In-Situ, Simultaneous Irradiation and Monitoring of a Photocatalysed Organic Oxidation Reaction in a TiO2-coated NMR Tube


Autoria(s): Mills, Andrew; O'Rourke, Christopher
Data(s)

28/09/2015

Resumo

The semiconductor photocatalysed (SPC) oxidation of toluene is performed inside an NMR spectrometer and the reaction monitored simultaneously in-situ, using a fibre optic probe/diffuser to provide the UV light to activate the titania photocatalyst coating on the inside of the NMR tube. Such a system has great potential for the simple rapid screening of a wide range of SPC mediated organic reactions.

Identificador

http://pure.qub.ac.uk/portal/en/publications/insitu-simultaneous-irradiation-and-monitoring-of-a-photocatalysed-organic-oxidation-reaction-in-a-tio2coated-nmr-tube(8d445590-9e14-449b-93a5-481e0c7da1f9).html

http://dx.doi.org/10.1021/acs.joc.5b01001

Idioma(s)

eng

Direitos

info:eu-repo/semantics/closedAccess

Fonte

Mills , A & O'Rourke , C 2015 , ' In-Situ, Simultaneous Irradiation and Monitoring of a Photocatalysed Organic Oxidation Reaction in a TiO2-coated NMR Tube ' Journal of Organic Chemistry , vol 80 , pp. 10342-10345 . DOI: 10.1021/acs.joc.5b01001

Tipo

article