High density flux of Co nanoparticles produced by a simple gas aggregation apparatus


Autoria(s): Landi, Gabriel Teixeira; Romero, Sergio Antonio; Santos, Antonio Domingues dos
Contribuinte(s)

UNIVERSIDADE DE SÃO PAULO

Data(s)

18/04/2012

18/04/2012

2010

Resumo

Gas aggregation is a well known method used to produce clusters of different materials with good size control, reduced dispersion, and precise stoichiometry. The cost of these systems is relatively high and they are generally dedicated apparatuses. Furthermore, the usual sample production speed of these systems is not as fast as physical vapor deposition devices posing a problem when thick samples are needed. In this paper we describe the development of a multipurpose gas aggregation system constructed as an adaptation to a magnetron sputtering system. The cost of this adaptation is negligible and its installation and operation are both remarkably simple. The gas flow for flux in the range of 60-130 SCCM (SCCM denotes cubic centimeter per minute at STP) is able to completely collimate all the sputtered material, producing spherical nanoparticles. Co nanoparticles were produced and characterized using electron microscopy techniques and Rutherford back-scattering analysis. The size of the particles is around 10 nm with around 75 nm/min of deposition rate at the center of a Gaussian profile nanoparticle beam.

CNPq

FAPESP

Identificador

REVIEW OF SCIENTIFIC INSTRUMENTS, v.81, n.3, 2010

0034-6748

http://producao.usp.br/handle/BDPI/16220

10.1063/1.3355075

http://dx.doi.org/10.1063/1.3355075

Idioma(s)

eng

Publicador

AMER INST PHYSICS

Relação

Review of Scientific Instruments

Direitos

openAccess

Copyright AMER INST PHYSICS

Palavras-Chave #aggregation #cobalt #electron microscopy #nanoparticles #particle size #Rutherford backscattering #sputter deposition #CLUSTERS #Instruments & Instrumentation #Physics, Applied
Tipo

article

original article

publishedVersion