Desenvolvimento e avaliação de um porta-amostra de baixo custo para caracterização elétrica de materiais cerâmicos


Autoria(s): Lima,Luiz Rogério Pinho de Andrade; Nóbrega,Shayenne Diniz da; Vasconcelos,Carmel Suzarte Ayres; Pepe,Iuri Muniz; Soares Júnior,Luiz Carlos Simões
Data(s)

01/01/2010

Resumo

Conventional sample holder cells used to the electric characterization of ceramics at high temperature consists of an alumina tube and platinum wires and plates using a complex design. The high cost materials used in the conventional sampler holder cell were replaced by stainless steel and conventional ceramics. The sample holder was validated by characterizing yttria-stabilized-zirconia in a temperature range of 25 to 700 ºC. The results do not present variations, discontinuity or unusual noise in the electric signals. Several samples were characterized without maintenance, which demonstrates that the sample holder is electric and mechanic adequate to be used to electrical characterization of ceramics up to 700 ºC.

Formato

text/html

Identificador

http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422010000500033

Idioma(s)

pt

Publicador

Sociedade Brasileira de Química

Fonte

Química Nova v.33 n.5 2010

Palavras-Chave #sample holder #solid oxide fuel cell #impedance spectroscopy
Tipo

journal article