Rapid Screening and Identification of Polar Constituents from Brazilian Arnica Lychnophora sp by LC-UV/DAD-ESI-MS and LC-UV/DAD-ESI-MS/MS Analysis
Contribuinte(s) |
UNIVERSIDADE DE SÃO PAULO |
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Data(s) |
19/10/2012
19/10/2012
2009
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Resumo |
This paper describes an analytical method for the rapid screening and identification of the phenolic constituents present in the polar extracts of different Lychnophora spp. using LC-UV/DAD-ESI-MS and LC-UV/DAD-ESI-MS/MS. Compounds were identified based on UV, retention time, MS experiments and MS/MS of precursor ion or standard. On-line phytochemical investigation of Lychnophora spp. allowed for the identification of flavonoids, chlorogenic acid derivatives and lactones. Some of the observed compounds were for the first time identified in Lychnophora species in a fast analytical procedure. The data obtained here may be helpful to the investigation of polar constituents from other Lychnophora species. |
Identificador |
CHROMATOGRAPHIA, v.69, p.157-165, 2009 0009-5893 http://producao.usp.br/handle/BDPI/20035 10.1365/s10337-009-1036-9 |
Idioma(s) |
eng |
Publicador |
VIEWEG |
Relação |
Chromatographia |
Direitos |
restrictedAccess Copyright VIEWEG |
Palavras-Chave | #Column liquid chromatography-mass spectrometry #Lychnophora #Chlorogenic acid derivatives #Flavonoid #Natural products #TANDEM MASS-SPECTROMETRY #SESQUITERPENE LACTONES #CHLOROGENIC ACIDS #PHENOLIC-COMPOUNDS #FLAVONOIDS #ERICOIDES #ASTERACEAE #ANTIOXIDANTS #GLYCOSIDES #PLANTS #Biochemical Research Methods #Chemistry, Analytical |
Tipo |
article original article publishedVersion |