Strength improvement of LPS-SiC ceramics by oxidation treatment


Autoria(s): SIMBA, B. G.; SANTOS, C.; BONDIOLI, M. J.; STRECKER, K.; LIMA, E. S.; SILVA, M. H. Prado da
Contribuinte(s)

UNIVERSIDADE DE SÃO PAULO

Data(s)

18/10/2012

18/10/2012

2010

Resumo

In this work, SiC ceramics were liquid phase sintered (LPS), using AIN-Y(2)O(3) as additives, and oxidized at 1400 degrees C in air for up to 120 h. Oxidation was monitored by the weight gain of the samples as function of exposition time and temperature. A parabolic growth of the oxidation layer has been observed and the coefficient of the growth rate has been determined by relating the weight gain and the surface area. The effect of oxidation on strength has been determined by 4-point bending tests. Phase analysis by Xray diffraction and microstructural observation by scanning electron microscopy indicated the formation of a uniform and dense oxidation layer. The elimination of surface flaws and pores and the generation of compressive stresses in the surface resulted in a strength increase of the oxidized samples. (C) 2009 Published by Elsevier Ltd.

CAPES

CNPq

FAPESP

Identificador

INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS, v.28, n.4, p.484-488, 2010

0263-4368

http://producao.usp.br/handle/BDPI/17649

10.1016/j.ijrmhm.2009.08.004

http://dx.doi.org/10.1016/j.ijrmhm.2009.08.004

Idioma(s)

eng

Publicador

ELSEVIER SCI LTD

Relação

International Journal of Refractory Metals & Hard Materials

Direitos

closedAccess

Copyright ELSEVIER SCI LTD

Palavras-Chave #Silicon carbide #Oxidation #Parabolic growth rate #Bending strength #SILICON-CARBIDE #MECHANICAL-PROPERTIES #MICROSTRUCTURAL DEVELOPMENT #PHASE-TRANSFORMATION #BEHAVIOR #ADDITIVES #POROSITY #Materials Science, Multidisciplinary #Metallurgy & Metallurgical Engineering
Tipo

article

original article

publishedVersion