Rapid Screening and Identification of Polar Constituents from Brazilian Arnica Lychnophora sp by LC-UV/DAD-ESI-MS and LC-UV/DAD-ESI-MS/MS Analysis


Autoria(s): MORAES, Solange Leite de; GREGORIO, Luiz Elidio; TOMAZ, Jose Carlos; LOPES, Norberto Peporine
Contribuinte(s)

UNIVERSIDADE DE SÃO PAULO

Data(s)

19/10/2012

19/10/2012

2009

Resumo

This paper describes an analytical method for the rapid screening and identification of the phenolic constituents present in the polar extracts of different Lychnophora spp. using LC-UV/DAD-ESI-MS and LC-UV/DAD-ESI-MS/MS. Compounds were identified based on UV, retention time, MS experiments and MS/MS of precursor ion or standard. On-line phytochemical investigation of Lychnophora spp. allowed for the identification of flavonoids, chlorogenic acid derivatives and lactones. Some of the observed compounds were for the first time identified in Lychnophora species in a fast analytical procedure. The data obtained here may be helpful to the investigation of polar constituents from other Lychnophora species.

Identificador

CHROMATOGRAPHIA, v.69, p.157-165, 2009

0009-5893

http://producao.usp.br/handle/BDPI/20035

10.1365/s10337-009-1036-9

http://dx.doi.org/10.1365/s10337-009-1036-9

Idioma(s)

eng

Publicador

VIEWEG

Relação

Chromatographia

Direitos

restrictedAccess

Copyright VIEWEG

Palavras-Chave #Column liquid chromatography-mass spectrometry #Lychnophora #Chlorogenic acid derivatives #Flavonoid #Natural products #TANDEM MASS-SPECTROMETRY #SESQUITERPENE LACTONES #CHLOROGENIC ACIDS #PHENOLIC-COMPOUNDS #FLAVONOIDS #ERICOIDES #ASTERACEAE #ANTIOXIDANTS #GLYCOSIDES #PLANTS #Biochemical Research Methods #Chemistry, Analytical
Tipo

article

original article

publishedVersion