Síntese, caracterização e análise térmica dos sais de lítio, sódio e potássio do ácido palmítico e do seu éster etílico


Autoria(s): SALES, André Luis Castro de; RAMOS, Luiz Antônio; NUNES, Ronaldo Spezia; CLARO NETO, Salvador; CAVALHEIRO, Éder Tadeu Gomes
Contribuinte(s)

UNIVERSIDADE DE SÃO PAULO

Data(s)

26/03/2012

26/03/2012

2008

Resumo

Alkaline salts of the palmitic acid were synthesized and characterized from aqueous and ethanolic medium. The salts were characterized by elemental analysis (EA) and infrared spectroscopy (IR). EA and IR, being its synthesis comproved, also characterized the ethyl palmitate. All the salts and the ester were submitted to thermal analysis using thermogravimetry (TG), and differential thermal analysis (DTA) in the temperature ranging from room to 700 ºC under air dynamic atmosphere. Differential scanning calorimetry (DSC) measurements were taken from -90 ºC up to temperatures close to the starting of the decomposition temperature, determined by thermogravimetry, using heating and cooling cycles.

Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)

CNPq

Identificador

Química Nova, v.31, n.7, p.1722-1726, 2008

0100-4042

http://producao.usp.br/handle/BDPI/12193

10.1590/S0100-40422008000700024

http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000700024

http://www.scielo.br/pdf/qn/v31n7/v31n7a24.pdf

Idioma(s)

por

Publicador

Sociedade Brasileira de Química

Relação

Química Nova

Direitos

openAccess

Copyright Sociedade Brasileira de Química

Palavras-Chave #Palmitic acid #Thermal analysis #Thermogravimetry
Tipo

article

original article

publishedVersion