Degree of conversion and mechanical properties of a BisGMA : TEGDMA composite as a function of the applied radiant exposure


Autoria(s): CALHEIROS, Fernanda C.; DARONCH, Marcia; RUEGGEBERG, Frederick A.; BRAGA, Roberto R.
Contribuinte(s)

UNIVERSIDADE DE SÃO PAULO

Data(s)

19/10/2012

19/10/2012

2008

Resumo

Objective: Verify the influence of radiant exposure (H) on composite degree of conversion (DC) and mechanical properties. Methods: Composite was photoactivated with 3, 6, 12, 24, or 48 J/cm(2). Properties were measured after 48-h dry storage at room temperature. DC was determined on the flat surfaces of 6 mm x 2 mm disk-shaped specimens using FTIR. Flexural strength (FS) and modulus (FM) were accessed by three-point bending. Knoop microhardness number (KHN) was measured on fragments of FS specimens. Data were analyzed by one-way ANOVA/Tukey test, Student`s t-test, and regression analysis. Results: DC/top between 6 and 12 J/cm(2) and between 24 and 48 J/cm(2) were not statistically different. No differences between DC/top and bottom were detected. DC/bottom, FM, and KHN/top showed significant differences among all H levels. FS did not vary between 12 and 24 J/cm(2) and between 24 and 48 J/cm(2). KHN/bottom at 3 and 6 J/cm(2) was similar. KHN between top and bottom was different up to 12 J/cm(2). Regression analyses having H as independent variable showed a plateau region above 24 J/cm(2). KHN increased exponentially (top) or linearly (bottom) with DC. FS and FM increased almost linearly with DC/bottom up to 55% conversion. Conclusions: DC and mechanical properties increased with radiant exposure. Variables leveled off at high H levels. (C) 2007 Wiley Periodicals, Inc.

Identificador

JOURNAL OF BIOMEDICAL MATERIALS RESEARCH PART B-APPLIED BIOMATERIALS, v.84B, n.2, p.503-509, 2008

1552-4973

http://producao.usp.br/handle/BDPI/25816

10.1002/jbm.b.30897

http://dx.doi.org/10.1002/jbm.b.30897

Idioma(s)

eng

Publicador

WILEY-LISS

Relação

Journal of Biomedical Materials Research Part B-applied Biomaterials

Direitos

restrictedAccess

Copyright WILEY-LISS

Palavras-Chave #radiant exposure #composite #mechanical properties #degree of conversion #LIGHT-ACTIVATED COMPOSITES #RESIN-BASED COMPOSITE #CONTRACTION STRESS #ENERGY DENSITY #VISIBLE-LIGHT #CURING UNITS #DENTAL RESIN #POLYMERIZATION CONTRACTION #CURE #INTENSITY #Engineering, Biomedical #Materials Science, Biomaterials
Tipo

article

original article

publishedVersion