras-Chave #large volume of sample #solid phase extraction #positive pressure
Tipo

journal article