Determinations of MC-LR and [Dha(7)] MC-LR Concentrations and Physicochemical Properties by Liquid Chromatography-Tandem Mass Spectrometry


Autoria(s): Yu, Ting; Xie, Ping; Dai, Ming; Liang, Gaodao
Data(s)

01/11/2009

Resumo

A liquid chromatography electrospray mass spectrometry (LC/ESI/MS) method working in multiple reactions monitoring mode for the determination of trace amounts of microcystin variants (MC-LR and [Dha(7)] MC-LR) in waters was developed. The limit of quantification was 0.05 mu g/L and the limit of detection was 0.015 mu g/L for MC-LR and [Dha(7)] MC-LR, respectively. Recoveries for MCs were in the range of 68%-81%. MC-LR and [Dha(7)] MC-LR were chemically stable with similar physiochemical behavior.

A liquid chromatography electrospray mass spectrometry (LC/ESI/MS) method working in multiple reactions monitoring mode for the determination of trace amounts of microcystin variants (MC-LR and [Dha(7)] MC-LR) in waters was developed. The limit of quantification was 0.05 mu g/L and the limit of detection was 0.015 mu g/L for MC-LR and [Dha(7)] MC-LR, respectively. Recoveries for MCs were in the range of 68%-81%. MC-LR and [Dha(7)] MC-LR were chemically stable with similar physiochemical behavior.

Chinese Academy of Sciences [KZCX1-YW-14-6-1]

Identificador

http://ir.ihb.ac.cn/handle/152342/7558

http://www.irgrid.ac.cn/handle/1471x/58292

Idioma(s)

英语

Fonte

Yu, Ting; Xie, Ping; Dai, Ming; Liang, Gaodao.Determinations of MC-LR and [Dha(7)] MC-LR Concentrations and Physicochemical Properties by Liquid Chromatography-Tandem Mass Spectrometry,BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY,2009,83(5):757-760

Palavras-Chave #Environmental Sciences; Toxicology #MC-LR #[Dha(7)] MC-LR #LC-MS #Physiochemistry
Tipo

期刊论文