Separation and identification of compounds in Rhizoma chuanxiong by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry
Data(s) |
25/06/2004
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Resumo |
A comprehensive two-dimensional liquid chromatographic separation system based on the combination of a CN column and an ODS column is developed for the separation of components in a traditional Chinese medicine (TCM) Rhizoma chuanxiong. Two columns are coupled by a two-position, eight-port valve equipped with two storage loops and controlled by a computer. The effluent is detected by both the diode array detector and atmospheric pressure chemical ionization (APCI) mass spectrometer. More than 52 components in the methanol extract of R. chuanxiong were resolved and 11 of them were preliminary identified according to their UV and mass spectra. (C) 2004 Elsevier B.V. All rights reserved. |
Identificador | |
Idioma(s) |
英语 |
Fonte |
陈学国;孔亮;苏兴业;倪坚毅;付红靖;赵瑞环;邹汉法.Separation and Identification of Compounds in Rhizoma chuanxiong by Comprehensive Two-dimensional Liquid Chromatography Coupled to Mass Spectrometry,Journal of Chromatography A,2004,1040():169-178 |
Palavras-Chave | #Rhizoma chuanxiong #liquid chromatography #comprehensive two-dimensional #Chinese medicines |
Tipo |
期刊论文 |