Síntese, caracterização e análise térmica dos sais de lítio, sódio e potássio do ácido palmítico e do seu éster etílico
| Contribuinte(s) |
UNIVERSIDADE DE SÃO PAULO |
|---|---|
| Data(s) |
26/03/2012
26/03/2012
2008
|
| Resumo |
Alkaline salts of the palmitic acid were synthesized and characterized from aqueous and ethanolic medium. The salts were characterized by elemental analysis (EA) and infrared spectroscopy (IR). EA and IR, being its synthesis comproved, also characterized the ethyl palmitate. All the salts and the ester were submitted to thermal analysis using thermogravimetry (TG), and differential thermal analysis (DTA) in the temperature ranging from room to 700 ºC under air dynamic atmosphere. Differential scanning calorimetry (DSC) measurements were taken from -90 ºC up to temperatures close to the starting of the decomposition temperature, determined by thermogravimetry, using heating and cooling cycles. Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES) CNPq |
| Identificador |
Química Nova, v.31, n.7, p.1722-1726, 2008 0100-4042 http://producao.usp.br/handle/BDPI/12193 10.1590/S0100-40422008000700024 http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000700024 |
| Idioma(s) |
por |
| Publicador |
Sociedade Brasileira de Química |
| Relação |
Química Nova |
| Direitos |
openAccess Copyright Sociedade Brasileira de Química |
| Palavras-Chave | #Palmitic acid #Thermal analysis #Thermogravimetry |
| Tipo |
article original article publishedVersion |